FITTING FOR ELASTICALLY-BIASING A CAPILLARY FOR A FLUID-TIGHT CONNECTION TO A FLUIDIC CONDUIT

• US 20150090595A1
• Filed: 11/15/2012
• Published: 04/02/2015
• Est. Priority Date: 11/15/2012
• Status: Active Grant

• Current Assignee: Agilent Technologies, Inc.
• Original Assignee: Agilent Technologies, Inc.
• Inventors: Zeko, Darijo, Lueth, Claus
• Granted Patent: US 9,482,649 B2
• Time in Patent Office: Days
• US Class Current: 204/605
• CPC Class Codes: B01D 15/22 relating to the construction of the column
• CPC Class Codes: B01D 53/0407 Constructional details of adsorbing systems
• CPC Class Codes: B01D 57/02 by electrophoresis treatment of water, waste water, sewage or sludge by electrophoresis C02F1/469; electrophoretic production of compounds or non-metals C25B7/00; investigating or analysing materials by using electrophoresis G01N27/26
• CPC Class Codes: F16L 15/08 with supplementary elements F16L15/04, F16L41/00 and F16L43/02 take precedence
• CPC Class Codes: F16L 19/02 Pipe ends provided with collars or flanges, integral with the pipe or not, pressed together by a screwed member
• CPC Class Codes: G01N 2030/025 Gas chromatography
• CPC Class Codes: G01N 2030/027 Liquid chromatography
• CPC Class Codes: G01N 30/60 Construction of the column
• CPC Class Codes: G01N 30/6004 end pieces
• CPC Class Codes: G01N 30/6026 Fluid seals
• CPC Class Codes: Y10T 29/49826 Assembling or joining

Abstract

A fitting (200) for providing a fluid connection between a capillary (202) and a fluidic conduit (204) of a fluidic component (30), the fitting (200) comprising a male piece (240) and a female piece (250) for connection with the male piece (240), wherein the male piece (240) comprises a housing (252) with a capillary reception (212) configured for receiving the capillary (202), wherein a part of the capillary (202) being received in the capillary reception (212) is circumferentially covered by a sleeve (214), an elastic biasing mechanism (206) being arranged at least partially within the housing (252), being configured for biasing the capillary (202) against the female piece (250) and being supported by the sleeve (214), and a locking mechanism (208) being arranged at least partially within the housing (252) and being configured for locking the capillary (202) to the fitting (200).

Claims

1. A fitting for providing a fluid connection between a capillary and a fluidic conduit of a fluidic component, the fitting comprising a male piece and a female piece for connection with the male piece, the male piece comprising:

a housing with a capillary reception configured for receiving the capillary, wherein a part of the capillary being received in the capillary reception is circumferentially covered by a sleeve;

an elastic biasing mechanism being arranged at least partially within the housing, being configured for biasing the capillary against the female piece and being supported by the sleeve; and

a locking mechanism being arranged at least partially within the housing and being configured for locking the capillary to the fitting.

2. The fitting according to claim 1, wherein the elastic biasing mechanism is supported by an annular flange face of the sleeve, particularly by an annular flange face at a back side of the sleeve.

3. The fitting according to claim 1, wherein the locking mechanism is configured for locking the capillary at an annular flange face of the sleeve, particularly by an annular flange face at a back side of the sleeve.

4. The fitting according to claim 1, wherein the elastic biasing mechanism is mounted so as to press the sleeve forwardly towards the female piece.

5. The fitting according to claim 1, wherein the elastic biasing mechanism is supported between the sleeve and an abutment face at a back side of the housing.

6. The fitting according to claim 1, wherein the elastic biasing mechanism comprises a spring.

7. The fitting according to claim 1, wherein the elastic biasing mechanism comprises a mechanical spring.

8. The fitting according to claim 7, wherein the mechanical spring comprises one of the group consisting of a helical spring, a disc spring, and a leaf spring.

9. The fitting according to claim 1, wherein the elastic biasing mechanism comprises a magnetic spring.

10. The fitting according to claim 9, wherein the magnetic spring comprises a first magnetic element and a second magnetic element which are configured to attract or to repel one another and being mounted movably relative to one another.

11. The fitting according to claim 10, wherein the first magnetic element is mounted at a fixed position within the housing of the male piece, and the second magnetic element is mounted movably within the housing so as to apply a biasing force to the sleeve.

12. The fitting according to claim 1, wherein the elastic biasing mechanism comprises a fluid-based spring.

13. The fitting according to claim 12, wherein the fluid-based spring comprises one of the group consisting of a hydraulic spring, and a pneumatic spring, particularly a gas pressure spring.

14. The fitting according to claim 1, wherein the male piece comprises a clamping ring being axially interposed between the elastic biasing mechanism and the sleeve and being shaped so as to convert an axial biasing force exerted by the elastic biasing mechanism partially into a radial gripping force exerted to the capillary surrounded by the sleeve.

15. The fitting according to claim 1,

wherein the elastic biasing mechanism comprises a first magnetic element fixed to the housing and a second magnetic element mounted movable in the capillary reception and attracting the first magnetic element;

wherein the male piece comprises a clamping ring being axially interposed between the second magnetic element on the one hand and the first magnetic element and the sleeve on the other hand and being shaped so as to convert an axial biasing force exerted by the attracting magnetic elements partially into a radial gripping force exerted to the capillary surrounded by the sleeve.

16. The fitting according to claim 15, wherein the clamping ring has a tapering back part and a widening front part, the tapering back part being configured for centering the capillary along the capillary reception upon insertion from the back of the male part, and the widening front part being configured for locking the capillary to the fitting upon forwarding the capillary to such an extent that a back end of the sleeve passes from the tapering front part into the widening back part.

17. The fitting according to claim 1,

wherein the elastic biasing mechanism comprises a first magnetic element mounted movable or fixed to the housing and a second magnetic element mounted movable in the capillary reception and repelling the first magnetic element;

wherein the male piece comprises a clamping ring being attached to a front flange face of the second magnetic element opposing a back surface of the second magnetic element facing the first magnetic element, the clamping ring being lockable to the sleeve.

18. The fitting according to claim 17, wherein the clamping ring has a support annulus and a plurality of beams protruding inwardly from the support annulus for being bent upon interaction with the sleeve.

19. The fitting according to claim 1, wherein the elastic biasing mechanism and the locking mechanism are integrally formed as a single component, particularly as an injection molded component.

20. The fitting according to claim 19, wherein the single component has an axial lumen for receiving the capillary, has an axial slit and multiple radial slits for providing a spring property, having an annular front flange for abutting against an annular back flange of the sleeve, and having an annular protrusion.

21. The fitting according to claim 1, wherein the male piece comprises an annular cap inserted into a back portion of the capillary reception of the housing and being configured for preventing the elastic biasing mechanism from leaving the capillary reception, particularly engaging a back end of the elastic biasing mechanism.

22. The fitting according to claim 1, wherein the capillary reception has a neck in a central portion of the housing, the neck connecting a wider back portion and a wider front portion of the capillary reception.

23. The fitting according to claim 22, wherein the wider back portion accommodates at least part of the elastic biasing mechanism and at least part of the locking mechanism.

24. The fitting according to claim 22, wherein the male piece comprises

a clamping chuck accommodated in the wider front portion;

and

a ferrule abutting against the clamping chuck, being accommodated partially in and protruding over the wider front portion and being configured for sealingly abutting against a sealing surface of the female piece upon connecting the male piece and the female piece.

25. The fitting according to claim 24, wherein the ferrule has a tubular back part accommodated in the wider front portion and has a tapering front part protruding over the wider front portion&

.

26. The fitting according to claim 1, wherein the male piece comprises a first connection element, particularly an external thread, and the female piece comprises a second connection element, particularly an internal thread, being configured correspondingly to the first connection element so that the first connection element and the second connection element are connectable to form a connection, particularly a screwing connection, between the male piece and the female piece.

27. The fitting according to claim 1, wherein the locking mechanism is configured so that the locking of the capillary to the fitting is releasable by applying a locking release force for removing the capillary from the capillary reception via a back side of the male piece.

28. A fluidic device for conducting a fluidic sample, the fluidic device comprising

a fluidic component having a fluidic conduit;

a capillary; and

a fitting according to claim 1 for providing a fluid connection between the capillary when received in the fitting and the fluidic conduit of the fluidic component when connected to or forming part of the fitting for conducting the fluidic sample through the fluidic device.

29. The fluidic device according to claim 28, wherein a part of the capillary portion being received in the capillary reception is circumferentially covered by a sleeve, particularly by a tubular sleeve being integrally formed with the capillary.

30. The fluidic device according to claim 28, wherein the fluidic component comprises a processing element configured for processing the fluidic sample.

31. The fluidic device according to claim 30, wherein the processing element is configured for retaining the fluidic sample being a part of a mobile phase and for allowing other components of the mobile phase to pass the processing element.

32. The fluidic device according to claim 30, wherein the processing element is a separation column.

33. The fluidic device according to claim 30, wherein the processing element comprises a chromatographic column for separating components of the fluidic sample.

34. The fluidic device according to claim 28, configured to conduct the fluidic sample through the fluidic conduit and the capillary with a high pressure.

35. The fluidic device according to claim 28, configured to conduct the fluidic sample through the fluidic conduit and the capillary with a pressure of at least 100 bar, particularly of at least 500 bar, more particularly of at least 1000 bar.

36. The fluidic device according to claim 28, configured as a fluid separation system for separating compounds of the fluidic sample.

37. The fluidic device according to claim 28, configured as a chromatography device, particularly a liquid chromatography device or a gas chromatography device, more particularly a HPLC.

38. The fluidic device according to claim 28, configured as at least one of the group consisting of a sensor device, a device for chemical, biological and/or pharmaceutical analysis, and a gel electrophoresis device.

39. The fluidic device according to claim 28, configured as a microfluidic device or a nanofluidic device.

40. A method for providing a fluid connection between a capillary and a fluidic conduit of a fluidic component by a fitting and a female piece, the method comprising:

receiving the capillary in a capillary reception within a housing of the male piece, wherein a part of the capillary received in the capillary reception is circumferentially covered by a sleeve;

locking the capillary to the fitting by a locking mechanism of the male piece (240), the locking mechanism (208) being arranged at least partially within the housing; and

connecting the male piece with the female piece to thereby form a fluid-tight connection between the capillary and the fluidic conduit forming part of or being in fluid connection with the female piece, wherein the capillary is elastically biased against the female piece by an elastic biasing mechanism of the male piece supported by the sleeve, the elastic biasing mechanism being arranged at least partially within the housing.

41. The method according to claim 40, wherein the method comprises inserting the capillary in the capillary reception from a back side of the male piece by a user applying a locking force until the capillary is locked to the fitting.

42. The method according to claim 40, wherein the method comprises removing the capillary from the capillary reception via a back side of the male piece by a user overcoming a locking release force with which the capillary is locked to the fitting.

43. The method according to claim 41, wherein the locking release force is higher than the locking force.