Method of making graphene sheets and applicatios thereor

• US 20100126660A1
• Filed: 10/30/2009
• Published: 05/27/2010
• Est. Priority Date: 10/30/2008
• Status: Abandoned Application

• Current Assignee: David O'Hara
• Original Assignee: David O'Hara
• Inventors: O'Hara, David
• Application Number:
  US12/589,897
• Publication Number:
  US 20100126660A1
• Time in Patent Office: Days
• US Class Current: 156/249
• CPC Class Codes: B32B 37/12 characterised by using adhesives
• CPC Class Codes: B82Y 30/00 Nanotechnology for materials or surface science, e.g. nanocomposites
• CPC Class Codes: B82Y 40/00 Manufacture or treatment of nanostructures
• CPC Class Codes: C01B 2204/04 Specific amount of layers or specific thickness
• CPC Class Codes: C01B 32/184 Preparation
• CPC Class Codes: G01T 1/00 Measuring X-radiation, gamma radiation, corpuscular radiation, or cosmic radiation G01T3/00, G01T5/00 take precedence
• CPC Class Codes: H01J 5/18 Windows permeable to X-rays, gamma-rays, or particles

Abstract

A method of making graphene sheets having a desired thickness. The method starts with Highly Oriented Pyrolytic Graphite (“HOPG”). A plurality of graphene layers are pulled off of the HOPG and attached to a substrate. An adhesive device is then used to pull a selected number of graphene layers off of the HOPG sample attached to the substrate. The number of layers selected determines the thickness of the graphene sheet produced. The graphene sheet has many applications. It is particularly suitable as an X-ray window.

Claims

1. A method of producing a sheet of graphene having a desired thickness, comprising:

a. providing a piece of Highly Oriented Pyrolytic Graphite;

b. providing a substrate;

c. applying an adhesive to said substrate;

d. pulling a plurality of graphene layers from said Highly Oriented Pyrolytic Graphite and attaching them to said substrate using said adhesive placed on said substrate;

e. providing an adhesive cylinder;

f. rolling said adhesive cylinder over said plurality of graphene layers on said substrate to selectively remove some of said graphene layers, thereby leaving a desired number of graphene layers on said substrate.

2. A method of producing a sheet of graphene as recited in claim 1, wherein said adhesive cylinder has a radius, and wherein said radius is selected to determine the number of graphene layers removed from said substrate for each pass of said adhesive cylinder.

3. A method of producing a sheet of graphene as recited in claim 1, further comprising:

a. providing a piece of double sided tape; and

b. wherein said step of pulling a plurality of graphene layers from said Highly Oriented Pyrolytic Graphite is performed by applying said piece of double sided tape to said Highly Oriented Pyrolytic Graphite and pulling said piece of double sided tape away.

4. A method of producing a sheet of graphene as recited in claim 2, further comprising:

a. providing a piece of double sided tape; and

b. wherein said step of pulling a plurality of graphene layers from said Highly Oriented Pyrolytic Graphite is performed by applying said piece of double sided tape to said Highly Oriented Pyrolytic Graphite and pulling said piece of double sided tape away.

5. A method of producing a sheet of graphene having a desired thickness, comprising:

a. providing a piece of Highly Oriented Pyrolytic Graphite;

b. providing a substrate;

c. pulling a plurality of graphene layers from said Highly Oriented Pyrolytic Graphite and attaching them to said;

d. providing an adhesive object; and

f. using said adhesive object to selectively remove some of said graphene layers from said substrate, thereby leaving a desired number of graphene layers on said substrate.

6. A method of producing a sheet of graphene as recited in claim 5, wherein said adhesive cylinder has a radius, and wherein said radius is selected to determine the number of graphene layers removed from said substrate for each pass of said adhesive cylinder.

7. A method of producing a sheet of graphene as recited in claim 5, further comprising:

a. providing a piece of double sided tape; and

b. wherein said step of pulling a plurality of graphene layers from said Highly Oriented Pyrolytic Graphite is performed by applying said piece of double sided tape to said Highly Oriented Pyrolytic Graphite and pulling said piece of double sided tape away.

8. A method of producing a sheet of graphene as recited in claim 6, further comprising:

a. providing a piece of double sided tape; and

b. wherein said step of pulling a plurality of graphene layers from said Highly Oriented Pyrolytic Graphite is performed by applying said piece of double sided tape to said Highly Oriented Pyrolytic Graphite and pulling said piece of double sided tape away.