Systems and methods for producing a sugar stream

• US 10,119,157 B2
• Filed: 08/05/2016
• Issued: 11/06/2018
• Est. Priority Date: 07/23/2015
• Status: Active Grant

• Current Assignee: Fluid Quip Technologies, LLC
• Original Assignee: Fluid Quip Process Technologies, LLC
• Inventors: Jakel, Neal, Kwik, John, Franko, Michael, Whalen, Andrew
• Primary Examiner(s): Yamasaki, Robert J
• Application Number:
  US15/230,280
• Publication Number:
  US 20170022466A1
• Time in Patent Office: 823 Days
• Field of Search: None
• CPC Class Codes: C12M 21/12 for producing fuels or solvents C12M21/04 takes precedence; liquid carbonaceous fuels C10L1/00, solid fuels C10L5/00
• CPC Class Codes: C12M 23/58 Reaction vessels connected in series or in parallel combinations of bioreactors with other apparatus, C12M43/00
• CPC Class Codes: C12M 29/04 Filters; Permeable or porous membranes or plates, e.g. dialysis
• CPC Class Codes: C12M 45/02 by mechanical forces; Stirring; Trituration; Comminuting crushing, pulverizing, disintegrating in general B02C
• CPC Class Codes: C12M 45/09 by enzymatic treatment
• CPC Class Codes: C12M 47/10 Separation or concentration of fermentation products bioreactors combined with means for distillation or extraction of liquid fuel C12M43/02
• CPC Class Codes: C12P 19/02 Monosaccharides 2-ketogulonic acid C12P7/60
• CPC Class Codes: C12P 19/14 produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase , e.g. by cellulase, hemicellulase
• CPC Class Codes: C12P 2203/00 Fermentation products obtained from optionally pretreated or hydrolyzed cellulosic or lignocellulosic material as the carbon source ethanol C12P7/10
• CPC Class Codes: C12P 7/06 Ethanol, i.e. non-beverage
• CPC Class Codes: C12P 7/10 substrate containing cellulosic material
• CPC Class Codes: C12P 7/649 Biodiesel, i.e. fatty acid alkyl esters
• CPC Class Codes: C13K 1/06 obtained by saccharification of starch or raw materials containing starch
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel
• CPC Class Codes: Y02E 50/30 Fuel from waste, e.g. synthetic alcohol or diesel

Abstract

An improved dry grind system and method for producing a sugar stream from grains or similar carbohydrate sources and/or residues, such as for biofuel production. In particular, a sugar/carbohydrate stream, which includes a desired Dextrose Equivalent (DE) where DE describes the degree of conversion of starch to dextrose (aka glucose) and/or has had removed therefrom an undesirable amount of unfermentable components, can be produced after saccharification and prior to fermentation (or other sugar conversion process), with such sugar stream being available for biofuel production, e.g., alcohol production, or other processes. In addition, the systems and methods also can involve the removal of certain grain components, e.g., corn kernel components, including protein, oil and/or fiber, prior to fermentation or other conversion systems. In other words, sugar stream production and/or grain component separation occurs on the front end of the system and method.

Claims

1. A system for producing a sugar stream, the system comprising:

a first grind device that is configured to receive and grind grain and/or grain components;

a slurry tank that is situated after the first grind device and that is configured to receive a liquid and the ground grain and/or grain components, the liquid and ground grain and/or grain components defining a slurry including starch and unfermentable components;

a liquefaction system that is situated after the slurry tank and that is configured to receive the slurry of the ground grain and/or grain components, which includes the starch and unfermentable components, and convert the starch in the slurry to oligosaccharides;

a saccharification system that is situated after the liquefaction system and that is configured to receive the slurry including the oligosaccharides, and convert the oligosaccharides to simple sugars thereby producing a stream including the simple sugars and unfermentable components;

a first separation device selected from a paddle screen, a vibration screen, a screen decanter centrifuge, a conic screen centrifuge, a pressure screen, a preconcentrator, or a filter press that is situated after the saccharification system and that is configured to receive and separate the stream into a solids portion including the unfermentable components and a liquid portion including the simple sugars;

a sugar separation device selected from a clarifier or a filtration centrifuge that is situated after the first separation device and that is configured to receive the liquid portion and separate out heavier residual protein from the liquid portion, wherein the sugar separation device is capable of producing a liquid portion, after the heavier residual protein is separated out, having a dextrose equivalent of at least 70 D.E. and a total unfermentable solids fraction that is less than or equal to 30% of the total solids content; and

a microfiltration device that is situated after the sugar separation device and that is configured to receive the liquid portion therefrom and filter out additional insoluble components from the liquid portion, wherein the microfiltration device is capable of producing a liquid portion, after microfiltration, which defines a sugar stream having a total unfermentable solids fraction that is less than or equal to 10% of the total solids content.

2. The system of claim 1 further comprising a biofuel and/or biochemical device that is situated after the microfiltration device and that is configured to receive the sugar stream and produce biofuel and/or biochemicals from the simple sugars.

3. The system of claim 1 further including a second grind device that follows the first grind device and that is configured to receive and further grind the slurry of ground grain and/or grain components.

4. The system of claim 1 wherein the sugar stream includes the simple sugars and free oil, and further comprising an oil separator that is situated after the first separation device and prior to the sugar separation device and that is configured to receive the liquid portion and separate the free oil from the liquid portion to yield an oil co-product.

5. The system of claim 4 wherein the oil separator is a mud centrifuge, a two or three phase decanter, a disc decanter, a two or three phase disc centrifuge, a flotation tank, or a dissolved air flotation tank.

6. The system of claim 4 further comprising an oil polish device that is situated after the oil separator and that is configured to receive and further purify the free oil from the oil separator to yield an oil co-product.

7. The system of claim 1 further comprising a second separation device that is situated after the first separation device and that is configured to receive and separate the solids portion into a second solids portion including unfermentable components and a second liquid portion including simple sugars.

8. The system of claim 7 further comprising a third separation device that is situated after the second separation device and that is configured to receive and separate the second solids portion into a thirds solids portion including unfermentable components and a third liquid portion including simple sugars.

9. system of claim 8 further comprising a fourth separation device that is situated after the third separation device and that is configured to receive and separate the third solids portion into a fourth solids portion, including fiber, and a fourth liquid portion.

10. The system of claim 1 wherein the unfermentable components of the solids portion includes fiber and protein, and further comprising a second separation device that is situated after the first separation device and that is configured to receive and separate the solids portion into a second solids portion, including the fiber, and a second liquid portion, including the protein, and a protein separation device that is situated after the second separation device and that is configured to receive the second liquid portion and separate out the protein from the second liquid portion to yield a protein co-product.

11. The system of claim 1 wherein the grain and/or grain component are one or more selected from the group consisting of corn, wheat, barley, sorghum, rye, rice, oats, sugar cane, tapioca, and cassava.

12. The system of claim 1 further comprising a second separation device that is situated after the first separation device and that is configured to receive and separate the solids portion into a second solids portion including unfermentable components and a second liquid portion including simple sugars, wherein the system is configured to combine the separated sugar stream from the first separation device and the separated sugar stream from the second separation device.

13. A system for producing a sugar stream, the system comprising:

a first grind device that is configured to receive and grind grain and/or grain components;

a slurry tank that is situated after the first grind device and that is configured to receive a liquid and the ground grain and/or grain components, the liquid and ground grain and/or grain components defining a slurry including starch and unfermentable components;

a liquefaction system that is situated after the slurry tank and that is configured to receive the slurry of the ground grain and/or grain components, which includes the starch and unfermentable components, and convert the starch in the slurry to oligosaccharides;

a saccharification system that is situated after the liquefaction system and that is configured to receive the slurry including the oligosaccharides, and convert the oligosaccharides to simple sugars thereby producing a stream including the simple sugars and unfermentable components;

a first separation device selected from a paddle screen, a vibration screen, a screen decanter centrifuge, a conic screen centrifuge, a pressure screen, a preconcentrator, or a filter press that is situated after the saccharification system and that is configured to receive and separate the stream into a solids portion including the unfermentable components and a liquid portion including the simple sugars;

a sugar separation device selected from a clarifier or a filtration centrifuge that is situated after the first separation device and that is configured to receive the liquid portion and separate out heavier residual protein from the liquid portion, wherein the sugar separation device is capable of producing a liquid portion, after the heavier residual protein is separated out, having a dextrose equivalent of at least 70 D.E. and a total unfermentable solids fraction that is less than or equal to 30% of the total solids content;

a microfiltration device that is situated after the sugar separation device and that is configured to receive the liquid portion therefrom and filter out additional insoluble components from the liquid portion, wherein the microfiltration device is capable of producing a liquid portion, after microfiltration, which defines a sugar stream having a total unfermentable solids fraction that is less than or equal to 10% of the total solids content; and

a reactor that is situated after the microfiltration device and that is configured to receive the sugar stream and produce biofuel from the simple sugars.

14. The system of claim 13 wherein the reactor is a fermenter that receives the sugar stream and produces an alcohol from the simple sugars.

15. The system of claim 13 further including a second grind device that follows the first grind device and that is configured to receive and further grind the slurry of ground grain and/or grain components.

16. The system of claim 13 wherein the sugar stream includes the simple sugars and free oil, and further comprising an oil separator that is situated after the first separation device and prior to the sugar separation device and that is configured to receive the liquid portion and separate the free oil from the liquid portion to yield an oil co-product.

17. The system of claim 16 wherein the oil separator is a mud centrifuge, a two or three phase decanter, a disc decanter, a two or three phase disc centrifuge, a flotation tank, or a dissolved air flotation tank.

18. The system of claim 16 further comprising an oil polish device that is situated after the oil separator and that is configured to receive and further purify the free oil from the oil separator to yield an oil co-product.

19. The system of claim 13 further comprising a second separation device that is situated after the first separation device and that is configured to receive and separate the solids portion into a second solids portion including unfermentable components and a second liquid portion including simple sugars.

20. The system of claim 19 further comprising a third separation device that is situated after the second separation device and that is configured to receive and separate the second solids portion into a thirds solids portion including unfermentable components and a third liquid portion including simple sugars.

21. The system of claim 20 further comprising a fourth separation device that is situated after the third separation device and that is configured to receive and separate the third solids portion into a fourth solids portion, including fiber, and a fourth liquid portion.

22. The system of claim 13 wherein the unfermentable components of the solids portion includes fiber and protein, and further comprising a second separation device that is situated after the first separation device and that is configured to receive and separate the solids portion into a second solids portion, including the fiber, and a second liquid portion, including the protein, and a protein separation device that is situated after the second separation device and that is configured to receive the second liquid portion and separate out the protein from the second liquid portion to yield a protein co-product.

23. The system of claim 13 wherein the grain and/or grain component are one or more selected from the group consisting of corn, wheat, barley, sorghum, rye, rice, oats, sugar cane, tapioca, and cassava.

24. The system of claim 13 further comprising a second separation device that is situated after the first separation device and that is configured to receive and separate the solids portion into a second solids portion including unfermentable components and a second liquid portion including simple sugars, wherein the system is configured to combine the separated sugar stream from the first separation device and the separated sugar stream from the second separation device.