Sterilization reactor and method patent application

• US 10,194,680 B2
• Filed: 03/13/2013
• Issued: 02/05/2019
• Est. Priority Date: 03/13/2013
• Status: Active Grant

• Current Assignee: Millisecond Technologies Corp.
• Original Assignee: Millisecond Technologies Corp.
• Inventors: Arofikin, Nikolay V.
• Primary Examiner(s): Nguyen, Phuong T
• Application Number:
  US13/800,100
• Publication Number:
  US 20140261017A1
• Time in Patent Office: 2,155 Days
• Field of Search: 99453, 99470, 99483, 99471, 99516, 99473-476, 99534, 426237, 426521, 426520, 426522, 426511, 426453, 426483, 426516
• CPC Class Codes: A23C 3/0375 by pulverisation of the milk, including free falling film
• CPC Class Codes: A23L 2/46 by heating
• CPC Class Codes: A23L 3/001 Details of apparatus, e.g. for transport, for loading or unloading manipulation, pressure feed valves
• CPC Class Codes: A23L 3/01 using microwaves or dielectric heating
• CPC Class Codes: A23L 3/0155 using sub- or super-atmospheric pressures, or pressure variations transmitted by a liquid or gas
• CPC Class Codes: A23L 3/16 by heating loose unpacked materials
• CPC Class Codes: B05B 1/267 the liquid or other fluent material being deflected in determined directions
• CPC Class Codes: B05B 15/62 Arrangements for supporting spraying apparatus, e.g. suction cups

Abstract

A method and device to treat liquid to reduce the amount of microorganisms in the liquid to a preselected level and/or to mitigate the growth of microorganisms are disclosed. Utilizing the method or device, liquid product is sprayed into a cavity of a reactor using a nozzle that produces a flat spray to provide means for efficient heating and treatment of the liquid.

Claims

1. A reactor for treating a liquid product by heating it, the reactor comprising:

(a) two spaced-apart walls wherein each wall has a planar interior surface, an exterior surface, and an interior cavity between the interior surfaces;

(b) an entrance to the interior cavity;

(c) one or more heating sources for each wall, wherein each of the one or more heating sources is external to the interior cavity and is configured to raise the temperature of the interior surface of each wall to a temperature equal to or greater than the highest temperature to which the liquid product is heated; and

(d) a nozzle at the entrance, the nozzle having an inlet into which the liquid product enters and an exit opening to the interior cavity and through which the liquid product enters the interior cavity, the nozzle projecting a flat stream of the liquid product into the interior cavity.

2. The reactor of claim 1 wherein the interior surfaces of the spaced-apart walls are parallel.

3. The reactor of claim 2 wherein the parallel interior surfaces of the spaced-apart walls are vertically oriented.

4. The reactor of claim 3 wherein the entrance to the interior cavity is at the top of the reactor and the flat spray is directed downward.

5. The reactor of claim 1 wherein the nozzle is centered between the interior surfaces of the spaced-apart walls.

6. The reactor of claim 1 wherein the interior surfaces are not parallel.

7. The reactor of claim 6 wherein the inner surfaces are vertically oriented.

8. The reactor of claim 7 wherein the inner surfaces each has a top and a bottom, and are closer together at the top than at the bottom.

9. The reactor of claim 7 wherein the inner surfaces each has a top and bottom and are closer together at the bottom than at the top.

10. The reactor of claim 1 that includes more than two spaced-apart walls with each spaced-apart wall having an interior surface that faces another interior surface, and each two facing interior surfaces defining an interior cavity between, there being a nozzle at the entrance of each interior cavity.

11. The reactor of claim 10 wherein there is a plurality of nozzles, and at least one nozzle is centered between each interior cavity.

12. The reactor of claim 11 wherein each nozzle is at an entrance at the top of the reactor and the nozzle projects flat spray downward into the interior cavity.

13. The reactor of claim 11 wherein at least one of the plurality of nozzles is centered between each interior cavity.

14. The reactor of claim 1 further comprising a reservoir at the bottom of the reactor to collect the liquid.

15. The reactor of claim 1 that includes one or more ports to introduce steam or hot air into the interior cavity.

16. The reactor of claim 1 wherein each interior surface is heated to between 160°

F. and 200°

F.

17. The reactor of claim 1 wherein the temperature of the interior cavity is between 48°

C. and 82°

C.

18. The reactor of claim 1 wherein the temperature of the interior cavity is between 50°

C. and 72°

C.

19. The reactor of claim 1 wherein the temperature of the interior cavity is below the pasteurization temperature of the liquid product.

20. The reactor of claim 1 wherein the liquid product pressure changes at a rate of between 10⁵ to 10¹⁰ Pa/sec as the liquid product moves through the nozzle and into the interior cavity.

21. The reactor of claim 1 wherein the liquid product pressure changes at a rate of between 10⁹ Pa/sec or more as the liquid product moves through the nozzle and into the interior cavity.

22. The reactor of claim 1 wherein the liquid product spray is in droplets of 0.3 mm in diameter or less.

23. The reactor of claim 1 wherein the speed of the liquid product spray is 10³ m/sec or more.

24. The reactor of claim 1 wherein the liquid product is heated before entering the nozzle.

25. The reactor of claim 1 wherein the heating rate of liquid product exiting the nozzle does not exceed 1100°

C./sec.

26. The reactor of claim 1 wherein the nozzle comprises a cavity, a nozzle in fluid communication with the cavity, the nozzle for creating a flat spray from a cylindrical or conical stream of liquid, a vacuum control unit in communication with the cavity, wherein the vacuum control unit and nozzle create a pressure change in the liquid product entering the inner cavity.

27. The reactor of claim 1 wherein the temperature of the liquid entering the nozzle is 10°

C.-20°

C. less than the liquid exiting the nozzle.

28. The reactor of claim 1 wherein the nozzle is attached to a wall whose inner surface helps define the inner cavity.

29. The reactor of claim 1 wherein the nozzle includes an inlet, a central portion and an outlet offset at a 45°

-90°

angle from the inlet.

30. The reactor of claim 1 wherein the nozzle includes an interior structure that comprises a flat plate that converts a generally cylindrical stream of liquid product into a flat spray.

31. The reactor of claim 1 wherein the liquid product is kept below its pasteurization temperature.