Methods and systems for producing ethanol using raw starch and fractionation

• US 20050233030A1
• Filed: 03/10/2005
• Published: 10/20/2005
• Est. Priority Date: 03/10/2004
• Status: Abandoned Application

• Current Assignee: Broin & Associates, Inc.
• Original Assignee: Broin & Associates, Inc.
• Inventors: Van Hulzen, Shon Erron, Lewis, Steven M.
• Application Number:
  US11/077,969
• Publication Number:
  US 20050233030A1
• Time in Patent Office: Days
• US Class Current: 426/49
• CPC Class Codes: C12C 12/00 Processes specially adapted for making special kinds of beer
• CPC Class Codes: C12C 12/006 Yeasts processes for seeding C12C11/02
• CPC Class Codes: C12P 19/14 produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase , e.g. by cellulase, hemicellulase
• CPC Class Codes: C12P 7/06 Ethanol, i.e. non-beverage
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel

Abstract

The present invention relates to methods for producing high levels of alcohol during fermentation of plant material, and to the high alcohol beer produced. The method can include fractionating the plant material. The present invention also relates to methods for producing high protein distiller'"'"'s dried grain from fermentation of plant material, and to the high protein distiller'"'"'s dried grain produced. The method can include drying a co-product by ring drying, flash drying, or fluid bed drying. The present invention further relates to reduced stack emissions from drying distillation products from the production of ethanol.

Claims

1. A process for producing ethanol from plant material, comprising:

fractionating the plant material;

reducing the plant material to produce material comprising starch;

the reduced plant material having particle size such that at least about 50% of the particles fit through a sieve with a 0.1-0.5 mm mesh;

saccharifying the starch, without cooking, with an enzyme composition;

fermenting the incubated starch to yield a composition comprising at least 15 vol-% ethanol;

fermenting comprising reducing temperature of fermenting mixture; and

recovering the ethanol and co-products from the fermentation.

2. The process of claim 1, wherein plant material comprises corn, which comprises high amylopectin starch.

3. The process of claim 1, wherein the plant material comprises corn, sorghum, millet, wheat, barley, rye, or mixtures thereof.

4. The process of claim 3, wherein the corn comprises waxy corn.

5. The process of claim 3, wherein the corn comprises high protein corn.

6. The process of claim 3, wherein the corn comprises #2 yellow dent corn.

7. The process of claim 1, comprising reducing the plant material with hammer mill, roller mill, or both hammer mill and roller mill.

8. The process of claim 7, comprising reducing the plant material to produce plant material of a size that at least 35% of the reduced plant material fits through a 0.1-0.5 mm screen.

9. The process of claim 1, comprising reducing the plant material with particle size reduction emulsion technology.

10. The process of claim 1, comprising simultaneous saccharifying and fermenting.

11. The process of claim 1, comprising decreasing temperature during saccharifying, fermenting, or simultaneous saccharifying and fermenting.

12. The process of claim 1, comprising saccharifying, fermenting, or simultaneous saccharifying and fermenting at temperature of 25-40°

C.

13. The process of claim 1, comprising saccharifying, fermenting, or simultaneous saccharifying and fermenting at temperature of 27-35°

C.

14. The process of claim 1, comprising reducing temperature from about 40°

C. and to about 25°

C. during saccharifying, fermenting, or simultaneous saccharifying and fermenting.

15. The process of claim 1, comprising saccharifying, fermenting, or simultaneous saccharifying and fermenting at pH of about 3.0 to about 6.0.

16. The process of claim 1, comprising saccharifying, fermenting, or simultaneous saccharifying and fermenting at pH of about 4.1 to about 5.3.

17. The process of claim 1, comprising a pH of about 4 to about 4.5 at start of fermentation fill.

18. The process of claim 1, comprising a pH of about 5 to about 5.5 as ethanol production reaches maximum level.

19. The process of claim 1, comprising increasing pH from about 4 to about 5.3 during saccharifying, fermenting, or simultaneous saccharifying and fermenting.

20. The process of claim 1, comprising decreasing solid content from about 40% to about 15% during saccharifying, fermenting, or simultaneous saccharifying and fermenting.

21. The process of claim 1, wherein the enzyme composition comprises alpha amylase, glucoamylase, protease, or mixtures thereof.

22. The process of claim 1, wherein saccharifying, fermenting, or simultaneous saccharifying and fermenting comprises adding protease.

23. The process of claim 1, wherein saccharifying, fermenting, or simultaneous saccharifying and fermenting comprises adding backset.

24. The process of claim 1, wherein saccharifying, fermenting, or simultaneous saccharifying and fermenting comprising adding nitrogen.

25. The process of claim 1, comprising saccharifying and fermenting at rates that maintain concentration of glucose less than 3 wt-% in fermentation.

26. The process of claim 1, comprising saccharifying, fermenting, or both saccharifying and fermenting with about 0.1 to about 10 acid fungal amylase units (AFAU) per gram of dry solids reduced plant material and about 0.1 to about 6 glucoamylase units (AGU) per gram dry solids reduced plant material.

27. The process of claim 1, comprising starting saccharifying, fermenting, or both saccharifying and fermenting with about 25 to about 45 wt-% reduced plant material in water.

28. The process of claim 1, comprising starting saccharifying, fermenting, or both saccharifying and fermenting with residual starch at up to 20%.

29. The process of claim 1, comprising producing greater than 18 vol-% ethanol in about 48 to 96 hours.

30. The process of claim 1, comprising producing 18 vol-% to about 23 vol-% ethanol.

31. The process of claim 1, further comprising recovering the solids from the fermentation.

32. The process of claim 31, recovering before, during, and after recovering the ethanol.

33. The process of claim 31, comprising recovering distiller'"'"'s dried grain.

34. The process of claim 31, wherein the distiller'"'"'s dried grain comprises about 30-38 wt-% protein, about 11-19 wt-% fat, about 25-37 wt-% fiber.

35. The process of claim 31, wherein the distiller'"'"'s dried grain comprises at least about 30% protein.

36. The process of claim 1, comprising running the process as a batch process or as a continuous process.

37. A process for producing ethanol from plant material, comprising:

fractionating the plant material;

reducing the plant material to produce material comprising starch;

saccharifying the starch, without cooking, with an enzyme composition comprising acid fungal amylase;

fermenting the incubated starch to yield a composition comprising at least about 18 vol-% ethanol;

recovering ethanol from the fermentation.

38. A distiller'"'"'s dried gain comprising at least about 40 wt-% protein.

39. A process for producing ethanol from plant material, comprising:

reducing the plant material to produce material comprising starch;

the reduced plant material having particle size such that at least about 50% of the particles fit through a sieve with a 0.1-0.5 mm mesh;

saccharifying the starch, without cooking, with an enzyme composition;

fermenting the incubated starch to yield a composition comprising at least 15 vol-% ethanol;

fermenting comprising reducing temperature of fermenting mixture; and

recovering the ethanol and co-products from the fermentation;

drying a co-product by ring drying, flash drying, or fluid bed drying.