Methods for manufacturing bulked continuous filament

• US 10,124,513 B2
• Filed: 07/07/2016
• Issued: 11/13/2018
• Est. Priority Date: 05/31/2012
• Status: Active Grant

• Current Assignee: Aladdin Manufacturing Corporation (Mohawk Industries Incorporated)
• Original Assignee: Mohawk Industries Incorporated
• Inventors: Clark, Thomas R.
• Primary Examiner(s): Tentoni, Leo B
• Application Number:
  US15/204,645
• Publication Number:
  US 20160318225A1
• Time in Patent Office: 859 Days
• Field of Search: 264 401, 264101, 264102, 26421122, 26421123
• CPC Class Codes: B01D 29/0095 Flat filtering elements B01D25/12, B01D25/26 take precedence
• CPC Class Codes: B07C 2501/0036 Sorting out metallic particles
• CPC Class Codes: B29B 17/00 Recovery of plastics or other constituents of waste material containing plastics; volume reduction of waste plastics, e.g. by mechanical compacting or melting disposal of solid waste B09B; chemical recovery C08J11/00
• CPC Class Codes: B29B 17/02 Separating plastics from other materials
• CPC Class Codes: B29B 2013/002 Extracting undesirable residual components, e.g. solvents, unreacted monomers, from material to be moulded
• CPC Class Codes: B29B 2013/005 Degassing undesirable residual components, e.g. gases, unreacted monomers, from material to be moulded
• CPC Class Codes: B29B 2017/0015 Washing, rinsing
• CPC Class Codes: B29B 2017/0203 Separating plastics from plastics
• CPC Class Codes: B29B 2017/0224 Screens, sieves
• CPC Class Codes: B29B 7/427 with independently driven screws rotating about the same axis, e.g. oscillating axially; with axially oscillating screws B29B7/423 takes precedence
• CPC Class Codes: B29B 7/485 with three or more shafts provided with screws
• CPC Class Codes: B29B 7/486 with screws surrounded by a casing provided with grooves or cavities
• CPC Class Codes: B29B 7/726 Measuring properties of mixture, e.g. temperature or density B29B7/724 takes precedence
• CPC Class Codes: B29B 7/7466 Combinations of similar mixers
• CPC Class Codes: B29C 2791/003 Making articles of indefinite length B29C53/48 takes precedence
• CPC Class Codes: B29C 2791/006 Using vacuum
• CPC Class Codes: B29C 2948/922 Viscosity; Melt flow index [MFI]; Molecular weight
• CPC Class Codes: B29C 2948/9238 Feeding, melting, plasticising or pumping zones, e.g. the melt itself
• CPC Class Codes: B29C 2948/9239 Screw or gear
• CPC Class Codes: B29C 2948/92514 Pressure
• CPC Class Codes: B29C 2948/92876 : Feeding, melting, plasticising or pumping zones, e.g. the melt itself
• CPC Class Codes: B29C 37/006 : Degassing moulding material or draining off gas during moulding venting means in moulds B29C33/10
• CPC Class Codes: B29C 48/05 : Filamentary, e.g. strands
• CPC Class Codes: B29C 48/144 : at the plasticising zone
• CPC Class Codes: B29C 48/145 : at a venting zone
• CPC Class Codes: B29C 48/255 : Flow control means, e.g. valves flow dividers B29C48/695
• CPC Class Codes: B29C 48/2552 : provided in the feeding, melting, plasticising or pumping zone, e.g. screw, barrel, gear-pump or ram
• CPC Class Codes: B29C 48/38 : using two or more serially arranged screws in the same barrel
• CPC Class Codes: B29C 48/385 : using two or more serially arranged screws in separate barrels
• CPC Class Codes: B29C 48/40 : using two or more parallel screws or at least two parallel non-intermeshing screws, e.g. twin screw extruders
• CPC Class Codes: B29C 48/425 : using three or more screws serially arranged screws B29C48/38, B29C48/385
• CPC Class Codes: B29C 48/43 : Ring extruders
• CPC Class Codes: B29C 48/435 : Sub-screws
• CPC Class Codes: B29C 48/44 : Planetary screws
• CPC Class Codes: B29C 48/70 : comprising means for dividing, distributing and recombining melt flows
• CPC Class Codes: B29C 48/765 : in the extruder apparatus
• CPC Class Codes: B29C 48/766 : in screw extruders
• CPC Class Codes: B29C 48/767 : through a degassing opening of a barrel
• CPC Class Codes: B29C 48/92 : Measuring, controlling or regulating
• CPC Class Codes: B29D 99/0078 : Producing filamentary materials
• CPC Class Codes: B29K 2067/003 : PET, i.e. poylethylene terephthalate
• CPC Class Codes: B29K 2105/0067 : Melt
• CPC Class Codes: B29K 2105/26 : Scrap or recycled material
• CPC Class Codes: C08J 11/04 : of polymers
• CPC Class Codes: C08J 11/06 : without chemical reactions
• CPC Class Codes: C08J 2367/02 : Polyesters derived from dicarboxylic acids and dihydroxy compounds; C08J2367/06 takes precedence
• CPC Class Codes: D01D 1/103 : De-aerating
• CPC Class Codes: D01D 1/106 : Filtering
• CPC Class Codes: D01D 5/00 : Formation of filaments, threads, or the like
• CPC Class Codes: D01D 5/08 : Melt spinning methods D01D5/0023 takes precedence
• CPC Class Codes: D01F 6/62 : from polyesters
• CPC Class Codes: D10B 2503/04 : Floor or wall coverings; Carpets
• CPC Class Codes: Y02P 20/143 : the feedstock being recycled material, e.g. plastics
• CPC Class Codes: Y02W 30/62 : Plastics recycling; Rubber recycling
• CPC Class Codes: Y02W 30/64 : Paper recycling

Abstract

A method of manufacturing bulked continuous carpet filament which, in various embodiments, comprises: (A) grinding recycled PET bottles into a group of flakes; (B) washing the flakes; (C) identifying and removing impurities, including impure flakes, from the group of flakes; (D) passing the group of flakes through an MRS extruder while maintaining the pressure within the MRS portion of the MRS extruder below about 5 millibars; (E) passing the resulting polymer melt through at least one filter having a micron rating of less than about 50 microns; and (F) forming the recycled polymer into bulked continuous carpet filament that consists essentially of recycled PET.

Claims

1. A method of manufacturing bulked continuous carpet filament, said method comprising:

(A) providing a multi-screw extruder that comprises;

a multi-screw extruder housing that defines at least six satellite screw barrels;

at least six satellite screws each mounted within a respective one of said at least six satellite screw barrels and each mounted to rotate about a respective central axis of each of said at least six satellite screws; and

a pressure regulation system that is adapted to maintain a pressure within each of said respective satellite screw barrels between about 0.5 millibars and about 5 millibars;

(B) using said pressure regulation system to reduce a pressure within said at least six satellite screw barrels to between about 0.5 millibars and about 5 millibars;

(C) while maintaining said pressure within said at least six satellite screw barrels between about 0.5 millibars and about 5 millibars, passing a melt comprising recycled polymer through said multi-screw extruder so that at least a portion of said melt is fed through each of said at least six satellite screws; and

(D) after said step of passing said melt of recycled polymer through said multi-screw extruder, forming said recycled polymer into bulked continuous carpet filament.

2. The method of claim 1, wherein said multi-screw extruder comprises a satellite screw support system that is adapted to rotate said at least six satellite screws about a main axis that is substantially parallel to each said respective central axis of each of said at least six satellite screw extruders.

3. The method of claim 2, wherein said pressure regulation system comprises a vacuum pump that is in communication with an interior chamber of said multi-screw extruder housing.

4. The method of claim 3, wherein said step of passing said melt of recycled polymer though said multi-screw extruder occurs while said at least six satellite screws are orbitally rotating about said main axis via said satellite screw support system.

5. The method of claim 4, wherein said method further comprises using said pressure regulation system to reduce said pressure within said at least six satellite screw barrels to between about 1 millibar and about 3 millibars.

6. The method of claim 5, wherein:

said multi-screw extruder housing defines at least eight satellite screw barrels;

said multi-screw extruder further comprises at least eight satellite screws each mounted within a respective one of said at least eight satellite screw barrels and mounted to rotate about a respective central axis of each of said at least eight satellite screws;

said pressure regulation system is adapted to maintain a pressure within each of said respective at least eight satellite screw barrels between about 1 millibar and about 3 millibars; and

said method further comprises;

using said pressure regulation system to reduce said pressure within said at least eight satellite screw barrels to between about 1 millibar and about 3 millibars;

while maintaining said pressure within said at least eight satellite screw barrels between about 1 millibar and about 3 millibars, passing said melt comprising recycled polymer through said multi-screw extruder so that at least a portion of said melt is fed through each of said at least eight satellite screws; and

after said step of passing said melt of recycled polymer through said multi-screw extruder, forming said recycled polymer into bulked continuous carpet filament.

7. The method of claim 6, wherein:

said multi-screw extruder comprises a vacuum attachment portion;

said multi-screw extruder defines an opening between said vacuum attachment portion and said interior chamber of said multi-screw extruder housing;

said vacuum pump is attached to said vacuum attachment portion such that said vacuum pump is in communication with said interior chamber of said multi-screw extruder via said opening.

8. The method of claim 7, wherein said at least eight satellite screw barrels are about thirty percent open to said interior chamber of said multi-screw extruder.

9. The method of claim 8, further comprising, before said step of forming said recycled polymer into bulked continuous carpet filament:

using a viscosity sensor to determine whether an intrinsic viscosity of at least a portion of said melt of recycled polymer is within a pre-determined range; and

in response to determining that said intrinsic viscosity is not within said predetermined range, adjusting said pressure regulation system to lower said pressure within said multi-screw extruder.

10. The method of claim 1, said method further comprising:

providing a plurality of polymer flakes consisting essentially of recycled PET;

washing said plurality of polymer flakes;

drying said plurality of flakes to at least substantially remove any surface moisture from said plurality of flakes; and

at least partially melting said plurality of polymer flakes to form said melt of recycled polymer.

14. The method of claim 1, wherein said multi-screw extruder comprises a satellite screw support system that is adapted to rotate said first, second, third, fourth, fifth and sixth satellite screws about a main axis, said main axis being substantially parallel to:

(a) said central axis of said first satellite screw;

(b) said central axis of said second satellite screw;

(c) said central axis of said third satellite screw;

(d) said central axis of said fourth satellite screw;

(e) said central axis of said fifth satellite screw; and

(f) said central axis of said sixth satellite screw.

15. The method of claim 14, wherein said step of passing said melt of recycled polymer through said multi-screw extruder occurs while said first, second, third, fourth, fifth, and sixth satellite screws are orbitally rotating about said main axis.

16. The method of claim 15, wherein:

said satellite screw extruder support system comprises a drum that is adapted to rotate about said main axis;

said drum defines a first screw barrel having a central axis that is substantially parallel to said main axis;

said drum defines a second screw barrel having a central axis that is substantially parallel to said main axis;

said drum defines a third screw barrel having a central axis that is substantially parallel to said main axis;

said drum defines a fourth screw barrel having a central axis that is substantially parallel to said main axis;

said drum defines a fifth screw barrel having a central axis that is substantially parallel to said main axis;

said drum defines a sixth screw barrel having a central axis that is substantially parallel to said main axis;

said first satellite screw is rotatably mounted within said first screw barrel;

said second satellite screw is rotatably mounted within said second screw barrel;

said third satellite screw is rotatably mounted within said third screw barrel;

said fourth satellite screw is rotatably mounted within said fourth screw barrel;

said fifth satellite screw is rotatably mounted within said fifth screw barrel; and

said sixth satellite screw is rotatably mounted within said sixth screw barrel.

17. The method of claim 16, wherein, after said step of passing said melt comprising recycled polymer through said multi-screw extruder, said melt has an intrinsic viscosity of between about 0.79 dL/g and about 1.00 dL/g.

21. The method of claim 1, wherein forming said recycled polymer into bulked continuous carpet filament comprises directly feeding said melt of recycled polymer into a bulked continuous filament spinning machine.

22. The method of claim 21, wherein an output of said multi-screw extruder is connected substantially directly to an input of said bulked continuous filament spinning machine.

11. A method of manufacturing bulked continuous carpet filament, said method comprising:

(A) providing a plurality of polymer flakes comprising recycled polyethylene terephthalate;

(B) washing said plurality of polymer flakes;

(C) drying said plurality of flakes to at least substantially remove any surface moisture from said plurality of flakes;

(D) at least partially melting said plurality of polymer flakes to form a melt comprising recycled polymer;

(E) providing a multi-screw extruder that defines an interior chamber and comprises;

(i) a first satellite screw that is mounted to rotate about a central axis of said first satellite screw;

(ii) a second satellite screw that is mounted to rotate about a central axis of said second satellite screw;

(iii) a third satellite screw that is mounted to rotate about a central axis of said third satellite screw;

(iv) a fourth satellite screw that is mounted to rotate about a central axis of said fourth satellite screw;

(v) a fifth satellite screw that is mounted to rotate about a central axis of said fifth satellite screw; and

(vi) a sixth satellite screw that is mounted to rotate about a central axis of said sixth satellite screw;

(F) providing at least one vacuum pump that is in operative communication with said interior chamber of said multi-screw extruder and adapted to maintain a pressure within said interior chamber of said multi-screw extruder between about 0 millibars and about 5 millibars;

(G) using said at least one vacuum pump to reduce said pressure within said interior chamber of said multi-screw extruder to between about 0 millibars and about 5 millibars;

(H) while maintaining said pressure within said interior chamber of said multi-screw extruder between about 0 millibars and about 5 millibars, passing said melt comprising recycled polymer through said multi-screw extruder so that;

(1) a first portion of said melt is fed through said first satellite screw, (2) a second portion of said melt is fed through said second satellite screw, (3) a third portion of said melt is fed through said third satellite screw, (4) a fourth portion of said melt is fed through said fourth satellite screw, (5) a fifth portion of said melt is fed through said fifth satellite screw, and (6) a sixth portion of said melt is fed through said sixth satellite screw; and

(I) after said step of passing said melt of recycled polymer through said multi-screw extruder, forming said recycled polymer into bulked continuous carpet filament.

12. The method of claim 11, wherein said bulked continuous carpet filament consists essentially of recycled polyethylene terephthalate.

13. The method of claim 11, wherein said step of passing said melt comprising recycled polymer through said multi-screw extruder so that:

(1) said first portion of said melt is fed through said first satellite screw, (2) said second portion of said melt is fed through said second satellite screw, (3) said third portion of said melt is fed through said third satellite screw, (4) said fourth portion of said melt is fed through said fourth satellite screw, (5) said fifth portion of said melt is fed through said fifth satellite screw, and (6) said sixth portion of said melt is fed through said sixth satellite screw removes substantially all water and contaminants from said melt.

23. The method of claim 11, wherein forming said recycled polymer into bulked continuous carpet filament comprises directly feeding said melt of recycled polymer into a bulked continuous filament spinning machine.

24. The method of claim 23, wherein an output of said multi-screw extruder is connected substantially directly to an input of said bulked continuous filament spinning machine.

18. A method of manufacturing bulked continuous carpet filament comprising the steps of:

(A) washing a group of polymer flakes to remove at least a portion of one or more contaminants from a surface of said flakes, said group of flakes comprising a first plurality of flakes that consist essentially of PET and a second plurality of flakes that do not consist essentially of PET;

(B) after said step of washing said first plurality of flakes;

(i) scanning said washed group of flakes to identify said second plurality of flakes,

(ii) separating said second plurality of flakes from said first plurality of flakes;

(C) after separating said second plurality of flakes from said first plurality of flakes, melting said first plurality of flakes to produce a polymer melt;

(D) providing a multi-screw extruder that extrudes material in a plurality of different extrusion streams;

(E) reducing a pressure within said multi-screw extruder to between about 0 millibars and about 5 millibars;

(F) while maintaining said pressure within said multi-screw extruder between about 0 millibars and about 5 millibars, passing said polymer melt through said multi-screw extruder so that said polymer melt is divided into at least eight extrusion streams, each having a pressure between about 0 millibars and about 5 millibars;

(G) after passing said polymer melt through said multi-screw extruder, forming said recycled polymer into bulked continuous carpet filament.

19. The method of claim 18, wherein:

said multi-screw extruder comprises;

a multi-screw extruder housing that defines at least eight satellite screw barrels; and

at least eight satellite screws each mounted within a respective one of said at least eight satellite screw barrels and mounted to rotate about a respective central axis of each of said at least eight satellite screws.

20. The method of claim 19, wherein passing said polymer melt through said multi-screw extruder so that said polymer melt is divided into at least eight extrusion streams comprises passing said polymer melt through said multi-screw extruder so that at least of portion of said polymer melt is fed through each of said at least eight satellite screws.

25. The method of claim 18, wherein forming said recycled polymer into bulked continuous carpet filament comprises directly feeding said melt of recycled polymer into a bulked continuous filament spinning machine.

26. The method of claim 25, wherein an output of said multi-screw extruder is connected substantially directly to an input of said bulked continuous filament spinning machine.