Controlled preparation of nanoparticle materials
First Claim
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1. A method of producing nanoparticles comprising:
- effecting conversion of a nanoparticle precursor composition to a material of the nanoparticles, the precursor composition comprising a first precursor species containing a first ion to be incorporated into the nanoparticles and a second precursor species containing a second ion to be incorporated into the nanoparticles, the conversion being effected in the presence of a molecular cluster compound under conditions permitting seeding and growth of the nanoparticles, by dispersing the molecular cluster compound and an initial portion of the nanoparticle precursor composition which is less than the total amount of the nanoparticle precursor composition to be used to produce the nanoparticles in a suitable dispersing medium at a first temperature;
increasing a temperature of the dispersing medium containing the cluster compound and precursor composition to a second temperature sufficient to initiate seeding and growth of the nanoparticles on the molecular clusters of the molecular cluster compound; and
adding at least one further portion of the nanoparticle precursor composition to the dispersing medium containing the nanoparticles, wherein the temperature of the dispersing medium containing the nanoparticles is increased at least before, during, or after the addition of the at least one further portion of the nanoparticle precursor composition.
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Abstract
A method of producing nanoparticles comprising effecting conversion of a nanoparticle precursor composition to the material of the nanoparticles, the precursor composition comprising a first precursor species containing a first ion to be incorporated into the growing nanoparticles and a second precursor species containing a second ion to be incorporated into the growing nanoparticles, said conversion being effected in the presence of a molecular cluster compound under conditions permitting seeding and growth of the nanoparticles.
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Citations
58 Claims
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1. A method of producing nanoparticles comprising:
effecting conversion of a nanoparticle precursor composition to a material of the nanoparticles, the precursor composition comprising a first precursor species containing a first ion to be incorporated into the nanoparticles and a second precursor species containing a second ion to be incorporated into the nanoparticles, the conversion being effected in the presence of a molecular cluster compound under conditions permitting seeding and growth of the nanoparticles, by dispersing the molecular cluster compound and an initial portion of the nanoparticle precursor composition which is less than the total amount of the nanoparticle precursor composition to be used to produce the nanoparticles in a suitable dispersing medium at a first temperature;
increasing a temperature of the dispersing medium containing the cluster compound and precursor composition to a second temperature sufficient to initiate seeding and growth of the nanoparticles on the molecular clusters of the molecular cluster compound; and
adding at least one further portion of the nanoparticle precursor composition to the dispersing medium containing the nanoparticles, wherein the temperature of the dispersing medium containing the nanoparticles is increased at least before, during, or after the addition of the at least one further portion of the nanoparticle precursor composition. - View Dependent Claims (2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17, 18, 19, 20, 21, 22, 23, 24, 25, 26, 27, 28, 29, 30, 31, 32, 33, 34, 35, 36, 37, 38, 39, 40, 41, 42, 43, 44, 45, 46, 47)
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48. A method of producing nanoparticles comprising:
effecting conversion of a nanoparticle precursor composition to a material of the nanoparticles, said precursor composition comprising a first precursor species containing a first ion to be incorporated into the nanoparticles and a separate second precursor species containing a second ion to be incorporated into the nanoparticles, said conversion being effected in the presence of a molecular cluster compound under conditions permitting seeding and growth of the nanoparticles, wherein the method comprises;
dispersing the molecular cluster compound and an initial portion of one of the first and second precursor species which is less than the total amount of said one of the first and second precursor species to be used to produce said nanoparticles in a suitable dispersing medium at a first temperature;
increasing the temperature of the dispersing medium containing the cluster compound and said one of the first and second precursor species to a second temperature which is sufficient to initiate seeding and growth of the nanoparticles on the molecular clusters of said molecular cluster compound; and
adding at least one further portion of said one of the first and second precursor species to the dispersing medium containing the nanoparticles, wherein the temperature of the dispersing medium containing the nanoparticles is increased at least before, during, or after the addition of the at least one portion of said one of the first and second precursor species. - View Dependent Claims (49, 50, 51, 52, 53, 54, 55, 56, 57, 58)
Specification