Automated soil measurement

• US 10,641,756 B2
• Filed: 12/05/2017
• Issued: 05/05/2020
• Est. Priority Date: 08/03/2012
• Status: Active Grant

• Current Assignee: Winfield Solutions LLC (Land O'Lakes Incorporated)
• Original Assignee: Winfield Solutions LLC (Land O'Lakes Incorporated)
• Inventors: Gerber-Siff, Bevan, White, Justin, Prouty, Stephen, Tirrell, Robert, Preiner, Michael, Koshnick, Nicholas
• Primary Examiner(s): Rogers, David A
• Application Number:
  US15/832,512
• Publication Number:
  US 20180224419A1
• Time in Patent Office: 882 Days
• CPC Class Codes: B01D 29/00 Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
• CPC Class Codes: G01N 1/4077 by other techniques involving separation of suspended solids
• CPC Class Codes: G01N 2001/4088 filtration
• CPC Class Codes: G01N 2035/00475 Filters
• CPC Class Codes: G01N 33/24 Earth materials G01N33/42 takes precedence
• CPC Class Codes: G01N 33/245 for agricultural purposes
• CPC Class Codes: G01N 35/1095 for supplying the samples to flow-through analysers for a specific analyser see relevant groups, e.g. under G01N15/00, G01N21/00, G01N27/00, G01N30/00, H01J49/00

Abstract

A filtration system for a soil analysis device and methods of pressure filtration and automated cleaning are disclosed for generating filtrate used in measuring characteristics of a soil sample and preparing the filtration system for repeated measurements. A mixing chamber combines a soil sample and an extractant into a liquid mixture. The filtration system receives and pressure filters the liquid mixture to quickly generate filtrate used to measure characteristics of the sample. The filtrate is passed to a measurement cell for analysis. Once the analysis is complete, the filtration system performs a cleaning process in preparation to receive a subsequent liquid mixture from another soil sample.

Claims

1. A filtration system of a soil analysis device, the filtration system comprising:

a chamber including a liquid mixture inlet and a filtrate drain;

a filter configured to remove particulates from a liquid mixture received from the liquid mixture inlet to generate a filtered liquid mixture, the filter oriented in a substantially vertical orientation and partitioning the chamber into a first chamber configured to receive the liquid mixture from the liquid mixture inlet and a second chamber configured to receive the filtered liquid mixture from the filter and provide the filtered liquid mixture to the filtrate drain, the filter including a perforated area located below the liquid mixture inlet and above the filtrate drain; and

a pressure source configured to create a pressure differential between the first chamber and the second chamber.

2. The filtration system of claim 1, wherein the filter includes a non-perforated area located above the perforated area.

3. The filtration system of claim 1, wherein the filter includes a non-perforated area located below the perforated area.

4. The filtration system of claim 1, wherein the perforated area is located in a central region of the filter.

5. The filtration system of claim 1, wherein the perforated area extends the full width of the filter.

6. The filtration system of claim 1, wherein the liquid mixture inlet is located at a top of the first chamber.

7. The filtration system of claim 1, wherein the filtrate drain is located at a bottom of the second chamber.

8. The filtration system of claim 1, further comprising a liquid mixture drain located at a bottom of the first chamber.

9. The filtration system of claim 8, further comprising a valve configured to selectively open and close the liquid mixture drain.

10. The filtration system of claim 8, wherein the liquid mixture drain is larger in size than the filtrate drain.

11. The filtration system of claim 1, further comprising a cleaner inlet located at a top of the second chamber.

12. The filtration system of claim 11, wherein the liquid mixture inlet is larger in size than the cleaner inlet.

13. The filtration system of claim 11, wherein the cleaner inlet is coupled to a cleaning fluid container containing a cleaning fluid.

14. The filtration system of claim 13, wherein the pressure source is configured to force the cleaning fluid through the filter to dislodge particulates caught in the filter.

15. The filtration system of claim 1, wherein the pressure source includes an air source coupled to at least one of the first chamber or the second chamber for forcing the liquid mixture through the filter by creating the pressure differential across the filter.

16. The filtration system of claim 15, wherein the air source is either:

coupled to the first chamber and is configured to increase the pressure in the first chamber to force the liquid mixture through the filter;

or

coupled to the second chamber and is configured to create a vacuum in the second chamber to force the liquid mixture through the filter.

17. The filtration system of claim 1, further comprising a measurement cell coupled to the filtrate drain and configured to analyze the filtered liquid mixture.

18. The filtration system of claim 17, wherein the measurement cell comprises a light source and one or more optical detectors for measuring at least one of an attenuation of light generated by the light source and passing through the filtered liquid mixture or a reflection spectrum of light generated by the light source and passing through the liquid mixture.

19. The filtration system of claim 1, wherein the liquid mixture comprises a portion of a soil sample mixed with an extractant.

20. A method comprising:

receiving, in a first chamber of a soil analysis device, a liquid mixture from a liquid mixture inlet;

generating a pressure differential across a filter separating the first chamber from a second chamber of the soil analysis device, the pressure differential causing the liquid mixture in the first chamber to pass through a perforated area of the filter located below the liquid mixture inlet and above a filtrate drain of the second chamber, the filter configured to remove particulates from the liquid mixture to create a filtered liquid mixture received in the second chamber; and

analyzing the filtered liquid mixture using a measurement cell coupled to the filtrate drain.