Process analysis systems with automatic liquid sample preparation and connection to process control systems

• US 20040158433A1
• Filed: 01/12/2004
• Published: 08/12/2004
• Est. Priority Date: 01/16/2003
• Status: Abandoned Application

• Current Assignee: Bayer AG
• Original Assignee: Bayer AG
• Inventors: Schmitz, Bernd, Lahme, Michael, Gerlach, Martin, Wimschneider, Andrea, Sommer, Karsten, Frisch, Burkhard
• Application Number:
  US10/755,754
• Publication Number:
  US 20040158433A1
• Time in Patent Office: Days
• US Class Current: 702/183
• CPC Class Codes: G01N 2030/8804 automated systems
• CPC Class Codes: G01N 2030/8886 Analysis of industrial production processes
• CPC Class Codes: G01N 2035/00326 Analysers with modular structure
• CPC Class Codes: G01N 2035/0091 GUI [graphical user interfaces]
• CPC Class Codes: G01N 30/20 using a sampling valve
• CPC Class Codes: G01N 30/8651 Recording, data aquisition, archiving and storage
• CPC Class Codes: G01N 30/88 Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
• CPC Class Codes: G01N 35/00584 Control arrangements for automatic analysers
• CPC Class Codes: G01N 35/00871 Communications between instruments or with remote terminals
• CPC Class Codes: G05D 21/02 characterised by the use of electric means

Abstract

An analysis system for a process, having:

means (100; 300) for taking a sample from the process,

sample preparation means (108; 302, 304, 306, 307, 308, 310, 312, 314, 316, 317, 318),

means (112) for analyzing the sample,

means (106, 116) for transmitting an analysis result (114) to a process control system (118, 120).

Claims

1. Analysis system for a process, having:

a sampling unit,

a sample preparation system,

an analyzer, and

a control unit

wherein said sampling unit is adapted to take a sample from a sample source and provide said sample to said sample preparation system, said sample preparation system is adapted to prepare said sample for analysis and provide the so prepared sample to said analyzer, and said analyzer is adapted to analyze said prepared sample and communicate the results of said analysis to said control unit, and said control unit is adapted to provide a signal to a process control unit in accordance with the results of said analysis.

2. Analysis system according to claim 1, wherein said sampling unit is a controllable bypass for taking a liquid sample.

3. Analysis system according to claim 1 or 2, wherein said sample preparation system is a modular system comprising a plurality of modules.

4. Analysis system according to claim 3, wherein said control unit is adapted to communicate with said sample preparation system and comprises a control program and driver programs for the modules of the sample preparationsystem.

5. Analysis system according to claim 4, wherein said control program comprises a program procedure which is determinable in accordance with data imported from a computer.

6. Analysis system according to claim 5, wherein said computer comprises a representation for each module of the sample preparationsystem, and a user interface through which representations of the modules and the actions to be carried out by the selected modules are selectable to assemble an analysis sequence, and the computer is adapted to export data defining said analysis sequence to the control program.

7. Analysis system according to claim 1, wherein said analyzer comprises a chromatograph or a combination of a chromatograph and a mass-spectrometry detector (GC-MS or HPLC-MS).

8. Analysis system according to claim 1, wherein said control unit comprises a bus interface and said analyzer communicates with said process control system through said interface with a bus system of the process control system.

9. Method for controlling a process, comprising the steps of:

taking a sample from the process by operation of a sampling unit, which is coupled to an automatic sample preparation system,

delivering the sample to the automatic sample preparation system,

carrying out an automatic sample preparation under the the control of a control program,

delivering the so prepared sample to an analysis unit, and analyzing said sample to produce an analysis result, and

transmitting said analysis result to a process control system which adjusts said process in accordance with said analysis result.

10. Method according to claim 9, wherein the automatic sample preparation system is modularly constructed, comprises a plurality of modules, said modules comprising driver software, and the control program is adapted to access the driver software of the modules in accordance with parameters which are predeterminable by a user.

11. Method according to claim 10, comprising transmitting parameters from a computer to a control unit of the automatic sample preparation system for parameterization of the control program before the start of the control program.

12. Method according to claim 11, comprising selecting modules and actions to be carried out by the modules by a user via a user interface of the computer in for transmission to the control unit.

13. Digital storage media having stored thereon a computer program product for a control unit of an analysis system for a process, for carrying out the following steps:

operation of a sampling unit for taking a sample from the process,

operation of a sample preparation system for automatically carrying out a sample preparation of the sample which has been taken,

operation of an analyzer for analysis of the prepared sample,

outputting an analysis result onto a bus system of a process control system, for adjustment of the process by the process control system in accordance with the analysis result.

14. Digital storage media according to claim 13, wherein the computer program accesses modules of the sample preparation system for the automatic sample preparation through driver program modules.

15. Digital storage media according to claim 14, on which the program procedure for the carrying out the automatic sample preparation is established by data imported from a computer.