Method and an apparatus for the detection of a tagging material in fluids

• US 10,054,565 B2
• Filed: 10/17/2017
• Issued: 08/21/2018
• Est. Priority Date: 10/23/2012
• Status: Active Grant

• Current Assignee: Koç University, Kuantag Nanoteknolojiler Gelistirme Ve Uretim A.S.
• Original Assignee: Koç University, Kuantag Nanoteknolojiler Gelistirme Ve Uretim A.S.
• Inventors: Urey, Hakan, Yagci Acar, Havva, Elbuken, Caglar, Can, Basarbatu, Akgun, Osman Vedat, Uygurmen, Fahri Kerem
• Primary Examiner(s): Kaur, Gurpreet
• Application Number:
  US15/785,441
• Publication Number:
  US 20180038826A1
• Time in Patent Office: 308 Days
• CPC Class Codes: C10L 1/003 Marking, e.g. coloration by addition of pigments
• CPC Class Codes: G01N 21/6428 Measuring fluorescence of fluorescent products of reactions or of fluorochrome labelled reactive substances, e.g. measuring quenching effects, using measuring "optrodes" in vivo A61B5/00; immunoassay G01N33/53
• CPC Class Codes: G01N 21/643 non-biological material
• CPC Class Codes: G01N 27/447 using electrophoresis
• CPC Class Codes: G01N 33/2882 Markers marking of fuels C10L1/003

Abstract

The present invention relates to a real time identification method of working/functional fluid products including a specified tagging material and an apparatus which is first capturing and then identifying the tagging material using a concentrator and an optical detector, simultaneously transferring the reading to a smart unit and finally releasing the tagging material.

Claims

1. An apparatus for real time identification of tagged working/functional fluids, comprising:

a main fluid conduit to flow a tagged working/functional fluid including a mixture of tagging materials and a working/functional fluid to be identified, the main fluid conduit connecting a fluid entry port of an equipment/machine to the apparatus;

a tagging material concentrator section located adjacent the main fluid conduit, the tagging material concentrator section including a magnetic concentrator to apply a magnetic field to capture the tagging materials in the tagging material concentrator section;

an optical measurement section including at least one light source to illuminate the tagging materials and at least one photodetector to detect emitted light from the tagging materials to determine a unique code which becomes a registration number for the working/functional fluid; and

a smart unit which is adapted to determine the identity of the working/functional fluid based on the unique code received from the optical measurement section.

2. The apparatus of claim 1, wherein the tagging materials comprise a concentrator material and a light emitting material.

3. The apparatus of claim 1, wherein the main fluid conduit has a constant cross section.

4. The apparatus of claim 1, wherein the main fluid conduit has a variable cross section.

5. The apparatus of claim 1, wherein the flow of the tagged working/functional fluid is adapted to slow down or temporarily stop at the tagging material concentrator section.

6. The apparatus of claim 1, wherein the magnetic concentrator is adapted to capture the tagging materials using magnetic field gradient.

7. The apparatus of claim 6, wherein the magnetic concentrator is a permanent magnet.

8. The apparatus of claim 6, wherein the magnetic concentrator is an electromagnet.

9. The apparatus of claim 6, wherein capturing the tagging materials is enhanced with a low flow chamber in the main fluid conduit.

10. The apparatus of claim 6, wherein capturing the tagging materials is enhanced with a mesh structure placed in the main fluid conduit.

11. The apparatus of claim 6, wherein capturing the tagging materials is enhanced with an extra pool placed in the main fluid conduit.

12. The apparatus of claim 6, wherein captured tagging materials are adapted to be released using a valve on the main fluid conduit upon completion of identification of the tagging materials in the smart unit.

13. The apparatus of claim 1, wherein the at least one photodetector is coupled with optical filters to measure the spectrum of the emitted light which provides the unique code.

14. The apparatus of claim 13, wherein the at least one photodetector has different color filters to identify different emission spectra.

15. The apparatus of claim 13, wherein the emitted light from the tagging materials is adapted to be focused and collected onto the at least one photodetector using at least one lens.

16. The apparatus of claim 1, wherein the working/functional fluid is selected from engine oils, refined petroleum products, aqueous urea solutions, heat transfer fluids, transmission and hydraulic fluids, metalworking fluids and dielectric fluids.

17. The apparatus of claim 2, wherein the concentrator material is a magnetic nanoparticle.

18. The apparatus of claim 2, wherein the light emitting material is at least one of one or more organic light emitting molecules and one or more quantum dots.

19. The apparatus of claim 2, wherein the light emitting material has an emission wavelength between 380-1100 nm.

20. The apparatus of claim 1, wherein the smart unit comprises:

a database module that stores registration numbers of approved working/functional fluids specific to the equipment/machine;

a comparison module that compares the registration number read by the at least one photodetector with the registration numbers stored in the database;

a memory module that records all events based on comparison;

a diagnostic module that receives data from the memory module; and

a transfer module that sends the data using a communication means to a receiver.