On-site analyzer
First Claim
1. An apparatus for analyzing a fluid sample to determine constituents thereof comprising:
- a housing;
a transfer assembly having an inlet configured to receive the fluid sample, said transfer assembly being configured to selectively flow the fluid sample to an outlet thereof;
an infrared (IR) spectral analyzer assembly disposed in said housing and coupled to said outlet, said IR spectral analyzer assembly being configured to analyze the fluid sample and generate a first data set;
an optical emission spectrometer (OES) assembly disposed in said housing and coupled to said outlet, said OES assembly being configured to analyze the fluid sample and generate a second data set substantially continuously valued over at least a first predetermined wavelength range;
a controller connected to said transfer assembly, said IR spectral assembly, and said OES assembly and configured to control the operation of said apparatus in accordance with a predetermined operating strategy, said controller being configured to determine constituents of the fluid sample in accordance with said first and second data sets.
4 Assignments
0 Petitions
Accused Products
Abstract
An apparatus (10) for analyzing lubricant oils and functional fluids includes an optical emission spectrometer (OES) (26) having a substantially continuously valued wavelength versus intensity output (140). The OES (26) analyzes light captured from a spark emission stand (58) through which the fluid sample is flowed. An expert system (160-172) operates according to a set of Rules, and generates diagnostic text (174) for an operator based on the information about the fluid sample provided by the OES (26) and other measurement devices. The apparatus (10) is reduce in size, weight and cost.
20 Citations
26 Claims
-
1. An apparatus for analyzing a fluid sample to determine constituents thereof comprising:
-
a housing;
a transfer assembly having an inlet configured to receive the fluid sample, said transfer assembly being configured to selectively flow the fluid sample to an outlet thereof;
an infrared (IR) spectral analyzer assembly disposed in said housing and coupled to said outlet, said IR spectral analyzer assembly being configured to analyze the fluid sample and generate a first data set;
an optical emission spectrometer (OES) assembly disposed in said housing and coupled to said outlet, said OES assembly being configured to analyze the fluid sample and generate a second data set substantially continuously valued over at least a first predetermined wavelength range;
a controller connected to said transfer assembly, said IR spectral assembly, and said OES assembly and configured to control the operation of said apparatus in accordance with a predetermined operating strategy, said controller being configured to determine constituents of the fluid sample in accordance with said first and second data sets. - View Dependent Claims (2, 3, 6, 7, 8, 9, 10)
-
- 4. The apparatus of claim 4 wherein said sample cell comprises zinc selenide material.
-
11. A sample flow cell assembly for an infrared (IR) spectral analyzer comprising:
-
a body having a first bore and a second bore;
a sample cell disposed in said first bore and including an inlet and an outlet for sample fluid flow therethrough, said sample cell including a first normal axis associated therewith; and
,a compensator window disposed in said second bore, said compensator window including a second normal axis associated therewith;
said compensator window and said sample cell each being arranged such that said first and second normal axes define a predetermined tilt angle relative to a principal axis along which an IR source generates an IR radiation beam, said compensator window and said sample cell each having a respective effective thickness and index of refraction that are substantially equal. - View Dependent Claims (12, 14, 15, 16, 17, 19, 20, 21, 22, 24, 25, 26)
-
-
13. A method of regularizing a sample spectrum of a fluid sample generated by a spectrometer having a pair of electrodes, the method comprising the steps of:
-
(A) defining a background spectrum having a plurality of spectral features indicative at least in part of the composition of the electrodes;
(B) selecting at least a first background spectral feature from said plurality of spectral features wherein the first background spectral feature has a predetermined wavelength value associated therewith;
(C) determining a measured wavelength value of the at least first background spectral feature in the sample spectrum; and
,(D) translating the sample spectrum with respect to wavelength in accordance with said predetermined wavelength value, said measured wavelength value, and a predetermined translation strategy.
-
-
18. A method of normalizing an intensity of a sample spectrum of a fluid sample by a spectrometer having a pair of electrodes, the method comprising the steps of:
-
(A) selecting a background spectral feature from a plurality of spectral features of a background spectrum that is indicative at least in part of the composition of the electrodes wherein the background spectral feature has an intensity variation characteristic; and
,(B) transforming the sample spectrum with respect to intensity in accordance with an intensity of said selected background spectral feature as indicated in the sample spectrum.
-
-
23. A method of analyzing a sample spectrum of one of lubricating oil sample and a functional fluid sample having one or more constituent elements wherein the sample spectrum is generated by a spectrometer having a pair of electrodes, the method comprising the steps of:
-
(A) translating the sample spectrum with respect to wavelength in accordance with a first background spectral feature having a known wavelength selected from a background spectrum having a plurality of spectral features indicative at least in part of the composition of the electrodes;
(B) determining an intensity of a second background spectral feature having an intensity variation characteristic;
(C) determining an intensity of a characteristic emission line associated with at least one of the constituent elements;
(D) transforming the constituent element intensity into a concentration parameter using (i) the intensity of the second background spectral feature in the sample spectrum, (ii) the intensity of the constituent emission line, and (iii) predetermined data.
-
Specification