High protein corn product production and use

• US 20030232109A1
• Filed: 06/17/2003
• Published: 12/18/2003
• Est. Priority Date: 12/04/2001
• Status: Active Grant

• Current Assignee: Greenstock Resources, Inc
• Original Assignee: Greenstock Resources, Inc
• Inventors: Dawley, Larry J., Dawley, James R.
• Granted Patent: US 6,962,722 B2
• Time in Patent Office: Days
• US Class Current: 426/53
• CPC Class Codes: A23K 10/38 from distillers' or brewers' waste
• CPC Class Codes: A23K 50/00 Feeding-stuffs specially adapted for particular animals
• CPC Class Codes: A23K 50/10 for ruminants
• CPC Class Codes: A23K 50/30 for swines
• CPC Class Codes: A23K 50/40 for carnivorous animals, e.g. cats or dogs
• CPC Class Codes: A23K 50/75 for poultry
• CPC Class Codes: A23K 50/80 for aquatic animals, e.g. fish, crustaceans or molluscs
• CPC Class Codes: C08B 30/10 Working-up residues from the starch extraction , e.g. potato peel or steeping water, including pressing water from the starch-extracted material
• CPC Class Codes: Y02A 40/818 Alternative feeds for fish, e.g. in aquacultures
• CPC Class Codes: Y02P 60/87 Re-use of by-products of food processing for fodder production

Abstract

The present invention relates to the production of a highly digestible, high protein product (high protein distillers dried grains or high protein DDG) from corn endosperm, and more particularly to a method for the recovery of high protein DDG by using: (i) dehulling and degermination to isolate a low fat, low fiber corn endosperm fraction, (ii) enzymatic hydrolysis to solubilize and alcoholic fermentation to assimilate the starch and non-starch carbohydrates present in the corn endosperm, and (iii) filtration and/or centrifugation to recover the dealcoholized insoluble solids that remain after fermentation of the corn endosperm. The present invention provides an alternative to the traditional dry mill method of processing corn to produce ethanol, and results in the production and recovery of a distillers'"'"' by-product (high protein DDG) with increased value and range of use as an ingredient in feeds for farm-raised ruminants and non-ruminants and pet foods. The product of the present invention contains less than about 2.0 weight percent starch, from about 55.0 to about 65.0 weight percent protein, from about 4.5 to about 7.5 weight percent fat, from about 3.0 to about 5.0 weight percent crude fiber, and from about 78.0 to about 90.0 percent total digestible nutrients, and improves the palatability and digestibility of animal feeds and/or pet foods into which it is incorporated, and aids in the management of the health and weight gain of the animal.

Claims

1. An animal feed composition that is comprised of from about 1.5 to about 20.0 weight percent of a high protein corn product (high protein distillers dried grains or high protein DDG), wherein said high protein DDG is produced as a result of recovering the insoluble solids that remain after the enzymatic hydrolysis and alcoholic fermentation of the starch and non-starch carbohydrates present in the endosperm fraction of dry-milled corn;

and wherein said high protein DDG has a;

(a) starch content less than about 2.0 weight percent, (b) protein content of from about 55.0 to about 65.0 weight percent, (c) fat content of from about 4.5 to about 7.5 weight percent, (d) crude fiber content of from about 3.0 to about 5.0 weight percent, and (e) a total digestible nutrient value of from about 78.0 to about 90.0 percent.

2. The animal feed composition as recited in claim 1, wherein said animal feed composition is comprised of from about 2.5 to about 20.0 weight percent of said high protein DDG.

3. The animal feed composition as recited in claim 1, wherein said animal feed composition is comprised of from about 2.5 to about 15.0 weight percent of said high protein DDG.

4. The animal feed composition as recited in claim 1, wherein said animal feed composition is comprised of from about 1.5 to about 10.0 weight percent of said high protein DDG

5. The animal feed composition as recited in claim 1, wherein said high protein DDG is comprised of from about 57.5 to about 65.0 weight percent of protein, from about 3.0 to about 4.5 weight percent crude fiber, from about 6.0 to about 7.5 weight percent fat, and wherein said high protein DDG has a total digestible nutrient value of from about 80 to about 87.5 percent.

6. The animal feed composition as recited in claim 1, wherein said high protein DDG is produced as a result of recovering the insoluble solids that remain after enzymatic hydrolysis and alcoholic fermentation of the starch and non-starch carbohydrates present in the endosperm fraction of dry-milled corn.

7. The animal feed composition as recited in claim 6, wherein said endosperm fraction used to produce said high protein DDG is derived from the dry-milling of a variety of corn selected from the group consisting of yellow dent, hard endosperm yellow, white, flint, high amylose, or waxy corn.

9. The animal feed composition as recited in claim 6, wherein said endosperm fraction used to produce said high protein DDG is derived from the dry-milling of a single variety or mixture of two or more varieties of yellow dent and/or hard endosperm yellow corn.

10. The animal feed composition as recited in claim 6, wherein said endosperm fraction used to produce said high protein DDG is derived from the dry-milling of a single variety or mixture of two or more varieties of flint and/or white corn.

11. The animal feed composition as recited in claim 1, wherein said high protein DDG is produced by a process comprising the steps of:

(a) tempering clean, conditioned corn in water to loosen the attachment of the fractions consisting of the endosperm from the germ from the pericarp (hull), (b) dehulling and degerminating or decorticating said tempered corn to separate said endosperm from the germ from the pericarp (hull), (c) recovering said endosperm from the germ from the pericarp (hull), keeping as a single distinct fraction the large, medium and fine grits, and the meal and flour generated during said degermination or decortication of corn, (d) liquefying, saccharifying, and/or solubilizing the starch and non-starch carbohydrates present in said endosperm fraction, (e) performing an alcoholic fermentation using the fermentable sugars generated by the liquefaction, saccharification, and/or solubilization of the starch and non-starch carbohydrates present in said endosperm fraction, (f) removing the alcohol produced from said alcoholic fermentation, (g) separating the solids that remain after said alcoholic fermentation and/or solubilization of starch and non-starch carbohydrates and said alcohol recovery into an insoluble solids and soluble solids fraction, (h) recovering said soluble solids fraction and drying said soluble solids fraction with the pericarp (hull) and/or germ generated during said dehulling and degermination or decortication of corn, and (i) recovering said insoluble solids fraction and drying said insoluble solids fraction to produce said high protein DDG.

12. The animal feed composition as recited in claim 11, wherein said step of tempering clean, conditioned corn, as part of the process to produce said high protein DDG, is done with water at ambient temperature to increase the moisture content of the corn from about 12.0 to about 15.0 weight percent to about 17.0 to about 20.0 weight percent.

13. The animal feed composition as recited in claim 11, wherein said step of tempering clean, conditioned corn, as part of the process to produce said high protein DDG, is done with water at ambient temperature for a period of from about 0.167 to about 2.0 hours.

14. The animal feed composition as recited in claim 11, wherein said step of dehulling and degermination or decortication of corn, as part of the process to produce said high protein DDG is done with machinery that through impaction, abrasion, and/or shearing separates said tempered corn into fractions comprising endosperm, germ and pericarp (hull).

15. The animal feed composition as recited in claim 11, wherein said step of recovering endosperm from the germ and from the pericarp (hull), as part of the process to produce said high protein DDG, comprises the use of sieves or screens, gravity tables, and/or aspirators, and wherein said recovered endosperm contains, as a single distinct fraction, all of the large, medium, and small grits, and the meal and flour generated during said dehulling and degerminating or decorticating of corn.

16. The animal feed composition as recited in claim 11, wherein said recovered endosperm, as part of the process to produce said high protein DDG, represents from about 65.0 to about 80.0 weight percent of said tempered corn.

17. The animal feed composition as recited in claim 11, wherein said recovered endosperm, as part of the process to produce said high protein DDG, has a fat content from about 0.60 to about 1.10 weight percent and a crude fiber content from about 0.40 to about 0.80 weight percent.

18. The animal feed composition as recited in claim 11, wherein said liquefaction, saccharification and/or solubilization of the starch and non-starch carbohydrates present in said endosperm, as part of the process to produce said high protein DDG, is done using an acid-acid, acid-enzyme, or enzyme-enzyme process.

19. The animal feed composition as recited in claim 11, wherein said liquefaction, saccharification and/or solubilization of the starch and non-starch carbohydrates present in said endosperm, as part of the process to produce said high protein DDG, is done using an enzyme-enzyme process using enzymes selected from the group consisting of amylases, glucoamylases, cellulases, hemicellulases, beta-glucanases, and mixtures thereof.

20. The animal feed composition as recited in claim 11, wherein said alcoholic fermentation of the fermentable sugars obtained from the liquefaction, saccharification and/or solubilization of the starch and non-starch carbohydrates present in said endosperm, as part of the process to produce said high protein DDG, is done using a single or mixed culture of either yeast or bacteria.

21. The animal feed composition as recited in claim 11, wherein the recovery of said insoluble solids that remain after said alcoholic fermentation and said alcohol recovery, as part of the process to produce said high protein DDG, is accomplished using sedimentation, filtration, centrifugation, or combinations thereof.

22. The animal feed composition as recited in claim 11, wherein said insoluble solids that remain after said alcoholic fermentation and said alcohol recovery, as part of the process to produce said high protein DDG, are dried in a dryer selected from the group consisting of a spray dryer, flash dryer, ring dryer, freeze dryer, vacuum dryer, rotary gas-fired dryer or rotary steam-tube dryer.