Parallel flow reactor having variable composition
First Claim
1. A parallel flow reaction system for effecting four or more simultaneous reactions in four or more reaction channels, the reaction system comprising four or more reactors, each of the four or more reactors comprising a surface defining a reaction cavity for carrying out a chemical reaction, an inlet port in fluid communication with the reaction cavity, and an outlet port in fluid communication with the reaction cavity, and a fluid distribution system for simultaneously supplying a feed composition comprising at least two feed components in varying relative amounts to the reaction cavity of each of the four or more reactors, and for discharging a reactor effluent from the outlet port of each such reaction cavity to one or more effluent sinks, the fluid distribution system comprising a feed-composition subsystem that comprises four or more mixing zones, each of the four or more mixing zones being in fluid communication with one of the four or more reactors, a first feed component source in fluid communication with each of the four or more mixing zones, a set of four or more first-feed-component flow restrictors, each of the four or more first-feed-component flow restrictors providing fluid communication between the first feed component source and one of the four or more mixing zones, each of the four or more first-feed-component flow restrictors having a flow resistance that varies relative to other first-feed-component flow restrictors in the set, and a second feed component source in fluid communication with each of the four or more mixing zones.
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Abstract
Parallel flow reaction systems comprising four or more reaction channels are disclosed. Distribution systems, and parallel flow reaction systems comprising such distribution systems are also disclosed. Specifically, the distribution systems comprise a feed-composition subsystem for providing a different feed composition to each of the four or more reactors. In preferred embodiments, the feed composition subsystem comprises at least one set of four or more feed-component flow restrictors, each of the four or more feed-component flow restrictors having a flow resistance that varies relative to other flow restrictors in the set.
129 Citations
76 Claims
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1. A parallel flow reaction system for effecting four or more simultaneous reactions in four or more reaction channels, the reaction system comprising
four or more reactors, each of the four or more reactors comprising a surface defining a reaction cavity for carrying out a chemical reaction, an inlet port in fluid communication with the reaction cavity, and an outlet port in fluid communication with the reaction cavity, and a fluid distribution system for simultaneously supplying a feed composition comprising at least two feed components in varying relative amounts to the reaction cavity of each of the four or more reactors, and for discharging a reactor effluent from the outlet port of each such reaction cavity to one or more effluent sinks, the fluid distribution system comprising a feed-composition subsystem that comprises four or more mixing zones, each of the four or more mixing zones being in fluid communication with one of the four or more reactors, a first feed component source in fluid communication with each of the four or more mixing zones, a set of four or more first-feed-component flow restrictors, each of the four or more first-feed-component flow restrictors providing fluid communication between the first feed component source and one of the four or more mixing zones, each of the four or more first-feed-component flow restrictors having a flow resistance that varies relative to other first-feed-component flow restrictors in the set, and a second feed component source in fluid communication with each of the four or more mixing zones.
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50. A method for evaluating a chemical reaction process, the method comprising
feeding a first feed component from a first feed component source to four or more mixing zones, each of the four or more mixing zones being in fluid communication with one of four or more reactors, the first feed component being fed through a set of four or more first-feed-component flow restrictors, each of the four or more first-feed-component flow restrictors providing fluid communication between the first feed component source and one of the four or more mixing zones, each of the four or more first-feed-component flow restrictors having a flow resistance that varies relative to other first-feed-component flow restrictors in the set, and feeding a second feed component from a second feed component source to the four or more mixing zones to form four or more feed compositions having varying relative amounts of the first and second feed components, simultaneously supplying the four or more varying feed compositions to the four or more reactors, controlling the reaction conditions in each of the four or more reaction cavities to effect a chemical reaction of interest, and discharging a reactor effluent from each of the four or more microreactors.
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58. A reaction system for effecting a chemical reaction, the reaction system comprising
one or more reactors, each of one or more reactors comprising a surface defining a reaction cavity for carrying out a chemical reaction, an inlet port in fluid communication with the reaction cavity, and optionally, an outlet port in fluid communication with the reaction cavity, and a fluid distribution system for selectively supplying a plurality of different feed compositions to the one or more reactors, each of the plurality of different feed compositions comprising at least two feed components in varying relative amounts, and optionally, for discharging a reactor effluent from the optional outlet port of the one or more reactors to one or more effluent sinks, the fluid distribution system comprising a feed-composition subsystem that comprises two or more mixing zones, each of the two or more mixing zones being in selectable fluid communication with the one or more reactors, a first feed component source in fluid communication with each of the two or more mixing zones, a set of two or more first-feed-component flow restrictors, each of the two or more first-feed-component flow restrictors providing fluid communication between the first feed component source and one of the two or more mixing zones, each of the two or more first-feed-component flow restrictors having a flow resistance that varies relative to other first-feed-component flow restrictors in the set, and a second feed component source in fluid communication with each of the two or more mixing zones.
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60. A fluid distribution system for simultaneously forming four or more fluid compositions comprising at least two or more components in varying relative amounts, the fluid distribution system comprising
four or more mixing zones for forming the four or more fluid compositions, a first feed component source in fluid communication with each of the four or more mixing zones, a set of four or more first-feed-component flow restrictors, each of the four or more first-feed-component flow restrictors providing fluid communication between the first feed component source and one of the four or more mixing zones, each of the four or more first-feed-component flow restrictors having a flow resistance that varies relative to other first-feed-component flow restrictors in the set, and a second feed component source in fluid communication with each of the four or more mixing zones.
Specification