Spectral analysis with spectrum deconvolution

• US 10,126,154 B2
• Filed: 11/07/2014
• Issued: 11/13/2018
• Est. Priority Date: 11/08/2013
• Status: Active Grant

• Current Assignee: Schlumberger Technology Corporation (Schlumberger NV)
• Original Assignee: Schlumberger Technology Corporation (Schlumberger NV)
• Inventors: Chazal, Damien, Fiore, Massimiliano
• Primary Examiner(s): Porta, David
• Assistant Examiner(s): Riddick, Blake
• Application Number:
  US15/034,824
• Publication Number:
  US 20160290846A1
• Time in Patent Office: 1,467 Days
• Field of Search: 250256, 250261, 2502691, 2502693, 2502521, 250361 R, 2503561
• CPC Class Codes: E21B 47/10 Locating fluid leaks, intrusions or movements
• CPC Class Codes: G01F 1/66 by measuring frequency, phase shift or propagation time of electromagnetic or other waves, e.g. using ultrasonic flowmeters
• CPC Class Codes: G01N 23/083 the radiation being X-rays
• CPC Class Codes: G01N 23/12 the material being a flowing fluid or a flowing granular solid
• CPC Class Codes: G01N 33/2823 raw oil, drilling fluid or polyphasic mixtures hydrocarbon content of earth materials G01N33/241; prospecting G01V; drilling per se E21B
• CPC Class Codes: G01T 1/20 with scintillation detectors

Abstract

A method for inferring incident count rates of electromagnetic energy at a detector is provided. In one embodiment, the method includes transmitting electromagnetic radiation through a fluid and receiving a portion of the electromagnetic radiation at a detector. The method also includes measuring the energy spectrum of the portion of the electromagnetic radiation received by the detector and using the measured energy spectrum and a physical model of detector response to electromagnetic radiation to infer incident count rates for discrete energy levels of the portion of the electromagnetic radiation received by the detector. Additional systems, devices, and methods are also disclosed.

Claims

1. A method comprising:

transmitting electromagnetic radiation through a fluid, the electromagnetic radiation including x-ray or gamma radiation;

receiving a portion of the electromagnetic radiation at a detector; and

analyzing the fluid based on the portion of the electromagnetic radiation received at the detector, wherein analyzing the fluid includes;

measuring the energy spectrum of the portion of the electromagnetic radiation received by the detector;

using, via a processor, the measured energy spectrum and a physical model of detector response to electromagnetic radiation to infer incident count rates for discrete energy levels of the portion of the electromagnetic radiation received by the detector, wherein;

the physical model includes a detector response function that is based on physical characteristics of the detector and on a component response function for each of multiple components of a detection chain for the detector that relates inputs at each of the multiple components to corresponding outputs;

the multiple components of the detection chain include a first component and a second component that receives an output from the first component; and

the component response function for each of the multiple components of the detection chain includes a first component response function that relates an input at the first component to the output from the first component and a second component response function that relates the output from the first component, as an input to the second component, to an output from the second component; and

characterizing a physical attribute of the fluid based on the inferred incident count rates.

2. The method of claim 1, wherein using the measured energy spectrum and the physical model of detector response includes comparing the measured energy spectrum to the detector response function of the physical model to infer the incident count rates.

3. The method of claim 2, wherein comparing the measured energy spectrum to the detector response function includes performing least squares optimization of the detector response function with respect to the measured energy spectrum to infer the incident count rates.

4. The method of claim 3, wherein the physical model of detector response includes energy and resolution response models having detector-specific parameters, and the method comprises inferring the detector-specific parameters from the least squares optimization between the measured energy spectrum and the detector response function.

5. The method of claim 4, comprising calibrating the detector based on the inferred detector-specific parameters.

6. The method of claim 1, wherein the fluid is a multiphase fluid and characterizing the physical attribute of the fluid includes determining phase fractions for the multiphase fluid.

7. The method of claim 4, further comprising:

monitoring the health status of the detector using the measured spectrum.

8. An apparatus comprising:

a detector of electromagnetic radiation including x-rays or gamma rays the detector including a detection chain having a first component and a second component, wherein the second component is connected to receive an output from the first component as an input to the second component;

a multi-channel analyzer configured to measure an energy spectrum of electromagnetic radiation received by the detector; and

a controller configured to analyze, via a processor, a fluid through which the electromagnetic radiation is passed from an emitter to the detector, wherein such analysis includes deconvolving the measured energy spectrum using a physical model representative of the response of the detector to characterize the electromagnetic radiation received by the detector, the physical model representative of the response of the detector is based on physical characteristics of the detector and includes a component response function for each of multiple components of the detection chain for the detector, and the component response function for each of the multiple components of the detection chain includes a first component response function that relates an input at the first component to the output from the first component and a second component response function that relates the output from the first component, as the input to the second component, to an output from the second component.

9. The apparatus of claim 8, wherein the controller is configured to determine count rates for photons incident on the detector based on the deconvolution of the measured energy spectrum.

10. The apparatus of claim 8, wherein the detector is a solid-state detector.

11. The apparatus of claim 8, comprising a multiphase flow meter having the detector, the multi-channel analyzer, and the controller.

12. The apparatus of claim 11, wherein the controller is a flow computer operable to calculate phase fractions of the fluid passing through the multiphase flow meter based on the deconvolution of the measured energy spectrum using the physical model representative of the response of the detector.

13. The apparatus of claim 8, wherein the detector includes a shaping amplifier for providing to the multi-channel analyzer output pulses indicative of photons received by the detector.

14. The apparatus of claim 13, wherein the multi-channel analyzer includes a pile-up rejector configured to discard a shaping amplifier output pulse from the detector that is indicative of multiple photons received by the detector within a width of the shaping amplifier output pulse if a time interval between receipt of the multiple photons exceeds a threshold duration.

15. A method comprising:

emitting x-ray or gamma radiation into a fluid;

receiving photons of the x-ray or gamma radiation having different energies at a detector; and

analyzing, via a processor, the fluid based on the photons received at the detector, wherein analyzing the fluid includes;

measuring an energy spectrum of the photons;

using multiple monoenergetic response functions based on physical characteristics of the detector to derive spectral components of the energy spectrum for multiple energy levels of the photons;

measuring count rates for at least two energy levels of the received photons based on the derived spectral components, wherein measuring the count rates for the at least two energy levels of the received photons based on the derived spectral components includes inferring the count rates through comparing the measured energy spectrum with a physical model of detector response to electromagnetic radiation that includes response functions for multiple components of a detection chain of the detector, wherein;

the multiple components of the detection chain include a first component and a second component that receives an output from the first component;

the response functions for the multiple components of the detection chain include the multiple monoenergetic response functions;

the multiple monoenergetic response functions relate an input at the first component to the output from the first component; and

the response functions for the multiple components of the detection chain include a second component response function that relates the output from the first component, as an input to the second component, to an output from the second component; and

characterizing a physical attribute of the fluid based on the measured count rates.

16. The method of claim 15, wherein the fluid includes a multiphase fluid and receiving the photons at the detector includes receiving photons that have passed through the multiphase fluid in a conduit.

17. The method of claim 16, comprising calculating attenuation rates of the photons by the multiphase fluid for the at least two energy levels, wherein characterizing the physical attribute of the fluid includes calculating phase fractions of the multiphase fluid using the calculated attenuation rates.

18. A multiphase flow meter comprising:

a fluid conduit;

an emitter and a detector of electromagnetic radiation including x-rays or gamma rays, the emitter and the detector arranged with respect to the fluid conduit so as to enable the detector to receive photons transmitted from the emitter through a fluid within the fluid conduit, wherein the detector includes a detection chain having a scintillator, a photomultiplier tube, and an amplifier;

a multi-channel analyzer coupled to the detector to receive electrical signals from the amplifier and output a measured energy spectrum of the photons received by the detector; and

a flow computer encoded with a response model for the detector, the response model based on physical characteristics of the emitter and the detector, wherein the response model includes response functions for multiple components of the detection chain of the detector and the response functions include a response function for the scintillator, a response function for the photomultiplier tube, and a response function for the amplifier; and

wherein the flow computer is operable to analyze the fluid, such analysis including comparing the measured energy spectrum with the response model to infer count rates for the photons received by the detector and characterizing a physical attribute of the fluid based on the inferred count rates.

19. The multiphase flow meter of claim 18, wherein the response model includes detector energy and resolution functions having detector-specific parameters and a set of monoenergetic response functions that model response of the scintillator to photons incident on the scintillator.