Electrically conductive, gas-sealed, aluminum-to-aluminum connection and methods of making same

• US 10,510,520 B2
• Filed: 04/25/2019
• Issued: 12/17/2019
• Est. Priority Date: 05/04/2018
• Status: Active Grant

• Current Assignee: Douglas Electrical Components, Inc.
• Original Assignee: Douglas Electrical Components, Inc.
• Inventors: Schwed, Stephen, Douglas, Edward William, Pellegrino, Stephen Diego, Rempel, Christopher
• Primary Examiner(s): Bryant, Michael C
• Application Number:
  US16/394,864
• Publication Number:
  US 20190341239A1
• Time in Patent Office: 236 Days
• CPC Class Codes: G01N 23/046 using tomography, e.g. computed tomography [CT]
• CPC Class Codes: G01T 1/185 with ionisation chamber arrangements
• CPC Class Codes: H01J 47/001 Details
• CPC Class Codes: H01J 47/005 Gas fillings H01J47/12 takes precedence; Maintaining the desired pressure within the tube
• CPC Class Codes: H01J 47/008 Drift detectors

Abstract

Various configurations of electrically conductive, gas-sealed connections between two pieces of aluminum are described along with methods of making an electrically conductive, gas-sealed connection between two pieces of aluminum.

Claims

1. An electrically conductive, gas-sealed, aluminum-to-aluminum connection comprising:

a first piece of aluminum;

a second piece of aluminum;

the first and second pieces of aluminum being electrically connected by galling between a first segment of the first piece of aluminum and a corresponding first segment of the second piece of aluminum,

a high elongation polymer, located between a second segment of the first piece of aluminum and a corresponding second segment of the second piece of aluminum, such that the second segments are spaced apart from each other, with the high elongation polymer in between, the high elongation polymer having a thickness, measured normal to one of the second segments, that is greater than 76.2 micrometers; and

wherein the combination of the first and second segments, and high elongation polymer, form a seal having a Helium gas leak rate of less than 1×

10<sup>−

8</sup> bar l/s, measured by a mass spectrometer leak detector.

2. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the thickness of the high elongation polymer is less than 500 micrometers.

3. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein at least one of the first segments includes at least one protrusion.

4. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the second segment of the first piece of aluminum is a terminal end surface.

5. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the second segment of the second piece of aluminum is a terminal end surface.

6. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the first segment of the first piece of aluminum is a terminal end surface.

7. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the first segment of the second piece of aluminum is a terminal end surface.

8. A method of making an electrically conductive, gas-sealed, connection, the method comprising:

i) applying a curable high elongation polymer to at least one of two pieces of aluminum, each having a first segment and a second segment, wherein the first segments are correspondingly positioned relative to each other, and the second segments are correspondingly positioned relative to each other, the applying being performed such that the second segment of the at least one of the two pieces of aluminum contains the high elongation polymer and the first segments are substantially free of the high elongation polymer; and

ii) causing a relative sliding motion between the first segments of the two pieces of aluminum to cause galling between the respective first segments, while the respective second segments remain spaced apart from each other, but in contact with the high elongation polymer such that, when the high elongation polymer is cured, a flexible seal will exist between the respective second segments, and the joined first and second segments will collectively form an electrically conductive, gas-sealed, connection between the first and second pieces of aluminum with a Helium gas leak rate of less than 1×

10<sup>−

8</sup> bar l/s.

9. The method of claim 8, wherein, during “

ii)”

, the respective second segments remain spaced apart from each other by a spacing greater than 76.2 micrometers and less than 500 micrometers, measured normal to the two pieces of aluminum at corresponding locations of the second segments.

10. An electrically conductive, gas-sealed, aluminum-to-aluminum connection comprising:

an aluminum tube having an open end;

an aluminum end cap;

the aluminum tube and aluminum end cap being electrically connected by galling between a first segment of the aluminum end cap and a corresponding first segment of the aluminum tube, and

a high elongation polymer, located between a second segment of the aluminum tube and a corresponding second segment of the aluminum end cap, the second segments being spaced apart from each other such that the high elongation polymer has a thickness, measured normal to one of the second segments, that is greater than 76.2 micrometers;

wherein the combination of the first and second segments, and high elongation polymer, form a seal having a Helium gas leak rate of less than 1×

10<sup>−

8</sup> bar l/s, measured by a mass spectrometer leak detector.

11. The connection of claim 10, wherein the spacing between the second segments is less than 500 micrometers when measured in a radial direction.

12. The connection of claim 10 wherein the first segments are located between the second segments and an interior volume defined by an interior wall of the aluminum tube.

13. The connection of claim 10, wherein the second segments are located between the first segments and an interior volume defined by an interior wall of the aluminum tube.

14. The connection of claim 10, wherein at least one of the first segments includes at least one protrusion.

15. The connection of claim 10, wherein at least one of the first segments is located on an interior wall of the aluminum tube.

16. The connection of claim 10, wherein at least one of the first segments is located on an exterior wall of the aluminum tube.

17. The connection of claim 10, wherein at least one of the second segments is located on an interior wall of the aluminum tube.

18. The connection of claim 10, wherein at least one of the second segments is located on an exterior wall of the aluminum tube.

19. The connection of claim 10, wherein the second segment of the aluminum tube includes a terminal end surface of the aluminum tube.

20. A method of sealing an aluminum tube to an aluminum end cap comprising:

i) applying a curable high elongation polymer to at least one of an aluminum tube or an aluminum end cap, each having a first segment and a second segment, wherein, when assembled, the first segments are correspondingly positioned relative to each other, and the second segments are correspondingly positioned relative to each other, the applying being performed such that the second segment of the at least one of the aluminum tube or aluminum end cap contains the high elongation polymer and the first segments are substantially free of the high elongation polymer; and

ii) causing a relative sliding motion between the first segments of the aluminum tube and aluminum end cap to cause galling between the respective first segments, while the respective second segments remain spaced apart from each other, but in contact with the high elongation polymer such that, when the high elongation polymer is cured, a flexible seal will exist between the respective second segments to form a gas-sealed, connection between the aluminum tube and aluminum end cap with a Helium gas leak rate of less than 1×

10<sup>−

8</sup> bar l/s, and the joined first segments form an electrically conductive path between the aluminum tube and aluminum end cap.

21. The method of claim 20 wherein, prior to“

i)”

the method further comprises;

roughening at least one of;

a) the second segment of the aluminum end cap, or

b) the second segment of the aluminum tube.