Thin Stillage Clarification

• US 20140319066A1
• Filed: 03/23/2014
• Published: 10/30/2014
• Est. Priority Date: 03/23/2013
• Status: Abandoned Application

• Current Assignee: Yield and Capacity Group LLC
• Original Assignee: Yield and Capacity Group LLC
• Inventors: LoCascio, Michael B., Dunbar, Ronald K.
• Application Number:
  US14/222,678
• Publication Number:
  US 20140319066A1
• Time in Patent Office: Days
• US Class Current: 210/710
• CPC Class Codes: C12F 3/10 from distillery slops

Abstract

Systems and methods for improving the quality of solids and liquids recovered at atmospheric pressure and temperature from a stillage stream generated as a by-product of an ethanol production process, the recovered solids having higher bio-available amino and fatty acids than evaporation-produced condensed solubles, the recovered liquids having less total solids and total suspended solids than evaporation-produced condensate. A static mixer includes an input for receiving the stillage stream combined with a GRAS anionic polymer, a cylindrical mixing chamber that controllably mixes the stillage stream and the polymer to generate wet flocculated solids and liquid co-product, and a discharge chute that outputs the wet flocculated solids and liquid co-products onto a moving, gravity filter belt having a membrane surface that separates the output from the static mixer into recovered liquids in the form of clarified, thin stillage and recovered solids in the form of dry flocculated solids.

Claims

1. A system for improving quality of solids and liquids recovered at atmospheric pressure and temperature from a stillage stream generated as a by-product of an ethanol production process, the recovered solids having higher bio-available amino acids and fatty acids than evaporation-produced condensed solubles obtainable from the stillage stream, the recovered liquids having less total solids (TS) and total suspended solids (TSS) than centrifuge-produced thin stillage obtainable from the stillage stream, the system comprising:

a static mixer having;

(i) an input for receiving the stillage stream and for receiving a predetermined amount of generally-regarded-as-safe (GRAS) anionic polymer, the combined stillage stream and GRAS anionic polymer forming a GRAS-treated stillage;

(ii) a cylindrical mixing chamber configured to mix the GRAS-treated stillage at a predetermined laminar flow rate that chemically generates wet flocculated solids and liquid co-product; and

(iii) a discharge chute for outputting the wet flocculated solids and liquid co-products from the cylindrical mixing chamber;

and a moving, gravity filter belt being sloped at an angle relative to the discharge chute, one end of the filter belt positioned to receive the wet flocculated solids and liquid co-products output from the discharge chute of the cylindrical mixing chamber, the filter belt having a membrane surface configured to allow liquid co-products and liquids settling out from the wet flocculated solids to pass therethrough as clarified, thin stillage, the membrane surface further configured to retain and discharge dry flocculated solids at the other end of the filter belt;

wherein the clarified, thin stillage represents the recovered liquids and the dry flocculated solids represent the recovered solids.

2. The system of claim 1, wherein the stillage stream is thick or thin stillage.

3. The system of claim 1, wherein 10-60% of the total solids (TS) and 70-99% of the total suspended solids (TSS) in the stillage stream are captured in the dry flocculated solids.

4. The system of claim 1, wherein the GRAS anionic polymer is an anionic polyacrylamide having an anionicity mole charge percentage between 30-70%.

5. The system of claim 1, wherein the predetermined amount of GRAS anionic polymer is between 20-40 ppm.

6. The system of claim 1, wherein the cylindrical mixing chamber has a rotational mixing energy measured in revolutions per minute (RPM) that is a function of its height and its diameter, wherein the height (Ht) is equal to VV×

HRT, wherein VV represents vertical velocity of the GRAS-treated stillage through the cylindrical mixing chamber and HRT represents hydraulic retention time of the GRAS-treated stillage within the cylindrical mixing chamber, and wherein the diameter is equal to square root ((((PF×

(HRT/60))/7.48)/(Ht))/Pi, wherein PF represents process flow in gallons per minute of the GRAS-treated stillage within the cylindrical mixing chamber.

7. The system of claim 6, wherein the HRT is measured in seconds and has a range of between 60 and 300 seconds, wherein the VV is measured in feet/second and has a range of between 0.01 and 0.10 feet/second, and wherein the RPM of the GRAS-treated stillage within the cylindrical mixing chamber is between 2 and 5 RPM.

8. The system of claim 7, wherein the VV has a preferred range between 0.016 and 0.050 feet/second.

9. The system of claim 7, wherein the cylindrical mixing chamber includes baffles to control the RPM of the GRAS-treated stillage within the cylindrical mixing chamber.

10. The system of claim 1, wherein the membrane surface of the gravity filter belt has an air flow rating between 100-300 cubic feet per minute (cfm).

11. The system of claim 1, wherein the angle of the slope of the gravity filter belt relative to the discharge chute is between 0 and 15 degrees.

12. The system of claim 1, wherein the clarified, thin stillage is recycled back to a preparation stage of the ethanol production process.

13. The system of claim 1, wherein the clarified, thin stillage is then provided to an evaporator for further separation of solids and liquids contained in the clarified, thin stillage.

14. The system of claim 1, wherein the dry flocculated solids are collected and sold off either as wet distillers grains with solubles (WDGS) or dry distillers grains with solubles (DDGS).

15. The system of claim 1, wherein oil is extracted from the dry flocculated solids.

16. The system of claim 1, wherein the clarified, thin stillage includes spent yeast and wherein the spent yeast is extracted from the clarified, thin stillage using a solids-liquids separator.

17. The system of claim 16, wherein the solids-liquids separator is a disc stack centrifuge, a concentrating centrifuge, a cone bottom settling tank, or a hydrocyclone.

18. A method for improving quality of solids and liquids recovered at atmospheric pressure and temperature from a stillage stream generated as a by-product of an ethanol production process, the recovered solids having higher bio-available amino acids and fatty acids than evaporation-produced condensed solubles obtainable from the stillage stream, the recovered liquids having less total solids (TS) and total suspended solids (TSS) than centrifuge-produced thin stillage obtainable from the stillage stream, comprising the steps of:

combining (i) the stillage stream obtained from the ethanol production process with (ii) a predetermined amount of generally-regarded-as-safe (GRAS) anionic polymer in a static mixer, the static mixer having a cylindrical mixing chamber, the combined stillage stream and GRAS anionic polymer forming a GRAS-treated stillage;

mixing the GRAS-treated stillage at a predetermined laminar flow rate within the cylindrical mixing chamber of the static mixer, wherein mixing the GRAS-treated stillage chemically generates wet flocculated solids and liquid co-product;

discharging the wet flocculated solids and liquid co-product from the static mixer; and

filtering the discharged wet flocculated solids and liquid co-product to generate a clarified, thin stillage and dry flocculated solids;

wherein the clarified, thin stillage represents the recovered liquids and the dry flocculated solids represent the recovered solids, wherein 10-60% of the total solids (TS) and 70-99% of the total suspended solids (TSS) in the stillage stream are captured in the dry flocculated solids.

19. The method of claim 18, wherein the stillage stream is thick or thin stillage.

20. The method of claim 18, wherein the GRAS anionic polymer is an anionic polyacrylamide with an anionicity mole charge percentage between 30-70%.

21. The method of claim 18, wherein the predetermined amount of GRAS anionic polymer is between 20-40 ppm.

22. The method of claim 18, wherein the cylindrical mixing chamber has a rotational mixing energy measured in revolutions per minute (RPM) that is a function of its height and its diameter, wherein the height (Ht) is a function of the vertical velocity (VV), the hydraulic retention time (HRT), and the process flow (PF) of the GRAS-treated stillage within the cylindrical mixing chamber.

23. The method of claim 22, wherein the HRT is 60-300 seconds, the VV is 0.01-0.10 feet/second, and the RPM of the GRAS-treated stillage within the cylindrical mixing chamber is between 2 and 5 RPM.

24. The method of claim 18, further comprising recycling the clarified, thin stillage back to a preparation stage of the ethanol production process.

25. The method of claim 18, further comprising the steps of collecting and selling off the dry flocculated solids either as wet distillers grains with solubles (WDGS) or dry distillers grains with solubles (DDGS).

26. The method of claim 18, further comprising extracting oil from the dry flocculated solids.

27. The method of claim 18, wherein the clarified, thin stillage includes spent yeast and further comprising the step of extracting the spent yeast from the clarified, thin stillage using a solids-liquids separator.