DEVICES AND METHODS FOR SELECTIVE REMOVAL OF CONTAMINANTS FROM A COMPOSITION
First Claim
1. A method for removing organic acids from a crude product mixture comprising:
- contacting the crude product mixture with a metal oxide substrate, wherein free organic acids in the crude product mixture bind to the metal oxide substrate, thereby removing free organic acids and forming a refined product mixture; and
separating the refined product mixture from the metal oxide substrate.
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Abstract
The present invention relates to devices and methods for selectively removing contaminants from a crude product mixture. In an embodiment, the invention includes a method for removing free organic acids from a crude product mixture including contacting the crude product mixture with a metal oxide substrate, the metal oxide substrate having properties sufficient to bond with free organic acids in the crude product mixture, thereby removing free organic acids and forming a refined product mixture, and separating the refined product mixture from the metal oxide substrate. In an embodiment, the invention includes a device for removal of free organic acids from a crude product mixture including a first housing defining an interior volume, an input port, and an output port, and metal oxide media disposed within the first housing, the metal oxide media comprising a metal oxide selected from the group consisting of zirconia, alumina, hafnia, and titania. Other embodiments are also described herein.
119 Citations
20 Claims
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1. A method for removing organic acids from a crude product mixture comprising:
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contacting the crude product mixture with a metal oxide substrate, wherein free organic acids in the crude product mixture bind to the metal oxide substrate, thereby removing free organic acids and forming a refined product mixture; and separating the refined product mixture from the metal oxide substrate. - View Dependent Claims (2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16)
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17. A device for removal of free organic acids from a crude product mixture comprising:
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a first housing defining an interior volume, an input port, and an output port; metal oxide media disposed within the first housing, the metal oxide media comprising a metal oxide selected from the group consisting of zirconia, alumina, hafnia, and titania; and a temperature control unit configured to maintain the temperature within the first housing within a first temperature range for a first period of time and within a second temperature range for a second period of time following the first period, the second range higher than the first range. - View Dependent Claims (18, 19)
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20. A system for producing a refined oil product comprising:
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a production reactor for producing a crude oil product mixture, the reactor comprising a lipid reservoir, and an alcohol reservoir; and an organic acid removal reactor in fluid communication with the production reactor, the organic acid removal reactor comprising a housing defining an interior volume, the housing configured to receive the crude oil product mixture from the production reactor, metal oxide media disposed within the interior volume of the removal reactor housing, the metal oxide media comprising a metal oxide selected from the group consisting of zirconia, alumina, hafnia, and titania.
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Specification