SEALING ELEMENT FOR A FLUIDIC CONNECTION

• US 20150233503A1
• Filed: 05/22/2012
• Published: 08/20/2015
• Est. Priority Date: 05/22/2012
• Status: Active Grant

• Current Assignee: Agilent Technologies, Inc.
• Original Assignee: Agilent Technologies, Inc.
• Inventors: Reinhardt, Thomas, Wagner, Joachim-Richard
• Granted Patent: US 9,816,647 B2
• Time in Patent Office: Days
• US Class Current: 1/1
• CPC Class Codes: F16J 15/022 characterised by structure or material
• CPC Class Codes: F16L 19/065 the wedging action being effected by means of a ring
• CPC Class Codes: F16L 21/005 made of elastic material, e.g. partly or completely surrounded by clamping devices comprising packing adapted to sealing by fluid pressure F16L17/04, F16L11/20; hose clips F16L33/02
• CPC Class Codes: G01N 2030/027 Liquid chromatography
• CPC Class Codes: G01N 30/461 with serial coupling of separation columns
• CPC Class Codes: G01N 30/60 Construction of the column
• CPC Class Codes: G01N 30/6026 Fluid seals
• CPC Class Codes: G01N 30/6039 in series
• CPC Class Codes: Y10T 29/49826 Assembling or joining
• CPC Class Codes: Y10T 29/49872 Confining elastic part in socket

Abstract

A sealing element (100) for sealing a fluidic connection between a coupling element (258) and a tubular element (136) and thereby providing a sealed flow path through the tubular element (136) and between the coupling element (258) and the tubular element (136) in a longitudinal direction (104), the sealing element (100) comprising: a recess (102) extending in the longitudinal direction (104), the recess (102) being adapted for receiving the tubular element (136); a transverse wall (106) defining an extent of the recess (102) in the longitudinal direction (104), the transverse wall (106) having a through hole (108).

Claims

1. A sealing element for sealing a fluidic connection between a coupling element and a tubular element and thereby providing a sealed flow path through the tubular element and between the coupling element and the tubular element in a longitudinal direction, the sealing element comprising:

a recess extending in the longitudinal direction, the recess being adapted for receiving the tubular element; and

a transverse wall defining an extent of the recess in the longitudinal direction, the transverse wall having a through hole.

2. The sealing element claim 1, further comprising:

the recess comprises at least one retaining element for retaining the tubular element in the recess;

the sealing element further comprising at least one feature selected from a group of features consisting of;

the sealing element includes at least three of the retaining elements, the at least three retaining elements being spaced from each other in a circumferential direction;

least one retaining element is configured for exerting a radially inwardly directed force onto the tubular element;

the at least one retaining element is a protrusion located in the recess;

the at least one retaining element is formed in the recess by a straight wall portion extending between two curved wall portions flanking the straight wall portion in circumferential directions; and

the at least one retaining element formed as increased wall thickness extending radially inwardly, in particular extending radially inwardly as much as necessary to clamp and center the tubular element.

3. The sealing element claim 1, further comprising:

a conical outer surface portion, the conical outer surface portion having a diameter increasing in a direction from the transverse wall towards the recess;

wherein the sealing element comprises an inner surface portion defining the recess, wherein the inner surface portion is opposite the conical outer surface portion and wherein the sealing element further includes at least one feature selected from the group of features consisting of;

the inner surface portion and the conical outer surface portion diverge from each other in the direction from the transverse wall towards the recess; and

the inner surface portion and the conical outer surface portion are formed by a first longitudinal wall portion with a radial thickness that increases in the direction from the transverse wall towards the recess.

4. The sealing element claim 1, further comprising:

a cylindrical outer surface portion having a constant diameter in the longitudinal direction;

wherein the sealing element includes at least one feature selected from a group of features consisting of;

the cylindrical outer surface portion is the outer surface of a second longitudinal wall portion, the second longitudinal wall portion comprising at least one feature selected from a group of features consisting of;

the second longitudinal wall portion is located transverse wall and the first longitudinal wall portion; and

the second longitudinal wall portion has a radial wall thickness that is constant in the direction from the transverse wall towards the recess.

5. The sealing element claim 1, further comprising:

a compression surface being spaced from the transverse wall, the compression surface comprising at least one feature selected from a group of features consisting of;

the compression surface is the outer surface of a third longitudinal wall portion of the sealing element;

the third longitudinal wall portion comprises a cutout extending in the longitudinal direction wherein the cutout is a longitudinal slit wherein the longitudinal slit has a sharp-edged end in a direction to the sealing face or wherein the longitudinal slit has one of a rectangular end and a rounded end

the third longitudinal wall portion comprises three or more cutouts and wherein the three or more cutouts spread or nonuniformly distributed over the circumference;

the compression surface has a conical shape with a diameter decreasing in a direction from the transverse wall towards the recess of the sealing element; and

the transverse wall forms a first end of the sealing element and the compression surface forms second end of the sealing element, the second end being opposite the first end.

6. The sealing element of claim 1, wherein the sealing element comprises one selected from the group consisting of polymer.

a polyether,

polyetheretherketone,

a polymer,

a polyether,

and polyetheretherketone.

7. The sealing element of claim 1, further comprising at least one feature selected from a group of features consisting of:

the sealing element is formed as a single piece;

the sealing element is a molded single piece;

the sealing element is injection molded as a single piece.

8. A connection assembly, comprising:

a coupling element;

a tubular element fluidically connectable or fluidically connected to the coupling element; and

a sealing element comprising;

a recess extending in the longitudinal direction, the recess being adapted for receiving the tubular element; and

a transverse wall defining an extent of the recess in the longitudinal direction, the transverse wall having a through hole,

wherein the connection assembly provides a connected state in which the tubular element is fluidically connected to the coupling element.

9. The connection assembly of claim 8, further comprising:

the coupling element having a recess for receiving the sealing element;

wherein the connection assembly comprises at least one feature selected from a group of features consisting of;

in the connected state the recess of the coupling element is arranged coaxially with the recess of the sealing element;

the coupling element comprises a through hole wherein in the connected state the through hole of the coupling element is fluidically coupled to the through hole of the transverse wall of the sealing element;

the diameter of the through hole of the coupling element is larger than the diameter of the through hole of the transverse wall of the sealing element;

the diameter of the through hole in the transverse wall of the sealing element is smaller than the inner diameter of the tubular element.

10. The connection assembly of claim 8,

wherein the sealing element comprises a conical outer surface portion, the conical outer surface portion having a diameter increasing in a direction from the transverse wall towards the recess;

wherein the sealing element comprises an inner surface portion defining the recess, wherein the inner surface portion is opposite the conical outer surface portion and wherein the sealing element further includes at least one feature selected from the group of features consisting of;

wherein the inner surface portion and the conical outer surface portion diverge from each other in the direction from the transverse wall towards the recess,

wherein the inner surface portion and the conical outer surface portion are formed by a first longitudinal wall portion with a radial thickness that increases in the direction from the transverse wall towards the recess;

wherein the recess of the coupling element comprises a conical inner surface portion having a diameter which increases in a direction pointing outwardly from recess of the coupling element through an opening which is defined by the recess and through which the sealing element is inserted; and

wherein in the connected state the conical inner surface portion of the coupling element and the conical outer surface portion of the sealing element at least partially overlap in longitudinal direction;

wherein the connection assembly further comprises at least one feature selected from a group of features consisting of;

wherein the conical inner surface portion of the coupling element has a first slope and the conical outer surface portion of the sealing element has a second slope, wherein the first slope and the second slope are different;

wherein the first slope is steeper with regard to the longitudinal direction than the second slope; and

wherein the coupling element and the sealing element are configured such that without longitudinal pressure on the sealing element only a contact portion of the conical outer surface portion of the sealing element contacts the conical inner surface portion of the coupling element, wherein the contact portion has a smaller area than the conical outer surface portion; and

wherein the coupling element and the sealing element are configured such that a contact line of the sealing element is facing the transverse wall of the sealing element.

11. The connection assembly of claim 8,

wherein the sealing element further comprises a cylindrical outer surface portion having a constant diameter in the longitudinal direction;

wherein the sealing element includes at least one feature selected from a group of features consisting of;

wherein the cylindrical outer surface portion is the outer surface of a second longitudinal wall portion, the second longitudinal wall portion comprising at least one feature selected from a group of features consisting of;

wherein the second longitudinal wall portion is located between the transverse wall and the first longitudinal wall portion; and

wherein the second longitudinal wall portion has a radial wail thickness that is constant in the direction from the transverse wall towards the recess; and

the recess of the coupling element comprises a cylindrical inner surface portion, wherein in the connected state the cylindrical inner surface portion of the coupling element and the cylindrical outer surface portion of the sealing element at least partially overlap in longitudinal direction;

wherein the sealing element is configured such that in the connected state the second longitudinal wall portion, which forms the cylindrical outer surface portion of the sealing element, is compressed in longitudinal direction so as to expand in radial direction and thereby reduce a space between the cylindrical inner surface portion of the coupling element and the cylindrical outer surface portion of the sealing element.

12. The connection assembly of claim 8,

wherein the sealing element comprises a compression surface being spaced from the transverse wall, the compression surface comprising at least one feature selected from a group of features consisting of:

the compression surface is the outer surface of a third longitudinal wall portion of the sealing element;

the third longitudinal wall portion comprises a cutout extending in the longitudinal direction wherein the cutout is a longitudinal slit wherein the longitudinal slit has a sharp-edged end in a direction to the sealing face or wherein the longitudinal slit has one of a rectangular end and a rounded end;

the third longitudinal wall portion comprises three or more cutouts and wherein the three or more cutouts are evenly spread or nonuniformly distributed over the circumference;

the compression surface has a conical shape with a diameter decreasing in a direction from the transverse wall towards the recess of the sealing element; and

the transverse wall forms a first end of the sealing element and the compression surface forms second end of the sealing element, the second end being opposite the first end; and

the connection assembly further comprising a pressing element for pressing against the compression surface, the pressing element comprising at least one feature selected from a group of features consisting of;

the pressing element has pressing surface, and

the pressing element is configured for pressing the sealing element into the recess of the coupling element;

wherein compression of the sealing element by movement of pressing element includes at least one feature selected from a group of features consisting of;

the transverse wall of the sealing element contacts the recess of the coupling element;

the conical outer surface portion of the sealing element at least partially contacts the conical inner surface portion of the coupling element;

the second longitudinal wall portion of the sealing element is compressed in longitudinal direction; and

the sealing element radially presses against the tubular element located in the recess of the sealing element.

13. The connection assembly of claim 8, further comprising at least one feature selected from a group of features consisting of:

the tubular element has a first hardness and the sealing element has a second hardness smaller than the first hardness;

the tubular element comprises silicon dioxide;

the tubular element comprises a glass;

the tubular element comprises a body and a layer covering the body, wherein the layer is a protective layer;

the tubular element comprises fused silica;

the tubular element comprises steel

the coupling element is a fitting;

the tubular element is a capillary;

the sealing element is configured for providing a sealed fluidic connection between the coupling element and the tubular element, wherein the fluidic connection is configured to withstand a pressure of at least 1000 bar.

14. A measuring device for performing a measurement on a fluidic sample, the measuring device comprising:

a fluidic device;

a connection assembly for coupling the tubular element for conducting the fluidic sample to the fluidic device;

the connection assembly comprising;

a coupling element;

a tubular element fluidically connectable or fluidically connected to the coupling element; and

a sealing element comprising;

a recess extending in the longitudinal direction, the recess being adapted for receiving the tubular element; and

a transverse wall defining an extent of the recess in the longitudinal direction, the transverse wall having a through hole,

wherein the connection assembly provides a connected state in which the tubular element is fluidically connected to the coupling element,

wherein the fluidic sample is a mobile phase and the measuring device is a fluid separation system for separating compounds of a sample fluid in the mobile phase, the fluid separation system comprising;

a mobile phase drive, configured to drive the mobile phase (378) through the fluid separation system,

wherein the fluidic device is a separation unit, configured for separating compounds of the sample fluid in the mobile phase.

15. A method for providing a fluidic connection between a coupling element and a tubular element, the method comprising:

providing a connection assembly comprising;

a coupling element;

a tubular element fluidically connectable or fluidically connected to the coupling element, and

a sealing element comprising;

a recess extending in the longitudinal direction, the recess being adapted for receiving the tubular element; and

a transverse wall defining an extent of the recess in the longitudinal direction, the transverse wall having a through hole,

wherein the connection assembly provides a connected state in which the tubular element is fluidically connected to the coupling element;

inserting the tubular element into the sealing element;

inserting the sealing element into the recess of the coupling element.

16. The method of claim 15,

wherein the sealing element comprises a compression surface being spaced from the transverse wall, the compression surface comprising at least one feature selected from a group of features consisting of:

the compression surface is the outer surface of a third longitudinal wall portion of the sealing element;

the third longitudinal wall portion comprises a cutout extending in the longitudinal direction wherein the cutout is a longitudinal slit wherein the longitudinal slit has a sharp-edged end in a direction to the sealing face or wherein the longitudinal slit has one of a rectangular end and a rounded end;

the third longitudinal wail portion comprises three or more cutouts and wherein the three or more cutouts are evenly spread or nonuniformly distributed over the circumference;

the compression surface has a conical shape with a diameter decreasing in a direction from the transverse wall towards the recess of the sealing element; and

the transverse wall forms a first end of the sealing element and the compression surface forms second end of the sealing element, the second end being opposite the first end; and

the connection assembly further comprising a pressing element for pressing against the compression surface, the pressing element comprising at least one feature selected from a group of features consisting of;

the pressing element has pressing surface, and

the pressing element is configured for pressing the sealing element into the recess of the coupling element;

wherein compression of the sealing element by movement of pressing element includes at least one feature selected from a group of features consisting of;

the transverse wall of the sealing element contacts the recess of the coupling element;

the conical outer surface portion of the sealing element at least partially contacts the conical inner surface portion of the coupling element;

the second longitudinal wall portion of the sealing element is compressed in longitudinal direction; and

the sealing element radially presses against the tubular element located in the recess of the sealing element, the method further comprising;

operating the pressing element so as to press the sealing element into the recess of the coupling element;

wherein the method further comprises at least one of feature selected from a group of features consisting of;

pressing the transverse wall of the sealing element in contact with the recess of the coupling element;

pressing at least part of the conical outer surface portion of the sealing element into contact with the conical inner surface portion of the coupling element;

longitudinally compressing the sealing element so as to longitudinally compress the second longitudinal wall portion of the sealing element in the longitudinal direction;

compressing the sealing element so as to radially press the sealing element against the tubular element located in the recess of the sealing element;

frictionally engaging the tubular element by the sealing element and moving together the sealing element and the tubular element deeper into the recess so as to compress the transverse wall between the tubular element and a bottom of the recess of the coupling element opposite the transverse wall.