Extractor for high pressure extraction of a matrix

• US 10,625,175 B2
• Filed: 03/15/2017
• Issued: 04/21/2020
• Est. Priority Date: 04/06/2016
• Status: Expired due to Fees

• Current Assignee: Kiinja Corporation
• Original Assignee: Kiinja Corporation
• Inventors: Jackson, Gregory A.
• Primary Examiner(s): Joyner, Kevin
• Application Number:
  US15/460,113
• Publication Number:
  US 20170291120A1
• Time in Patent Office: 1,133 Days
• CPC Class Codes: B01D 11/02 of solids
• CPC Class Codes: B01D 11/0203 with a supercritical fluid
• CPC Class Codes: B01D 11/0207 Control systems
• CPC Class Codes: B01D 11/0219 Fixed bed of solid material
• CPC Class Codes: B01D 11/0288 Applications, solvents
• CPC Class Codes: B01J 3/03 Pressure vessels, or vacuum vessels, having closure members or seals specially adapted therefor
• CPC Class Codes: F16J 13/065 the clamp comprising a ring encircling the flange

Abstract

Generally, an extraction system useful in separating an extract from a matrix using one or more extractants. Specifically, an extractor including one or more of: an extraction vessel having an extractor vessel internal surface which defines an extraction chamber which communicates between open extraction vessel first and second ends, a first piston configured to sealably engage the extractor vessel internal surface of the extraction vessel first end or a second piston adapted to sealably engage the extractor vessel internal surface of the extraction vessel second end.

Claims

1. An extractor, comprising:

an extraction vessel having an internal surface which defines an extraction chamber which communicates between open extraction vessel first and second ends;

a first piston adapted to sealably engage said internal surface of said extraction vessel first end;

a first piston retaining member;

a first piston retaining member guide including a first piston retaining member guide channel in which said first piston retaining member moves to engage said first piston sealably engaged with said internal surface of said extraction vessel first end;

a first pressure receiving plate adjacently abuttingly engaging a first side of said first piston retaining member guide; and

a first end plate adjacently abuttingly engaging a second side of said first piston retaining member guide, said first end plate having a first piston aperture through which said first piston moves to sealably engage said internal surface of said extraction vessel first end.

2. The extractor of claim 1, further comprising a second piston adapted to sealably engage said internal surface of said extraction vessel second end.

3. The extractor of claim 2, further comprising:

a second piston retaining member removably engaging said second piston sealably engaged with said internal surface of said extraction vessel second end; and

a second piston retaining member guide including a second piston retaining member guide channel in which said second piston retaining member moves to engage said second piston sealably engaged with said internal surface of said extraction vessel second end.

4. The extractor of claim 3, further comprising a second pressure receiving plate adjacently abuttingly engaging a first side of said second piston retaining member guide in which said second piston retaining member moves to engage said second piston.

5. The extractor of claim 4, further comprising a second end plate adjacently abuttingly engaged to a second side of said second piston retaining member guide, said second end plate having a second piston aperture through which said second piston moves to sealably engage said internal surface of said extraction vessel second end.

6. The extractor of claim 5, further comprising first and second extraction vessel centering guides correspondingly coupled to said first and second end plate, said first and second extraction vessel centering guides each configured to engage a corresponding portion of the external surface of said extraction vessel proximate said extraction vessel first and second ends to align said internal surface of said extraction vessel first and second ends to correspondingly slidably receive said first and second pistons.

7. The extractor of claim 5, further comprising first and second connecting members interconnecting said first and second pressure receiving plates.

8. An extractor, comprising:

an extraction vessel having an internal surface which defines an extraction chamber which communicates between open extraction vessel first and second ends;

a first piston adapted to sealably engage said internal surface of said extraction vessel first end; and

a first piston actuator directly connected to said first piston, said first piston actuator including a first tubular actuator shaft connected to a first piston inlet port, said first tubular actuator shaft coupled to a first conduit adapted to convey an amount of extractant to or from said first piston inlet port, said first piston actuator operable to move said first piston to sealably engage said internal surface of said extraction vessel first end.

9. The extractor of claim 8, further comprising:

a second piston adapted to sealably engage said internal surface of said extraction vessel second end; and

a second piston actuator connected to said second piston, said second piston actuator including a second tubular actuator shaft connected to a second piston outlet port, said second tubular actuator shaft coupled to a second conduit adapted to convey an amount of extractant to or from said second piston outlet port, said second piston actuator operable to move said second piston to sealably engage said internal surface of said extraction vessel second end.

10. The extractor of claim 9, further comprising:

a first piston retaining member;

a first retaining member actuator connected to said first piston retaining member, said first retaining member actuator operable to move said first piston retaining member to engage said first piston sealably engaged with said internal surface of said extraction vessel first end.

11. The extractor of claim 10, further comprising:

a second piston retaining member;

a second retaining member actuator connected to said second piston retaining member, said second retaining member actuator operable to move said second piston retaining member to engage said second piston sealably engaged with said internal surface of said extraction vessel second end.

12. The extractor of claim 9, further comprising a fluid flow generator connected to said extraction vessel, said fluid flow generator capable of generating an extractant pressure inside of said extraction chamber of between about 500 psi to about 20,000 psi.

13. The extractor of claim 12, where said extractant pressure is selected from the group consisting of:

about 500 psi to about 1500 psi, 1000 psi to about 2000 psi, about 1500 psi to about 2500 psi, about 2000 psi to about 3000 psi, about 2500 psi to about 3500 psi, about 3000 psi to about 4000 psi, about 3500 psi to about 4500 psi, about 4000 psi to about 5000 psi, about 5500 psi to about 6500 psi, about 6000 psi to about 7000 psi, about 6500 psi to about 7500 psi, about 7000 psi to about 8000 psi, about 7500 psi to about 8500 psi, about 8000 psi to about 9000 psi, about 8500 psi to about 9500 psi, about 9000 psi to about 10,000 psi, about 9500 psi to about 10,500 psi, about 10,000 psi to about 11,000 psi, about 10,500 psi to about 11,500 psi, about 11,000 psi to about 12,000 psi, about 11,500 psi to about 12,500 psi, about 12,000 psi to about 13,000 psi, about 12,500 psi to about 13,500 psi, about 13,000 psi to about 14,000 psi, about 13,500 psi to about 14,500 psi, about 14,000 psi to about 15,000 , about 14,500 to about 15,500 psi, about 15,000 psi to about 15,500 psi, about 15,500 psi to about 16,500 psi, about 16,000 psi to about 17,000 psi, about 16,500 psi to about 17,500 psi, about 17,000 psi to about 18,000 psi, about 17,500 psi to about 18,500 psi, about 18,000 psi to about 19,000, about 18,500 psi to about 19,500 psi, and about 19,000 psi to about 20,000 psi, or combinations thereof over a period of time.

14. The extractor of claim 12, further comprising a heat source coupled to said extraction vessel external surface.

15. The extractor of claim 14, further comprising a temperature adjustment element coupled to said heat source, said temperature adjustment element allows pre-selection of an extraction vessel temperature of between about 5°

C. to about 155°

C.

16. The extractor of claim 15, wherein said extraction vessel temperature is selected from the group consisting of:

about 5°

C. to about 15°

C., about 10°

C. to about 20°

C., about 15°

C. to about 25°

C., about 20°

C. to about 30°

C., about 25°

C. to about 35°

C., about 30°

C. to about 40°

C., about 35°

C. to about 45°

C., about 40°

C. to about 50°

C., about 55°

C. to about 65°

C., about 60°

C. to about 70°

C., about 65°

C. to about 75°

C., about 70°

C. to about 80°

C., about 75°

C. to about 85°

C., about 80°

C. to about 90°

C., about 85°

C. to about 95°

C., about 90°

C. to about 100°

C., about 95°

C. to about 105°

C., about 100°

C. to about 110°

C., about 105°

C. to about 115°

C., about 110°

C. to about 120°

C., about 115°

C. to about 125°

C., about 120°

C. to about 130°

C., about 125°

C. to about 135°

C., about 130°

C. to about 145°

C., about 140°

C. to about 155°

C., or combinations thereof over a period of time.

17. An extractor, comprising;

A first piston and a second piston;

An extraction vessel having an internal surface which defines an extraction chamber which communicates between open extraction vessel first and second ends, said extraction vessel first and second ends each having an internal surface configured to correspondingly slidably receive said first and second pistons;

an extraction vessel support including an extraction vessel rotation element, said extraction vessel rotatable about an extraction vessel support axis of said extraction vessel support to position a longitudinal axis of said extraction vessel in a generally horizontal orientation.

18. The extractor of claim 17, further comprising a vessel actuator connected to said extraction vessel, said vessel actuator operable to move said extraction vessel to align said internal surface of said extraction vessel first and second ends to correspondingly slidably receive said first and second pistons.

19. The extractor of claim 18, further comprising first and second extraction vessel centering guides each configured to engage a corresponding portion of an external surface of said extraction vessel proximate said extraction vessel first and second ends to align said internal surface of said extraction vessel first and second ends to correspondingly slidably receive said first and second pistons.