METHOD FOR PRODUCING HOLLOW FIBER CARBON MEMBRANE
First Claim
1. A method for producing a hollow fiber carbon membrane using a hollow fiber carbon membrane-forming material by means of a dry method or dry-wet method comprising a spinning step, a drying step, an infusibilization step, and a carbonization step as basic steps;
- wherein in the infusibilization step, heat treatment is performed at least two times at different temperatures, with the second temperature being higher than the first temperature;
in the spinning step, spinning is performed using a water-soluble organic polyamine aqueous solution having a concentration of 10 to 30 wt. % as a core liquid.
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Abstract
Disclosed is a method for producing a hollow fiber carbon membrane using a hollow fiber carbon membrane-forming material by means of a dry method or dry-wet method comprising a spinning step, a drying step, an infusibilization step, and a carbonization step as basic steps; wherein in the infusibilization step, heat treatment is performed at least two times at different temperatures, with the second temperature being higher than the first temperature. It is preferable that the second heat treatment is performed directly after the first treatment is performed, without once cooling to room temperature. The obtained hollow fiber carbon membrane has improved permeability, without reducing its separation coefficient.
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Citations
13 Claims
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1. A method for producing a hollow fiber carbon membrane using a hollow fiber carbon membrane-forming material by means of a dry method or dry-wet method comprising a spinning step, a drying step, an infusibilization step, and a carbonization step as basic steps;
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wherein in the infusibilization step, heat treatment is performed at least two times at different temperatures, with the second temperature being higher than the first temperature; in the spinning step, spinning is performed using a water-soluble organic polyamine aqueous solution having a concentration of 10 to 30 wt. % as a core liquid. - View Dependent Claims (2, 3, 4, 6, 7, 8, 9, 10, 11, 12, 13)
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5. (canceled)
Specification