METHOD FOR OBTAINING HYDROCARBON SOLVENTS WITH BOILING POINT ABOVE 300 °C AND POUR POINT LOWER THAN OR EQUAL TO -25 °C
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Abstract
A method for producing hydrocarbon solvents having a sulfur content of less than 10 ppm, aromatic hydrocarbon content of less than 500 ppm, an initial boiling point higher than or equal to 300° C. and final boiling point lower than or equal to 500° C., for a fraction interval of a maximum of 100° C., and pour point lower than −25° C. according to the standard ASTM D5950, comprising of the following steps of:
- dewaxing of a hydrocarbon fraction having initial boiling point higher than 300° C. derived from the distillation of a gas oil fraction,
- hydrodearomatisation of all or part of the dewaxed effluent, in the presence of a catalyst comprising nickel on an alumina base, at a pressure ranging from 60 to 200 bar and a temperature ranging from 80° C. to 250° C.,
- recovery of the dewaxed and dearomatised fraction,
- distillation in fractions of the dewaxed and dearomatised fraction,
- recovery of at least one 300° C.+ fraction having pour point lower than −25° C., this fraction having a distillation interval lower than 100° C.
35 Citations
41 Claims
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1-23. -23. (canceled)
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24. A method for producing hydrocarbon solvents having a sulfur content of less than 10 ppm, aromatic hydrocarbon content of less than 500 ppm, an initial boiling point higher than or equal to 300°
- C. and final boiling point lower than or equal to 500°
C., as determined according to the standard ASTM D86, for a fraction interval of a maximum of 100°
C., and pour point lower than −
25°
C. according to the standard ASTM D5950, comprising the following steps of;dewaxing of a hydrocarbon fraction having initial boiling point higher than 300°
C. derived from the distillation of a gas oil fraction obtained by any crude oil refining process, and recovery of all or part of the dewaxed effluent,hydrodearomatisation of all or part of the dewaxed effluent, in the presence of a catalyst comprising nickel on an alumina base, at a pressure ranging from 60 to 200 bar and a temperature ranging from 80°
C. to 250°
C., and said dewaxed effluent being possibly previously desulphurised in advance if its sulfur content is greater than 15 ppm,recovery of the dewaxed fraction, possibly desulphurised, and dearomatised, distillation (DA1) in fractions of the said dewaxed and dearomatised fraction, and finally recovery of at least one 300°
C.+ fraction having pour point lower than −
25°
C. that is usable as solvent, this fraction having a distillation interval lower than 100°
C. - View Dependent Claims (25, 26, 27, 28, 29, 30, 31, 32, 33, 34, 35, 36, 37, 38, 39, 40, 41)
- C. and final boiling point lower than or equal to 500°
Specification