TRANSLUCENT SMOKELESS TOBACCO PRODUCT

• US 20130074855A1
• Filed: 09/22/2011
• Published: 03/28/2013
• Est. Priority Date: 09/22/2011
• Status: Active Grant

• Current Assignee: R J Reynolds Tobacco Company (R. J. Reynolds Tobacco)
• Original Assignee: R J Reynolds Tobacco Company (R. J. Reynolds Tobacco)
• Inventors: Holton, Darrell Jr.
• Granted Patent: US 9,084,439 B2
• Time in Patent Office: Days
• US Class Current: 131/275
• CPC Class Codes: A24B 15/10 Chemical features of tobacco products or tobacco substitutes
• CPC Class Codes: A24B 15/24 by extraction; Tobacco extracts
• CPC Class Codes: A24B 15/30 by organic substances A24B15/281 takes precedence

Abstract

The invention provides a smokeless tobacco product comprising a tobacco extract. In some embodiments, the smokeless tobacco product is translucent. The invention further provides methods for making and using the smokeless tobacco product. In certain embodiments, the smokeless tobacco product comprises isomalt, maltitol syrup, and a translucent tobacco extract prepared by ultrafiltration.

Claims

1. A smokeless tobacco product comprising:

a. a tobacco extract in an amount of at least about 3% by weight;

b. a sugar substitute in an amount of at least about 80% by weight; and

c. a sugar alcohol syrup,

wherein the smokeless tobacco product is translucent.

2. The smokeless tobacco product of claim 1, wherein the sugar substitute is a non-hygroscopic sugar alcohol capable of forming a glassy matrix.

3. The smokeless tobacco product of claim 1, wherein the sugar substitute is isomalt.

4. The smokeless tobacco product of claim 1, wherein the sugar substitute is present in an amount of at least about 85% by weight.

5. The smokeless tobacco product of claim 1, wherein the sugar substitute is present in an amount of at least about 90% by weight.

6. The smokeless tobacco product of claim 1, wherein the sugar alcohol syrup is maltitol syrup.

7. The smokeless tobacco product of claim 1, wherein the tobacco extract is an ultrafiltered tobacco extract characterized as translucent or transparent.

8. The smokeless tobacco product of claim 1, wherein the tobacco extract is a heat-treated tobacco extract that has been treated prior to inclusion in the smokeless tobacco product by heating the tobacco extract in an aqueous solution comprising L-lysine, L-cysteine, asparaginase, or hydrogen peroxide.

9. The smokeless tobacco product of claim 8, wherein the aqueous solution further comprises NaOH.

10. The smokeless tobacco product of claim 1, wherein the tobacco extract is a heat-treated tobacco extract that has been treated prior to inclusion in the smokeless tobacco product by heating the tobacco extract in an aqueous solution comprising L-lysine and NaOH.

11. The smokeless tobacco product of claim 1, wherein the tobacco extract consists of compounds having a molecular weight of less than about 50,000 Da.

12. The smokeless tobacco product of claim 10, wherein the tobacco extract consists of compounds having a molecular weight of less than about 5,000 Da.

13. The smokeless tobacco product of claim 1, further comprising one or more flavorants.

14. The smokeless tobacco product of claim 12, wherein the amount of flavorant is from about 0.1 to about 0.5 percent by weight of the smokeless tobacco product.

15. The smokeless tobacco product of claim 13, wherein the flavorant is vanillin or mint flavor.

16. The smokeless tobacco product of claim 1, further comprising at least one sweetener.

17. The smokeless tobacco product of claim 15, wherein the at least one sweetener comprises sucralose.

18. The smokeless tobacco product of claim 1, further comprising NaCl.

19. The smokeless tobacco product of claim 17, wherein the amount of NaCl is from about 0.5 to about 1 percent by weight of the smokeless tobacco product.

20. A translucent smokeless tobacco product comprising:

a. a translucent or transparent tobacco extract consisting of components having a molecular weight of no more than about 50,000 Da in an amount of at least about 3% by weight;

b. a non-hygroscopic sugar alcohol capable of forming a glassy matrix in an amount of at least about 80% by weight; and

c. a sugar alcohol syrup in an amount sufficient to slow recrystallization of the non-hygroscopic sugar alcohol,

wherein the smokeless tobacco product is translucent.

21. A method of preparing a translucent smokeless tobacco product, comprising:

(i) mixing a translucent or transparent tobacco extract with a non-hygroscopic sugar alcohol capable of forming a glassy matrix in a melted state to form a mixture; and

(ii) cooling the mixture to room temperature to form a solid smokeless tobacco product exhibiting translucency.

22. The method of claim 21, wherein the translucent or transparent tobacco extract has been treated by size exclusion chromatography, microfiltration, ultrafiltration, nanofiltration, reverse osmosis, or a combination thereof.

23. The method of claim 22, wherein the treatment removes components having a molecular weight above about 50,000 Da.

24. The method of claim 21, wherein the translucent or transparent tobacco extract has been heat treated by heating the tobacco extract in an aqueous solution comprising L-lysine, L-cysteine, asparaginase, or hydrogen peroxide.

25. The method of claim 23, wherein the aqueous solution further comprises NaOH.

26. The method of claim 23, wherein the heat treating step is conducted at about 88°

C.

27. The method of claim 24, wherein the translucent smokeless tobacco product has an acrylamide content of less than about 500 ppb.

28. The method of claim 21, wherein the mixing step comprises heating the non-hygroscopic sugar alcohol to a temperature above the hard crack stage in the absence of the tobacco extract and mixing the tobacco extract into the non-hygroscopic sugar alcohol at a temperature below the hard crack stage.

29. The method of claim 28, wherein the hard crack stage is about 145°

C. to about 155°

C. and the non-hygroscopic sugar alcohol is heated at a temperature between the hard crack stage and about 171°

C.

30. The method of claim 21, further comprising introducing the mixture into molds to create individual product units prior to the cooling step.

31. A method of preparing a translucent or transparent extract for incorporating into a smokeless tobacco product, comprising:

(i) extracting a tobacco material with an aqueous solvent to form an aqueous tobacco extract;

(ii) ultrafiltering the aqueous tobacco extract to remove components having a molecular weight above about 50,000 Da to form a translucent or transparent tobacco extract; and

(iii) heat treating the tobacco extract prior to or after step (ii) by heating the extract in an aqueous solution comprising L-lysine, L-cysteine, asparaginase, or hydrogen peroxide.

32. The method of claim 31, wherein the ultrafiltering step comprises passing the aqueous tobacco extract through multiple ultrafiltration membranes.