Continuous manufacture of high internal phase ratio emulsions using relatively low-shear and low-temperature processing steps
First Claim
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1. A continuous method for preparing a high internal phase silicone in water emulsion which comprises:
- a) providing an amount of a continuous phase in a system;
b) adding an amount of a dispersed phase to the system;
c) providing low shear means to mix the continuous phase and dispersed phase thus forming an intermediate emulsion;
d) incrementally adding additional amounts of the dispersed phase to the intermediate emulsion while shearing;
e) maintaining the amounts of continuous phase and dispersed phase in the system by continuously adding additional amounts of each to the system; and
, f) removing a high internal phase silicone in water emulsion from the system as it is formed.
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Abstract
Methods for continuously producing HIPR silicone in water emulsions are disclosed. The methods use low shear devices, and thus the temperature of the emulsions is kept low, while enhanced particle size and viscosity are obtained.
23 Citations
58 Claims
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1. A continuous method for preparing a high internal phase silicone in water emulsion which comprises:
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a) providing an amount of a continuous phase in a system;
b) adding an amount of a dispersed phase to the system;
c) providing low shear means to mix the continuous phase and dispersed phase thus forming an intermediate emulsion;
d) incrementally adding additional amounts of the dispersed phase to the intermediate emulsion while shearing;
e) maintaining the amounts of continuous phase and dispersed phase in the system by continuously adding additional amounts of each to the system; and
,f) removing a high internal phase silicone in water emulsion from the system as it is formed. - View Dependent Claims (2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17, 18, 19, 20, 21, 22, 23, 24, 25, 26, 27, 28, 29, 30, 31, 32, 33, 34, 35, 36, 37, 38, 39, 40, 41, 42, 43, 44, 45, 46, 47, 48, 49, 50, 51, 52, 53, 54, 55, 56, 57, 58)
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Specification