Acoustic impact particle size measurement

• US 10,309,887 B2
• Filed: 01/22/2014
• Issued: 06/04/2019
• Est. Priority Date: 01/22/2013
• Status: Active Grant

• Current Assignee: Cidra Corporate Services, Inc.
• Original Assignee: Cidra Corporate Services, Inc.
• Inventors: Newton, David V., Fernald, Mark R.
• Primary Examiner(s): Marini, Matthew G
• Application Number:
  US14/762,223
• Publication Number:
  US 20150362418A1
• Time in Patent Office: 1,959 Days
• CPC Class Codes: G01N 15/02 Investigating particle size or size distribution by measuring osmotic pressure G01N7/10; investigating sedimentation of particle suspensions G01N15/04; investigating individual particles G01N15/10
• CPC Class Codes: G01N 2015/0053 in liquids, e.g. trouble
• CPC Class Codes: G01N 2291/02408 Solids in gases, e.g. particle suspensions
• CPC Class Codes: G01N 2291/02416 Solids in liquids
• CPC Class Codes: G01N 29/046 using the echo of particles imparting on a surface; using acoustic emission of particles investigating concentration of particle suspensions G01N15/06; devices for measuring flow of solids in suspension G01F1/74
• CPC Class Codes: G01N 29/09 by measuring mechanical or acoustic impedance
• CPC Class Codes: G01N 29/14 using acoustic emission techniques echo of particles G01N29/046; measuring mechanical vibrations or acoustic waves in solids in general G01H1/00
• CPC Class Codes: G01N 29/222 Constructional or flow details for analysing fluids optoacoustic fluid cells G01N29/2425
• CPC Class Codes: G01N 29/46 by spectral analysis, e.g. Fourier analysis or wavelet analysis spectral signal processing per se G06F17/14

Abstract

Apparatus features a signal processor or processing module configured at least to: receive signaling containing information about acoustic emissions resulting from particles impacting a solid sensor element configured in a process pipe having a process fluid flowing therein, including a slurry; and determine particle sizes of solids in the process fluid, based at least partly on the signaling received. The signal processor module may also be configured to provide corresponding signaling containing information about the particle sizes of solids in the process fluid.

Claims

1. Apparatus comprising:

a solid sensor element configured in a process pipe having a process fluid flowing therein, the solid sensor element having an impact body configured to extend into the process pipe, the solid sensor element being configured to a pipe wall in a double threaded sleeve that is made from a material that has a different acoustic impedance than the impact body, the double threaded sleeve having a combination of a first threaded isolation material and a second threaded isolation material, the first threaded isolation material being threaded to the solid sensor element, the second threaded isolation material having two sides, each side having respective threads, a first side of the second threaded isolation material being threaded to the first threaded isolation material, and a second side of the second threaded isolation material being threaded to a rubber liner of the process pipe; and

a signal processor or signal processing module configured at least to;

receive signaling containing information about acoustic emissions resulting from particles impacting the solid sensor element configured in the process pipe having the process fluid flowing therein, including a slurry; and

determine corresponding signaling containing information about particle sizes of solids in the process fluid, based at least partly on the signaling received.

2. Apparatus according to claim 1, wherein the signal processor or signal processing module is configured to provide the corresponding signaling containing information about the particle sizes of solids in the process fluid.

3. Apparatus according to claim 1, wherein the signal processor or signal processing module is configured to determine a particle size distribution of the solids in the process fluid, based at least partly on the signaling received.

4. Apparatus according to claim 1, wherein the signaling contains information about particle impacts that generate acoustic impulses in the solid sensor element, which acts like a waveguide that transmits acoustic impulse energy to a transducer, including an ultrasonic transducer, in the solid sensor element.

5. Apparatus according to claim 1, wherein the apparatus comprises the solid sensor element configured with the impact body and a transducer, including an ultrasonic transducer, so that particle impacts generate acoustic impulses in the impact body, which acts like a waveguide that transmits acoustic impulse energy to the transducer.

6. Apparatus according to claim 5, wherein the frequency content of the acoustic impulse energy is a function of a particle size distribution.

7. Apparatus according to claim 5, wherein the shape and amplitude of an acoustic signal power spectral density at ultrasonic frequencies greater than 20 kHz will depend on a distribution of the particles in the process fluid.

8. Apparatus according to claim 7, wherein low frequency acoustic energy less than 10 kHz, which is dependent on environmental noise and not particle size, is isolated from an ultrasonic transducer by mechanical and electronic filtering.

9. Apparatus according to claim 1, wherein

the signaling is acoustic impulse signaling;

and

the signal processor or signal processing module is configured to convert the acoustic impulse signaling to a particle size distribution using a signal processing algorithm based at least partly on the Hertz theory of impact between solid bodies, including where contact time of the solid bodies and impulse amplitude is dependent on the diameter of the solid bodies.

10. Apparatus according to claim 9, wherein the signal processor or signal processing module is configured to make the determination by converting from a time domain to a frequency domain, where the Hertz theory indicates that a frequency content and amplitude of an acoustic impact signal will change based on a particle diameter.

11. Apparatus according to claim 9, wherein the signal processor or signal processing module is configured to determine a particle size distribution of impacting particles, based at least partly on the shape of a power spectral density spectrum being dependent on a size distribution of impacting particles.

12. Apparatus according to claim 1, wherein the solid sensor element is configured with an ultra-hard, high wear coating in order to withstand the process fluid, including a tungsten carbide plasma coating.

13. Apparatus according to claim 1, wherein the acoustic impedance of the solid sensor element substantially matches a base material of the impact body so that the solid sensor element does not act as a barrier to acoustic signaling.

14. Apparatus according to claim 1, wherein the double threaded sleeve is configured with a threaded interface having an angle that acts to disperse unwanted acoustic noise.

15. Apparatus according to claim 1, wherein the signaling contains information about the acoustic emissions in a series of snapshots, each having a predetermined time duration, and each snapshot in time containing information about acoustic energy generated by impacts from particles of all sizes in the process fluid.

16. Apparatus according to claim 15, wherein the signal processor or signal processing module is configured to calculate for each waveform collected and received a spectral density using a Discrete Fast Fourier Transform (DFFT).

17. Apparatus according to claim 16, wherein the signal processor or signal processing module is configured to smooth a frequency spectrum for each waveform using a ⅓

octave filter.

18. Apparatus according to claim 17, wherein the signal processor or signal processing module is configured to average the series of snapshots in order to smooth out variations caused by outliers.

19. Apparatus according to claim 17, wherein the signal processor or signal processing module is configured to interpret the ⅓

octave power spectrum in order to determine a particle size distribution.

20. Apparatus according to claim 19, wherein the signal processor or signal processing module is configured to determine the particle size distribution, based at least partly on some combination of a change in either:

the slope of an acoustic impact signal, or

the amplitude in particular frequency bins which changes with a mean particle size.

21. Apparatus according to claim 1, wherein the signal processor or signal processing module is configured with at least one processor and at least one memory including computer program code, and the at least one memory and computer program code is configured, with the at least one processor, to cause the apparatus at least to receive the signaling and determine the corresponding signaling containing information about the particle sizes of the solids in the process fluid, based at least partly on the signaling received.

22. Apparatus according to claim 1, wherein the process pipe includes a pipe wall and a rubber liner.

23. Apparatus according to claim 22, wherein the second threaded isolation material is threaded to the rubber liner using a threaded arrangement.

24. Apparatus according to claim 23, wherein the second threaded isolation material includes threads, the rubber liner includes corresponding threads, and the threaded arrangement includes the threads and corresponding threads coupled together.

25. Apparatus according to claim 1, wherein the first threaded isolation material has two sides, each side having respective threads, and a first side of the first threaded isolation material being threaded to the solid sensor element, and a second side of the first threaded isolation material being threaded to the second threaded isolation material.

26. Apparatus according to claim 1, wherein the apparatus is an acoustic impact particle measurement device.

27. A method comprising:

configuring a solid sensor element in a process pipe having a process fluid flowing therein, the solid sensor element having an impact body configured to extend into the process pipe, the solid sensor element being configured to a pipe wall in a double threaded sleeve that is made from a material that has a different acoustic impedance than the impact body, the double threaded sleeve having a combination of a first threaded isolation material and a second threaded isolation material, the first threaded isolation material being threaded to the solid sensor element, the second threaded isolation material having two sides, each side having respective threads, a first side of the second threaded isolation material being threaded to the first threaded isolation material, and a second side of the second threaded isolation material being threaded to a rubber liner of the process pipe; and

receiving in a signal processor or signal processing module signaling containing information about acoustic emissions resulting from particles impacting the solid sensor element configured in the process pipe having the process fluid flowing therein, including a slurry; and

determining in the signal processor or signal processing module corresponding signaling containing information about particle sizes of solids in the process fluid, based at least partly on the signaling received.

28. A method according to claim 27, wherein the method comprises providing with the signal processor or signal processing module the corresponding signaling containing information about the particle sizes of solids in the process fluid.

29. A method according to claim 27, wherein the method comprises determining in the signal processor or signal processing module a particle size distribution of the solids in the process fluid, based at least partly on the signaling received.

30. A method according to claim 27, wherein the signaling contains information about particle impacts that generate acoustic impulses in the solid sensor element, which acts like a waveguide that transmits acoustic impulse energy to a transducer, including an ultrasonic transducer, in the solid sensor element.

31. A method according to claim 27, wherein the method comprises configuring the solid sensor element with the impact body and a transducer, including an ultrasonic transducer, so that particle impacts generate acoustic impulses in the impact body, which acts like a waveguide that transmits acoustic impulse energy to the transducer.

32. Apparatus comprising:

means for configuring a solid sensor element in a process pipe having a process fluid flowing therein, the solid sensor element having an impact body configured to extend into the process pipe, the means for configuring comprising a double threaded sleeve that is made from a material that has a different acoustic impedance than the impact body, the double threaded sleeve having a combination of a first threaded isolation material and a second threaded isolation material, the first threaded isolation material being threaded to the solid sensor element, the second threaded isolation material having two sides, each side having respective threads, a first side of the second threaded isolation material being threaded to the first threaded isolation material, and a second side of the second threaded isolation material being threaded to a rubber liner of the process pipe; and

means for receiving signaling containing information about acoustic emissions resulting from particles impacting the solid sensor element configured in a process pipe having a process fluid flowing therein, including a slurry; and

means for determining corresponding signaling containing information about particle sizes of solids in the process fluid, based at least partly on the signaling received.

33. Apparatus according to claim 32, wherein the apparatus further comprises means for providing the corresponding signaling containing information about the particle sizes of solids in the process fluid.

34. Apparatus according to claim 32, wherein the means for determining particle sizes of solids in the process fluid includes determining a particle size distribution of the solids in the process fluid.