Method of characterizing a dispersion using transformation techniques

• US 20070134804A1
• Filed: 10/12/2004
• Published: 06/14/2007
• Est. Priority Date: 10/17/2003
• Status: Abandoned Application

• Current Assignee: Alberta Research Council Inc. (Alberta Science & Research Authority)
• Original Assignee: Alberta Research Council Inc. (Alberta Science & Research Authority)
• Inventors: Huang, Haibo, Girard, Marcel, Fisher, Douglas
• Application Number:
  US10/574,767
• Publication Number:
  US 20070134804A1
• Time in Patent Office: Days
• US Class Current: 436/164
• CPC Class Codes: G01N 21/59 Transmissivity G01N21/25 takes precedence
• CPC Class Codes: G01N 33/2847 Water in oils

Abstract

A method for analyzing a dispersion such as an oil/solid suspension or an oil/water emulsion. A set of original domain data is collected relating to an attribute of the dispersion, such as light transmittance therethrough. The set of original domain data is then transformed into a transformed set of original domain data which is in the frequency domain. Any transformation technique, such as a fast Fourier transform, may be used to transform the original domain data from a first domain, such as a time or spatial domain, into the frequency domain. The dispersion is then characterized using the transformed set of original domain data. One or more frequency domain spectra may be generated from the transformed set of original domain data, which frequency domain spectra express a parameter relating to the attribute of the dispersion as a function of frequency, in which case the characterizing step may be performed using the frequency domain spectra.

Claims

1. A method for analyzing a dispersion comprising the following steps:

(a) collecting a set of original domain data relating to an attribute of the dispersion;

(b) transforming the set of original domain data into a transformed set of original domain data, wherein the transformed set of original domain data is in the frequency domain; and

(c) characterizing the dispersion using the transformed set of original domain data.

2. The method as claimed in claim 1, further comprising the step of generating a frequency domain spectrum from the transformed set of original domain data, wherein the frequency domain spectrum expresses a parameter relating to the attribute of the dispersion as a function of frequency and wherein the characterizing step is performed using the frequency domain spectrum.

3. The method as claimed in claim 2 wherein the attribute of the dispersion is pressure of the dispersion.

4. The method as claimed in claim 2 wherein the attribute of the dispersion is transmittance of electromagnetic radiation through the dispersion.

5. The method as claimed in claim 4 wherein the set of original domain data is comprised of a transmittance signal representing transmittance of electromagnetic radiation through the dispersion over a period of time.

6. The method as claimed in claim 5, further comprising the step of manipulating the dispersion during the period of time in order to cause variations in the transmittance signal over the period of time.

7. The method as claimed in claim 6 wherein the collecting step is performed using a data collection apparatus comprising a transmittance sensor and wherein the manipulating step is comprised of moving the dispersion and the transmittance sensor relative to each other.

8. The method as claimed in claim 7 wherein the manipulating step is comprised of moving the dispersion through a conduit past the transmittance sensor.

9. The method as claimed in claim 8 wherein the data collection apparatus is further comprised of a source of electromagnetic radiation and wherein the manipulating step is comprised of moving the dispersion through the conduit between the source of electromagnetic radiation and the transmittance sensor.

10. The method as claimed in claim 2 wherein the transforming step is comprised of transforming the set of original domain data in one dimension.

11. The method as claimed in claim 10, further comprising the step of conditioning the set of original domain data before the transforming step in order to reduce at least one unwanted component in the set of original domain data.

12. The method as claimed in claim 11 wherein the conditioning step is comprised of calculating a derivative of the set of original domain data in one dimension.

13. The method as claimed in claim 2 wherein the transforming step is comprised of transforming the set of original domain data in two dimensions.

14. The method as claimed in claim 13, further comprising the step of conditioning the set of original domain data before the transforming step in order to reduce at least one unwanted component in the set of original domain data.

15. The method as claimed in claim 14 wherein the conditioning step is comprised of calculating a derivative of the set of original domain data in two dimensions.

16. The method as claimed in claim 2 wherein the collecting step is comprised of collecting a plurality of subsets of original domain data so that the set of original domain data is comprised of the subsets of original domain data, wherein the subsets of original domain data are transformed into a plurality of subsets of transformed original domain data, and wherein the characterizing step is performed using the subsets of transformed original domain data.

17. The method as claimed in claim 16 wherein the frequency domain spectrum generating step is comprised of generating a frequency domain spectrum from each of the subsets of transformed original domain data in order to produce a plurality of frequency domain spectra and wherein the characterizing step is performed using the frequency domain spectra.

18. The method as claimed in claim 17 wherein the collecting step is comprised of collecting each of the subsets of original domain data at a different value of a dispersion characterizing variable so that the dispersion may be characterized with respect to the dispersion characterizing variable.

19. The method as claimed in claim 18 wherein the dispersion is comprised of oil and wherein the dispersion characterizing variable is an amount of solvent mixed with the oil.

20. The method as claimed in claim 18 wherein the dispersion is comprised of an emulsion comprising oil and water and wherein the dispersion characterizing variable is time.

21. The method as claimed in claim 18 wherein the dispersion is comprised of an emulsion comprising oil and water and wherein the dispersion characterizing variable is a ratio of the relative amounts of oil and water contained in the emulsion.

22. The method as claimed in claim 18 wherein the characterizing step is comprised of the step of generating from the frequency domain spectra an expression of the parameter relating to the attribute of the dispersion as a function of both frequency and the dispersion characterizing variable in order to characterize the dispersion with respect to the dispersion characterizing variable.

23. The method as claimed in claim 22 wherein the transforming step is comprised of transforming the set of original domain data in one dimension.

24. The method as claimed in claim 23, further comprising the step of conditioning the set of original domain data before the transforming step in order to reduce at least one unwanted component in the set of original domain data.

25. The method as claimed in claim 24 wherein the conditioning step is comprised of calculating a derivative of the set of original domain data in one dimension.

26. The method as claimed in claim 18 wherein the characterizing step is comprised of the step of integrating each of the frequency domain spectra between an upper selected frequency and a lower selected frequency, thereby obtaining a characterization number for each of the frequency domain spectra.

27. The method as claimed in claim 26 wherein the characterizing step is further comprised of the step of generating from the characterization numbers an expression of characterization number as a function of the dispersion characterizing variable in order to characterize the dispersion with respect to the dispersion characterizing variable.

28. The method as claimed in claim 27 wherein the characterizing step is further comprised of calculating a derivative of the expression of characterization number as a function of the dispersion characterizing variable in order to characterize the dispersion with respect to the dispersion characterizing variable.

29. The method as claimed in claim 27 wherein the transforming step is comprised of transforming the set of original domain data in one dimension.

30. The method as claimed in claim 29, further comprising the step of conditioning the set of original domain data before the transforming step in order to reduce at least one unwanted component in the set of original domain data.

31. The method as claimed in claim 30 wherein the conditioning step is comprised of calculating a derivative of the set of original domain data in one dimension.

32. The method as claimed in claim 27 wherein the transforming step is comprised of transforming the set of original domain data in two dimensions.

33. The method as claimed in claim 32, further comprising the step of conditioning the set of original domain data before the transforming step in order to reduce at least one unwanted component in the set of original domain data.

34. The method as claimed in claim 33 wherein the conditioning step is comprised of calculating a derivative of the set of original domain data in two dimensions.

35. The method as claimed in claim 4 wherein the set of original domain data is comprised of a transmittance image representing distribution of transmittance of electromagnetic radiation through the dispersion over a spatial area.

36. The method as claimed in claim 35 wherein the transforming step is comprised of transforming the set of original domain data in one dimension along a sample line.

37. The method as claimed in claim 36, further comprising the step of conditioning the set of original domain data before the transforming step in order to reduce at least one unwanted component in the set of original domain data.

38. The method as claimed in claim 37 wherein the conditioning step is comprised of calculating a derivative of the set of original domain data in one dimension.

39. The method as claimed in claim 35 wherein the transforming step is comprised of transforming the set of original domain data in one dimension along a plurality of sample lines.

40. The method as claimed in claim 39, further comprising the step of conditioning the set of original domain data before the transforming step in order to reduce at least one unwanted component in the set of original domain data.

41. The method as claimed in claim 40 wherein the conditioning step is comprised of calculating a derivative of the set of original domain data in one dimension.

42. The method as claimed in claim 41 wherein the step of generating the frequency domain spectrum from the transformed set of original domain data is comprised of determining from the plurality of sample lines an average value for the parameter relating to the attribute of the dispersion as a function of frequency.

43. The method as claimed in claim 35 wherein the transforming step is comprised of transforming the set of original domain data in two dimensions.

44. The method as claimed in claim 43, further comprising the step of conditioning the set of original domain data before the transforming step in order to reduce at least one unwanted component in the set of original domain data.

45. The method as claimed in claim 44 wherein the conditioning step is comprised of calculating a derivative of the set of original domain data in two dimensions.