Method of delivering a dose of a fluid composition from a microfluidic delivery cartridge

• US 10,076,585 B2
• Filed: 06/20/2014
• Issued: 09/18/2018
• Est. Priority Date: 06/20/2014
• Status: Active Grant

• Current Assignee: The Procter & Gamble Company
• Original Assignee: The Procter & Gamble Company
• Inventors: Gruenbacher, Dana Paul, Bush, Stephan Gary, Neo, Teck Khim, Hunt, David S., Scheffelin, Joseph Edward, Webb, Steven L, Giusti, Domenico, Dodd, Simon, Sherman, Faiz Feisal
• Primary Examiner(s): Tran, Thien S
• Application Number:
  US14/310,367
• Publication Number:
  US 20150367014A1
• Time in Patent Office: 1,551 Days
• Field of Search: 219201, 347 7, 347 18, 347 29, 347 62, 347 85, 347 86, 347 87, 424 43, 424 761, 424 763, 424405
• CPC Class Codes: A45D 34/00 Containers or accessories specially adapted for handling liquid toiletry or cosmetic substances, e.g. perfumes
• CPC Class Codes: A61L 2209/133 Replaceable cartridges, refills
• CPC Class Codes: A61L 2209/134 Distributing means, e.g. baffles, valves, manifolds, nozzles
• CPC Class Codes: A61L 9/03 Apparatus therefor
• CPC Class Codes: A61L 9/037 comprising a wick
• CPC Class Codes: B41J 2/0458 controlling heads based on heating elements forming bubbles
• CPC Class Codes: B41J 2/04581 controlling heads based on piezoelectric elements
• CPC Class Codes: B41J 2/04588 using a specific waveform
• CPC Class Codes: B41J 2/14024 Assembling head parts
• CPC Class Codes: B41J 2/14072 Electrical connections, e.g. details on electrodes, connecting the chip to the outside...
• CPC Class Codes: B41J 2/14145 Structure of the manifold

Abstract

Microfluidic delivery systems and methods for dispensing a fluid composition into the air comprising microfluidic die and at least one heating element that is configured to receive an electrical signal comprising a certain on-time and wave form to deliver a fluid composition into the air.

Claims

1. A method of delivering a dose of a liquid composition from a microfluidic delivery refill, wherein the liquid composition comprises volatile components such that the liquid composition is defined by a boiling point temperature, and wherein the liquid composition comprises more than 50 wt. % of a perfume mixture, and wherein the microfluidic delivery refill comprises a reservoir enclosing the liquid composition and a microfluidic delivery member comprising a plurality of nozzles and a heater associated with each nozzle, wherein the microfluidic delivery member is in fluid communication with the reservoir, the method comprising:

receiving an electrical signal with one or more of the heaters of the microfluidic delivery member, wherein the electrical signal comprises a plurality of firing pulses that each alternate between a relatively low amplitude and a relatively high amplitude;

preheating the liquid composition before the heater of the microfluidic delivery member is activated, wherein the liquid composition is preheated for less than about 2 microseconds;

activating one or more non-adjacent heaters simultaneously in response to the relatively high amplitude of each of the firing pulses of the electrical signal, wherein, when the heater is activated, the temperature of the heater is greater than the boiling point temperature of the liquid composition, wherein only non-adjacent heaters are simultaneously activated, wherein the relatively high amplitude persists for a fire time (tFIRE) in each of the firing pulses, wherein the tFIRE is less than about 4 microseconds;

activating one or more of the heaters of the microfluidic delivery member in sequence in response to the relatively high amplitude of each of the firing pulses of the electrical signal, wherein no two adjacent nozzles are ejecting fluid in sequence;

utilizing an amount of energy while each heater is activated, wherein the amount of energy is between about 33 Milliwatts and about 8.5 Watts; and

vaporizing at least a portion of the volatile components of the liquid composition when each heater is activated, whereby the dose of the liquid composition is delivered by the microfluidic delivery member.

2. The method of claim 1, wherein:

the electrical signal comprises a firing period (tON) and a non-firing period (tOFF);

the plurality of firing pulses are pulsed during the firing period (tON) with an interposed delay time (tDELAY);

the electrical signal is maintained at the relatively low amplitude during the non-firing period (tOFF) and the interposed delay time (tDELAY); and

the plurality of firing pulses are pulsed at a burst frequency between about 1000 Hertz and about 8000 Hertz.

3. The method of claim 2, wherein:

the firing period (tON) comprises a burst of the firing pulses; and

the burst consists of between about 250 and about 80,000 of the firing pulses.

4. The method of claim 1, wherein the relatively high amplitude is between about 4 volts and about 16 volts.

5. The method of claim 1, wherein the heater has a resistance less than about 100 ohms.

6. The method of claim 1, wherein the dose delivered by the microfluidic delivery member is less than about 50 picoliters.

7. The method of claim 1, further comprising:

delivering additional doses of the liquid composition with the microfluidic delivery member, wherein the liquid composition is delivered at a rate between about 2 milligrams/hour and about 180 milligrams/hour.

8. The method of claim 1, wherein the boiling point temperature of the liquid composition is less than about 250°

Celsius.