METHOD AND APPARATUS FOR MONITORING A FLUID SYSTEM

• US 20030173272A1
• Filed: 03/13/2002
• Published: 09/18/2003
• Est. Priority Date: 03/13/2002
• Status: Active Grant

• Current Assignee: Dionex Corporation (Thermo Fisher Scientific Incorporated)
• Original Assignee: Dionex Corporation (Thermo Fisher Scientific Incorporated)
• Inventors: Staffler, Michael
• Granted Patent: US 6,623,630 B1
• Time in Patent Office: Days
• US Class Current: 210/87
• CPC Class Codes: F04B 11/0058 with piston speed control
• CPC Class Codes: F04B 2205/13 Pressure pulsations after the pump
• CPC Class Codes: G01M 3/26 by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors
• CPC Class Codes: G01N 2030/326 pumps
• CPC Class Codes: G01N 30/36 in high pressure liquid systems

Abstract

An apparatus for monitoring a fluid system particularly suited for use with high pressure liquid chromatography systems. The apparatus monitors seal leakage as well as the general wellness of the apparatus and can thus be used to provide preventive maintenance feedback. The apparatus includes a liquid chamber, a wash chamber, a reservoir, a supply pump, a return line, and a detector. The liquid chamber includes a seal for sealing a fluid within the liquid chamber. The wash chamber is located adjacent the seal. The reservoir supplies a wash solution to the wash chamber. The supply pump supplies a unidirectional flow of wash solution from the reservoir to the wash chamber. The return line conveys a return flow from the wash chamber to the reservoir, in which the return flow includes any leakage of the fluid from the liquid chamber into the wash chamber and the portion of the wash solution that returns from the wash chamber to the reservoir. The detector determines whether there is a differential between the unidirectional flow and the return flow. A method of monitoring a fluid system is also disclosed.

Claims

1. An apparatus for monitoring a fluid system comprising:

a liquid chamber;

a seal for sealing a fluid within said liquid chamber;

a wash chamber adjacent said seal on the opposite side of said seal from said liquid chamber;

a reservoir for supplying a wash solution to said wash chamber;

a supply pump for supplying a unidirectional flow of wash solution from said reservoir to said wash chamber;

a return line for conveying a return flow from said wash chamber to said reservoir, said return flow including any leakage of said fluid from said liquid chamber into said wash chamber and the portion of said wash solution that returns to said reservoir; and

a detector for determining whether there is a differential between said unidirectional flow and said return flow.

2. The apparatus of claim 1 wherein said liquid chamber is a pump chamber of a high pressure liquid chromatography (HPLC) pump.

3. The apparatus of claim 2 wherein said HPLC pump includes a piston extending through said pump chamber, said seal, and said wash chamber.

4. The apparatus of claim 1 further comprising a plurality of liquid chambers and a plurality of wash chambers, each said liquid chamber including a seal, and each said wash chamber being adjacent a respective one of said seals.

5. The apparatus of claim 1 wherein said supply pump is a peristaltic pump.

6. The apparatus of claim 1 wherein said detector comprises a drop counter.

7. The apparatus of claim 6 wherein said detector comprises a pair of spaced electrodes extending into said reservoir, the ends of said electrodes positioned such that a drop of wash solution falling into said reservoir bridges a space between said ends as the drop passes said ends.

8. The apparatus of claim 7 further comprising a detection circuit, said electrodes operably coupled with said detection circuit for monitoring the number of drops of wash solution that pass between and bridge the space between said electrodes.

9. The apparatus of claim 8 wherein said detection circuit monitors a parameter of said supply pump.

10. The apparatus of claim 9 wherein said detection circuit provides a first signal indicating that said supply pump is running and said detector senses drops of return flow entering said reservoir.

11. The apparatus of claim 9 wherein said detection circuit provides a second signal indicating that said supply pump is running and said detector does not sense drops of return flow entering said reservoir.

12. The apparatus of claim 9 wherein said detection circuit provides a third signal indicating that said supply pump is not running and said detector senses drops of return flow entering to said reservoir.

13. The apparatus of claim 8 wherein said detection circuit provides a fourth signal indicating continuous conductivity between said electrodes.

14. The apparatus of claim 7 further comprising a cap releasably engaging said reservoir and a return passageway for fluid connection with said return line, said return passageway extending through said cap, wherein said pair of spaced electrodes extend through said cap and into said reservoir, the ends of said electrodes positioned below said return passageway such that a drop of wash solution falling from said return passageway into said reservoir bridges a space between said ends as the drop passes said ends.

15. A method of monitoring leakage in a system including a liquid chamber, a seal for sealing a fluid under within said liquid chamber, and a wash chamber adjacent said seal, said method comprising the steps of:

providing a unidirectional flow of a wash solution from a reservoir to said wash chamber;

determining whether there is a differential between a return flow and said unidirectional flow, said return flow including any leakage of said fluid from said liquid chamber into said wash chamber and the portion of said wash solution that returns to said reservoir.

16. The method of claim 15 further comprising the step of providing a first signal indicating said return flow is above a predetermined expected threshold.

17. The method of claim 15 further comprising the step of providing a second signal indicating that said unidirectional flow is greater than said return flow.

18. The method of claim 15 further comprising the step of providing a third signal indicating that said unidirectional flow is less than said return flow.

19. The method of claim 15 further comprising the step of providing a fourth signal indicating that the level of said reservoir exceeds a predetermined level.