ALCOHOL PRODUCTION USING SONICATION

• US 20080096261A1
• Filed: 10/18/2007
• Published: 04/24/2008
• Est. Priority Date: 08/29/2003
• Status: Active Grant

• Current Assignee: FCStone Carbon LLC (StoneX Group, Inc.)
• Original Assignee: FCStone Carbon LLC (StoneX Group, Inc.)
• Inventors: Snodgrass, Jonathan, Krohn, Bradley, Kinley, Michael
• Granted Patent: US 7,514,246 B2
• Time in Patent Office: Days
• US Class Current: 435/165
• CPC Class Codes: C12M 21/12 for producing fuels or solvents C12M21/04 takes precedence; liquid carbonaceous fuels C10L1/00, solid fuels C10L5/00
• CPC Class Codes: C12M 35/04 Mechanical means, e.g. sonic waves, stretching forces, pressure or shear stimuli
• CPC Class Codes: C12N 1/066 by physical methods
• CPC Class Codes: C12N 13/00 Treatment of microorganisms or enzymes with electrical or wave energy, e.g. magnetism, sonic waves
• CPC Class Codes: C12P 7/06 Ethanol, i.e. non-beverage
• CPC Class Codes: C12P 7/16 Butanols
• CPC Class Codes: C12P 7/18 polyhydric
• CPC Class Codes: C12P 7/24 containing a carbonyl group
• CPC Class Codes: C12P 7/56 Lactic acid
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel

Abstract

A system comprising one or more transducers and an alcohol production facility having a liquid medium processing stream, the alcohol production facility adapted for use with the one or more transducers is provided. In one embodiment, the one or more transducers apply sonication to the liquid medium processing stream in one or more locations. In one embodiment, the alcohol production facility is an ethanol production facility. In one embodiment, the ethanol production facility utilizes a dry grind process, modified dry grind process or wet mill process. The systems of the present invention utilize sonication at the frequencies and intensities required on an industrial scale to reduce the production cost of alcohol, such as ethanol, by improving alcohol yield per bushel, reducing processing times for higher throughput, reducing operating costs, and increasing the marketability of co-products, among other benefits.

Claims

1. A method for increasing fermentable starch levels in a grain-based liquid medium processing stream comprising applying sonication in one or more locations to the liquid medium processing stream, causing starch granules present in the liquid medium processing stream to become destructured, wherein availability of the starch granules for hydrolysis is increased.

6. The method of claim 1 wherein grain in the grain-based liquid medium processing stream is selected from corn, rye, sorghum, wheat, barley, oats, rice and combinations thereof.

7. The method of claim 1 wherein protein present in the liquid medium processing stream is not degraded.

8. The method of claim 7 wherein sonication is applied with a transducer generating less than three (3) kW of power down to one (1) kW of power.

9. The method of claim 1 wherein sonication is applied with a high-powered transducer generating more than three (3) kW of power.

10. The method of claim 1 wherein the liquid medium processing stream produces starch-based products selected from animal feed, alcohol, high fructose corn syrup, food starch, industrial starch and organic acid.

11. The method of claim 10 wherein the alcohol is methanol, ethanol, isoproponal, butanol, or propane diol and the organic acid is lactic acid.

12. The method of claim 1 wherein the liquid medium processing stream is in an alcohol production process wherein enzymes are added to the liquid processing stream and the availability of the starch granules to the enzymes is increased during liquefaction and saccharification of the liquid medium processing stream.

13. The method of claim 12 wherein the alcohol production process is a dry grind ethanol production process which produces whole stillage and distiller'"'"'s dry grain solids.

14. The method of claim 13 wherein the whole stillage contains insoluble solids and sonication is applied to the whole stillage with a high-powered transducer, wherein complex proteins present in the insoluble solids are broken down.

15. The method of claim 1 wherein the starch granules are at least partially gelatinized.

16. The method of claim 15 wherein protein content in the distiller'"'"'s dry grain solids is increased.

17. The method of claim 16 wherein the distiller'"'"'s dry grain solids comprises animal feed containing proteins bio-available to an animal'"'"'s digestive system.

18. The method of claim 17 wherein the animal feed is pet food.

19. The method of claim 13 wherein sonication is applied to uncooked slurry in the liquid medium processing stream.

20. The method of claim 13 wherein sonication is applied during a cooking step or to cooked mash.

21. The method of claim 12 wherein sonication is applied to liquid mash exiting a liquefaction step.

22. The method of claim 12 wherein the alcohol production process is a modified dry grind ethanol production process.

23. The method of claim 22 wherein the modified dry process includes a soaking, further wherein the sonication is applied to the liquid medium processing stream at least after the soaking.

24. The method of claim 23 wherein the application of the sonication is followed by a degerm step, a defiber step or a fine grind step.

25. The method of claim 23 wherein the modified dry process includes a degerm step, further wherein the sonication is applied to the liquid medium processing stream at least after the degerm step.

26. The method of claim 25 wherein the sonication is followed by a defiber step or a fine grind step.

2-5. -5. (canceled)

27. A method for increasing extracted starch levels in a grain-based liquid medium processing stream comprising applying sonication in one or more locations to the liquid medium processing stream causing starch granules present in the liquid medium processing stream to become destructured, wherein availability of the starch granules for hydrolysis is increased.

28. The method of claim 27 wherein the liquid medium processing stream is in a wet milling alcohol production facility and the hydrolysis is acid hydrolysis.

29. The method of claim 28 wherein the wet milling alcohol production facility is a wet milling ethanol production facility.