MEASUREMENT APPARATUS AND METHOD

• US 20140320859A1
• Filed: 11/21/2012
• Published: 10/30/2014
• Est. Priority Date: 11/21/2011
• Status: Abandoned Application

• Current Assignee: University of Strathclyde
• Original Assignee: University of Strathclyde
• Inventors: Thennadil, Suresh N., Chen, Yi-Chieh
• Application Number:
  US14/358,653
• Publication Number:
  US 20140320859A1
• Time in Patent Office: Days
• US Class Current: 356/432
• CPC Class Codes: G01N 2021/0307 Insert part in cell
• CPC Class Codes: G01N 2021/4742 comprising optical fibres
• CPC Class Codes: G01N 2021/4769 Fluid samples, e.g. slurries, granulates; Compressible powdery of fibrous samples
• CPC Class Codes: G01N 2021/4783 Examining under varying incidence; Angularly adjustable head
• CPC Class Codes: G01N 2021/558 Measuring reflectivity and transmission
• CPC Class Codes: G01N 21/03 Cuvette constructions
• CPC Class Codes: G01N 21/0303 Optical path conditioning in cuvettes, e.g. windows; adapted optical elements or systems; path modifying or adjustment G01N21/031 - G01N21/15 take precedence
• CPC Class Codes: G01N 21/4738 Diffuse reflection precedence is given to G01N21/55 - G01N21/57 if specular component is taken into consideration, e.g. also for testing fluids, fibrous materials
• CPC Class Codes: G01N 21/55 Specular reflectivity
• CPC Class Codes: G01N 21/59 Transmissivity G01N21/25 takes precedence
• CPC Class Codes: G01N 2201/065 Integrating spheres

Abstract

A measurement system (5) comprises a radiation source (10) and a detection system (15), wherein the radiation source is arranged such that radiation from the radiation source is incident on a sample (25) and the detection system is configured to receive at least part of the radiation via the sample, wherein the system is reconfigurable so as to vary a path length that the radiation travels through the sample and/or a reflectance of at least one surface upon which the radiation is incident after passing through at least part of the sample. A property of the sample may be determined based on at least the first and second measurements.

Claims

1-38. -38. (canceled)

39. A measurement system comprising a radiation source and a detection system, wherein the radiation source is arranged or arrangeable such that radiation from the radiation source is incident on a sample and the detection system is configured or configurable to receive at least part of the radiation via the sample, wherein the system is reconfigurable so as to vary a path length that the radiation travels through the sample and/or a reflectance of at least one surface upon which the radiation is incident after passing through at least part of the sample.

40. The measurement system according to claim 39, wherein the measurement system comprises a sample holder, the sample holder being positioned or positionable so as to receive radiation from the radiation source.

41. The measurement system according to claim 39, wherein the measurement system is configured such that at least part of the radiation from the radiation source passes through at least part of the sample.

42. The measurement system according to claim 39, wherein the measurement system is configured to collect at least a first measurement of radiation that has passed through at least a first path length through the sample and/or been reflected from a surface having a first reflectance after passing through at least part of the sample and a second measurement of radiation that has passed through at least a second path length through the sample and/or has been reflected from a surface having a second reflectance after passing through at least part of the sample.

43. The measurement system according to claim 42, wherein the measurement system is configured to determine a property of the sample based on at least the first and second measurements.

44. The measurement system according to claim 41, wherein the measurement system is configured to make multiple measurements, each measurement being associated with a different radiation path length through the sample and/or reflectivity of a surface from which the radiation has been reflected after passing through at least a part of the sample relative to at least one other measurement.

45. The measurement system according to claim 40, wherein the sample holder comprises a sample chamber for holding the sample, wherein the sample chamber is divided or dividable into sections.

46. The measurement system according to claim 45, wherein the sample holder comprises at least one fitting for receiving a divider for the sample chamber and/or at least one divider for dividing the sample chamber.

47. The measurement system according to claim 46, wherein at least one of a divider or a back wall of the sample holder comprises a facing surface that is configured or configurable to face the radiation source, wherein the facing surface comprises a reflective or mirrored surface or a diffuse reflective surface or an opaque or blackened surface or a transmissive or transparent surface.

48. The measurement system according to claim 45, wherein the divider is movable within the sample chamber,

49. The measurement system according to claim 48, wherein the divider is mounted to a movable member comprise at least one marker for marking a range of motion of the movable member and/or at least one stopping member for limiting the motion of the divider at a predetermined position in the sample chamber.

50. The measurement system according to claim 40, wherein the measurement system comprises Interchangeable sample holders of varying dimensions, wherein at least the first and second path lengths are defined by the dimensions of differing sample holders and/or the first and second reflectivities are defined by differing reflectivities of at least one surface of differing sample holders.

51. The measurement system according to claim 40, wherein the detection system is movably mounted on guide apparatus so as to be movable relative to the sample holder and/or radiation source.

52. The measurement system according to claim 40, wherein the sample holder is movable or removable and the guide apparatus or a housing of the measurement system comprises placing means or fixing points for mounting the sample holder in a predetermined position and/or orientation.

53. The measurement system according to claim 43, wherein the measurement system comprises, or is configured to communicate with, processing apparatus, the processing apparatus being adapted to determine at least one property of the sample based on at least the first and second measurements.

54. The measurement system according to claim 53, wherein the processing apparatus is configured to determine the at least one property of the sample by fitting theoretically calculated parameters based on a trial model against the two or more measurements and/or to determine at least one property by comparing measurement data with reference data, which may be stored in a database or look up table.

55. The measurement system according to claim 39, wherein the measurement system comprises a measurement probe.

56. The measurement system according to claim 55, wherein a plurality of optical fibres are comprised in the measurement probe such that at least one optical fibre is spaced apart from at least one other optical fibre and/or at least one optical fibre Is oriented at a different angle relative to at least one other optical fibre.

57. The measurement system according to claim 56, wherein the one or more optical fibres are connected or connectable to a multiplexer and the multiplexer Is connected to a detector.

58. The measurement system according to claim 55, wherein the measurement probe comprises at least one light emitter.

59. The measurement system of claim 58, wherein at least one light emitter comprises an end of one of the optical fibres, and another end of the optical fibre being connected or connectable to the radiation source.

60. The measurement system according to any of claim 57, wherein the detector is configured to record radiation intensity at a number of wavelengths.

61. The measurement system according to any of claim 42, wherein the system is configured to collect both reflected and transmitted radiation, which corresponds to respective first and second measurements.

70. A processing system for processing measurements collected using the apparatus according to claim 39.

71. A computer program product comprising at least one non-transitory computer-readable storage medium having computer-readable program code portions stored therein, the computer-readable program code portions comprising one or more executable portions for implementing the system of claim 39.

62. A method of collecting optical measurements using a measurement system comprising a radiation source and detection system, the method comprising:

configuring the system such that radiation from the radiation source passes through the sample along a first path length and/or is reflected from a surface having a first reflectivity;

performing at least a first measurement that comprises measuring radiation from the sample after having passed through the first path length and/or having being reflected from the surface having the first reflectivity;

configuring the system such that radiation from the radiation source passes through the sample along a second path length and/or is reflected from a surface having a second reflectance;

performing at least a second measurement that comprises measuring radiation from the sample after having passed through the second path length and/or having being reflected from the surface having the second reflectivity;

determining at least one property of the sample from at least the first and second measurements.

63. An optical measurement system comprising a radiation source and detection system, wherein the detection system is mounted to a guide for moving the detection system between at least two collinear positions.

64. The optical measurement system according to claim 63, wherein the detection system is linearly movable.

65. The optical measurement system according to claim 63, wherein the system comprises a sample holder and the detection system is movable between a side of the sample holder towards the radiation source and a side of the sample holder away from the radiation source.

66. The optical measurement system according to claim 63, wherein the guide comprises at least two stopping means for limiting motion of the defection system in a corresponding predetermined position or positions.

67. The optical measurement system according to claim 63, wherein the sample holder is movable or removable, and the guide or a housing of the optical measurement systems comprises placing means or fixing points for mounting the sample holder in a predetermined position and/or orientation.

68. A sensor probe comprising two or more optical fibres for detecting radiation from a sample, wherein the at least one of the optical fibres is spaced apart from at least one other optical fibre and/or at least one optical fibre is angled with respect to at least one ether of the optical fibres.

69. The measurement probe according to claim 68, wherein the sensor probe comprises at least one Sight emitter, wherein the light emitter comprises an end of an optical fibre for receiving light from a light source.

72. A sample holder, the sample holder comprising a sample chamber for holding the sample, wherein the sample chamber is divided or dividable into sections and/or the sample holder comprises a movable divider for varying a dimension of the sample chamber.