SEED RETAINING MEMBER AND METHOD OF MANUFACTURING POLHYCRYSTALLINE SILICON USING THE SEED RETAINING MEMBER

• US 20120186300A1
• Filed: 09/02/2010
• Published: 07/26/2012
• Est. Priority Date: 09/02/2009
• Status: Abandoned Application

• Current Assignee: TOYO Tanso Company Limited
• Original Assignee: TOYO Tanso Company Limited
• Inventors: Ishizaki, Jun, Izumiya, Masaki
• Application Number:
  US13/392,688
• Publication Number:
  US 20120186300A1
• Time in Patent Office: Days
• US Class Current: 65/33.3
• CPC Class Codes: C01B 33/035 by decomposition or reduction of gaseous or vaporised silicon compounds in the presence of heated filaments of silicon, carbon or a refractory metal, e.g. tantalum or tungsten, or in the presence of heated silicon rods on which the formed silicon is deposited, a silicon rod being obtained, e.g. Siemens process

Abstract

A seed retaining member has a recessed portion for breaking and separating formed at an arbitrary location and thereby allows stress concentration to occur at the recessed portion when applying a breaking load, to enable the seed retaining member to break with a smaller load than conventional. So that the seed retaining member can prevent a crack from propagating in an unintended location in the seed retaining member by allowing the crack to propagate along the recessed portion, and also can reduce a workload in a separation work of the seed retaining member and polycrystalline silicon.

The seed retaining member for retaining a lower end portion of a seed serving as a seed rod and disposed at a bottom portion of a furnace for producing polycrystalline silicon by a Siemens method. A groove for breaking and separating is formed in an outer peripheral surface of the seed retaining member.

Claims

1-9. -9. (canceled)

10. A seed retaining member, made of graphite and attached to an electrode portion disposed at a bottom portion of a furnace for producing polycrystalline silicon by a Siemens method, for retaining a lower end portion of a seed serving as a seed rod, characterized by having a recessed portion for breaking and separating, formed at an arbitrary location in an outer peripheral surface thereof.

11. The seed retaining member according to claim 10, wherein the recessed portion is a groove for breaking and separating.

12. The seed retaining member according to claim 11, wherein the groove for breaking and separating is formed in an entire circumference of the seed retaining member or a portion of the circumference.

13. The seed retaining member according to claim 11, wherein the groove for breaking and separating extends along the circumference of the outer peripheral surface of the seed retaining member.

14. The seed retaining member according to claim 12, wherein the groove for breaking and separating extends along the circumference of the outer peripheral surface of the seed retaining member.

15. The seed retaining member according to claim 11, wherein the groove for breaking and separating is formed below a grown portion of the silicon crystal that has been grown from the seed surface and deposited on the surface of the seed retaining member.

16. The seed retaining member according to claim 12, wherein the groove for breaking and separating is formed below a grown portion of the silicon crystal that has been grown from the seed surface and deposited on the surface of the seed retaining member.

17. The seed retaining member according to claim 13, wherein the groove for breaking and separating is formed below a grown portion of the silicon crystal that has been grown from the seed surface and deposited on the surface of the seed retaining member.

18. The seed retaining member according to claim 14, wherein the groove for breaking and separating is formed below a grown portion of the silicon crystal that has been grown from the seed surface and deposited on the surface of the seed retaining member.

19. The seed retaining member according to claim 10, wherein a tip of the seed retaining member is formed in a conical frustum shape.

20. The seed retaining member according to claim 11, wherein a tip of the seed retaining member is formed in a conical frustum shape.

21. The seed retaining member according to claim 12, wherein a tip of the seed retaining member is formed in a conical frustum shape.

22. The seed retaining member according to claim 13, wherein a tip of the seed retaining member is formed in a conical frustum shape.

23. The seed retaining member according to claim 15, wherein a tip of the seed retaining member is formed in a conical frustum shape.

24. A method of manufacturing polycrystalline silicon by a Siemens method, comprising the steps of:

pre-forming a recessed portion for breaking and separating at an arbitrary location of an outer peripheral surface of a seed retaining member for retaining a lower end portion of a seed serving as a seed rod, and attaching the seed retaining member in which the recessed portion has been formed to an electrode portion disposed at a bottom portion of a furnace for manufacturing polycrystalline silicon;

depositing polycrystalline silicon on a surface of the seed;

after depositing polycrystalline silicon on the surface of the seed, breaking the seed retaining member at the recessed portion and taking the seed on which the polycrystalline silicon has been deposited out of the furnace; and

performing a separation work of the seed retaining member and the polycrystalline silicon from the seed that has been taken out of the furnace.

26. The method of manufacturing polycrystalline silicon according to claim 24, wherein the recessed portion is a groove for breaking and separating.

25. A method of manufacturing polycrystalline silicon by a Siemens method, comprising the steps of:

pre-forming a recessed portion for breaking and separating at an arbitrary location of an outer peripheral surface of a seed retaining member for retaining a lower end portion of a seed serving as a seed rod, and attaching the seed retaining member in which the recessed portion has been formed to an electrode portion disposed at a bottom portion of a furnace for manufacturing polycrystalline silicon;

depositing polycrystalline silicon on a surface of the seed;

after the depositing of polycrystalline silicon, removing the seed retaining member retaining the seed from the electrode portion and taking the seed retaining member retaining the seed out of the furnace; and

after taking the seed retaining member retaining the seed out of the furnace, breaking the seed retaining member with the seed being retained at the recessed portion to carry out a separation work of the seed retaining member and the polycrystalline silicon.

27. The method of manufacturing polycrystalline silicon according to claim 25, wherein the recessed portion is a groove for breaking and separating.