Assessing downhole WBM-contaminated connate water

• US 20040000400A1
• Filed: 12/13/2002
• Published: 01/01/2004
• Est. Priority Date: 11/28/2001
• Status: Active Grant

• Current Assignee: Schlumberger Technology Corporation (SLB)
• Original Assignee: Schlumberger Technology Corporation (SLB)
• Inventors: Mullins, Oliver C., Fujisawa, Go, Dong, Chengli, Kurkjian, Andrew
• Granted Patent: US 7,028,773 B2
• Time in Patent Office: Days
• US Class Current: 166/250.01
• CPC Class Codes: E21B 47/11 using tracers; using radioactivity
• CPC Class Codes: E21B 49/005 Testing the nature of borehole walls or the formation by using drilling mud or cutting data
• CPC Class Codes: E21B 49/08 Obtaining fluid samples or testing fluids, in boreholes or wells
• CPC Class Codes: E21B 49/0875 determining specific fluid parameters
• CPC Class Codes: G01N 21/645 Specially adapted constructive features of fluorimeters
• CPC Class Codes: G01N 33/241 for hydrocarbon content
• CPC Class Codes: G01N 33/2882 Markers

Abstract

Water-based mud filtrate concentration in a downhole fluid sample drawn from the borehole of an oil well is assessed. To measure water-based mud filtrate concentration, a water-based mud having a water-soluble fluorescent dye tracer is pumped into the borehole; sample fluid from a selected downhole location is pumped through a downhole flow line having a window; sample fluid flowing in an excitation region of the downhole flow line is illuminated through the window with fluorescence excitation light; and fluorescence emission from the excitation region is measured to produce a measured value. The measured value represents the fraction of water-based mud filtrate in the sample fluid. A calibration value is determined representing 100% water-based mud filtrate. A method for validating a sample of connate water as having an acceptably low WBM filtrate contamination tests for validation downhole, in real time. Each measured value of the series of measured values is compared with a predetermined fraction of a calibration value. Samples that are validated may be captured and brought to the surface for analysis. A method using the time series data and a predetermined fraction of the calibration value calculates a predicted flushing time to completion.

Claims

1. A method for assessing water-based mud filtrate concentration in a downhole fluid sample drawn from the borehole of an oil well, comprising:

a) pumping a water-based mud having a water-soluble fluorescent dye tracer into the borehole;

b) pumping sample fluid from a selected downhole location through a downhole flow line;

c) illuminating sample fluid in an excitation region of the downhole flow line with fluorescence excitation light; and

d) measuring fluorescence emission from the excitation region to produce a measured value representing the fraction of water-based mud filtrate in the sample fluid.

2. A method according to claim 1, further comprising:

e) establishing a calibration value representing 100% water-based mud filtrate.

3. A method according to claim 2, wherein the calibration value is established by pumping substantially 100% water-based mud filtrate through the downhole flow line and measuring fluorescence emission from the excitation region.

4. A method according to claim 2, wherein the calibration value is established by measuring fluorescence emission in a laboratory.

5. A method according to claim 2, further comprising:

f) repeating b), c), and d) to produce a series of measured values representing the fraction of water-based mud filtrate in each of a series of downhole fluid samples;

g) comparing each measured value of the series of measured values with a predetermined fraction of the calibration value; and

h) validating a downhole fluid sample as having an acceptably low fraction of water-based mud filtrate when the measured value of the sample is less than the predetermined fraction of the calibration value.

6. A method according to claim 2, further comprising:

i) repeating b), c), and d) at intervals of time to produce time series data including a series of times, and a corresponding series of measured values representing the fraction of water-based mud filtrate in each of a series of downhole fluid samples; and

j) using the time series data and a predetermined fraction of the calibration value to calculate a predicted flushing time to completion.

7. A method according to claim 6, further comprising:

k) comparing calculated flushing time to completion with a predetermined acceptable time to completion.

8. A tool for assessing water-based mud filtrate concentration in a downhole fluid sample drawn from the borehole of an oil well containing water-based mud with a water-soluble fluorescent dye tracer, comprising:

an elongated body containing a flow line having a window, the flow line containing an excitation region proximate to the window;

a pump configured to pump sample fluid from a selected downhole location through the flow line;

means for illuminating sample fluid in the excitation region with fluorescence excitation light; and

means for measuring fluorescence emission from the excitation region and producing a measured value representing the fraction of water-based mud filtrate in the sample fluid.

9. A tool according to claim 8, further comprising:

means for establishing a calibration value representing 100% water-based mud filtrate.

10. A tool according to claim 8, further comprising:

means for producing a series of measured values representing the fraction of water-based mud filtrate in each of a series of downhole fluid samples;

means for comparing each measured value of the series of measured values with a predetermined fraction of a calibration value; and

means for validating a downhole fluid sample as having an acceptably low fraction of water-based mud filtrate when the measured value of the sample is less than the predetermined fraction of the calibration value.

11. A tool according to claim 8, further comprising:

means for producing a series of measured values at intervals of time to produce time series data including a series of times, and a corresponding series of measured values representing the fraction of water-based mud filtrate in each of a series of downhole fluid samples; and

means for using the time series data and a predetermined fraction of a calibration value to calculate a predicted flushing time to completion.