ROTARY EVAPORATOR HAVING A FASTENING DEVICE WITH CLAMPING ELEMENTS

• US 20170209805A1
• Filed: 07/14/2015
• Published: 07/27/2017
• Est. Priority Date: 07/22/2014
• Status: Active Grant

• Current Assignee: Hans Heidolph GmbH
• Original Assignee: Hans Heidolph GmbH
• Inventors: DIL, Roman
• Granted Patent: US 10,537,827 B2
• Time in Patent Office: Days
• CPC Class Codes: B01D 3/08 in rotating vessels; Atomisation on rotating discs B01D1/222 , B01D3/10 take precedence
• CPC Class Codes: B01D 3/085 using a rotary evaporator
• CPC Class Codes: B01D 3/12 Molecular distillation
• CPC Class Codes: F16L 37/122 using hooks tightened by a wedge section

Abstract

The invention relates to a rotary evaporator comprising a rotary drive and a fastening device attached to the rotary drive and having a receiving space for receiving an evaporator flask rotatable by the rotary drive, wherein the fastening device comprises a connector section, in particular a ring-shaped connector section, at the rotary drive side and a retainer element, in particular a ring-shaped retainer element, at the evaporator flask side that coupled to the connector section and that is rotatable relative to the connector section between a starting position and an end position. The fastening device comprises at least one clamping element that is moved, on the rotation of the retainer element relative to the connector section from the starting position into the end position, from a release position radially inwardly into a holding position in which the respective clamping element projects into the receiving space to hold a flange-shaped connection region of an evaporator flask received in the receiving space of the fastening device in a form-fitting and/or force-fitting manner and to secure it against a removal from the receiving space.

Claims

1. A rotary evaporator comprising a rotary drive and a fastening device attached to the rotary drive and having a receiving space for receiving an evaporator flask rotatable by the rotary drive, wherein the fastening device comprises a connector section at the rotary drive side and a retainer element at the evaporator flask side that is coupled to the connector section and that is rotatable relative to the connector section between a starting position and an end position,

wherein the fastening device comprises at least one clamping element that is moved, on the rotation of the retainer element relative to the connector section from the starting position into the end position, from a release position radially inwardly into a holding position in which the respective clamping element projects into the receiving space to hold a flange-shaped connection region of an evaporator flask received in the receiving space of the fastening device in a form-fitting and/or force-fitting manner and to secure it against a removal from the receiving space.

2. The rotary evaporator in accordance with claim 1,

wherein the respective clamping element is moved, on a rotation of the retainer element relative to the connector section from the starting position into the end position, radially inwardly and simultaneously axially toward the connector section.

3. The rotary evaporator in accordance with claim 1,

wherein the connector section is fastened to the rotary drive.

4. The rotary evaporator in accordance with claim 1,

wherein the retainer element is releasably couplable to the connector section.

5. The rotary evaporator in accordance with claim 1,

wherein the coupling of the retainer element to the connector section takes place free of a screw connection.

6. The rotary evaporator in accordance with claim 1,

wherein the retainer element can be placed onto the connector section into the starting position in one or more discrete rotational positions.

7. The rotary evaporator in accordance with claim 1,

wherein the connector section comprises a plurality of radially outwardly projecting first engagement elements and the retainer element comprises a plurality of radially inwardly projecting second engagement elements, with the first engagement elements and the second engagement elements meshingly engaging into one another in the starting position and engaging behind one another in a rotated position.

8. The rotary evaporator in accordance with claim 7,

wherein the first engagement elements and the second engagement elements are each arranged evenly distributed in the peripheral direction at the connector section and at the retainer element, respectively.

9. The rotary evaporator in accordance with claim 1,

wherein the respective clamping element is arranged between the connector section and the retainer element.

10. The rotary evaporator in accordance with claim 1,

wherein, on the rotation of the retainer element relative to the connector section from the starting position into the end position, the respective clamping element is pressed by the retainer element axially toward the connector section.

11. The rotary evaporator in accordance with claim 1,

further comprising means that convert a rotation of the retainer element relative to the connector section from the starting position into the end position into an axial movement of the retainer element relative to the connector section, with further means being provided that convert the axial movement of the retainer element into the radial movement of the respective clamping element.

12. The rotary evaporator in accordance with claim 11,

wherein the means comprise mutually corresponding sloping surfaces that are formed at the connector section, on the one hand, and at the retainer element, on the other hand.

13. The rotary evaporator in accordance with claim 11,

wherein the further means comprise the respective clamping element being chamfered at its radially outer edge facing the connector section and the connector section having a chamfer corresponding hereto, whereby the respective clamping element is moved, on the rotation of the retainer element relative to the connector section into the end position, radially inwardly and axially toward the connector section.

14. The rotary evaporator in accordance with claim 1,

wherein the respective clamping element is chamfered at its radially inner edge facing the connector section to cooperate with a chamfer corresponding hereto at the flange-shaped connection region of an evaporator flask received in the fastening device.

15. The rotary evaporator in accordance with claim 1,

wherein the respective clamping element is preloaded from its holding position into the release position.

16. The rotary evaporator in accordance with claim 15,

wherein a circlip is provided to preload the respective clamping element.

17. The rotary evaporator in accordance with claim 1,

wherein the respective clamping element is elongated and/or is of part-circle shape.

18. The rotary evaporator in accordance with claim 1,

wherein a plurality of clamping elements are arranged evenly distributed in the peripheral direction.

19. The rotary evaporator in accordance with claim 1,

wherein the respective clamping element cooperates with a respective first engagement element of the connector section.

20. The rotary evaporator in accordance with claim 1,

wherein the retainer element is provided with a tensioning lever for rotation, with an end of said tensioning lever being pivotably supported at an articulation point at the retainer element and being adjustable between an open position and a closed position in which the respective clamping element adopts the holding position.

21. The rotary evaporator in accordance with claim 20,

wherein the tensioning lever is coupled to the retainer element and to the connector section such that the rotation of the retainer element relative to the connector section from the starting position into the end position takes place in two stages, with in a first stage the retainer element being rotated with an open tensioning lever from the starting position by a first part distance into an abutment position for the tensioning lever, and with in a second stage the tensioning lever being closed in a second stage to rotate the retainer element from the abutment position by a second part distance into the end position.

22. The rotary evaporator in accordance with claim 21,

wherein the first part distance is longer than the second part distance.

23. The rotary evaporator in accordance with claim 21,

wherein the rotating back of the retainer element relative to the connector section from the end position into the starting position takes place in two stages, with the tensioning lever being opened to rotate the retainer element by the second part distance from the end position in a first stage and with in retainer element being rotated back into the starting position with an open tensioning lever in a second stage.

24. The rotary evaporator in accordance with claim 20,

wherein the longitudinal extent of the tensioning lever extends in the peripheral direction of the retainer element;

wherein the tensioning lever is of part-circle shape and/or is received in a radially outer recess of the retainer element in the closed position.

25. The rotary evaporator in accordance with claim 20,

wherein pivot range of the tensioning lever between the open position and the closed position amounts to no more than 120°

.

26. The rotary evaporator in accordance with claim 20,

wherein the tensioning lever acts as a toggle lever on closing to rotate the retainer element from the abutment position by a second part distance into the end position.

27. The rotary evaporator in accordance with claim 20,

further comprising a control arm having a first end and a second end, with the first end being pivotably supported at the connector section and with the second end beings in engagement via a guide element with a control cam, with the control cam being formed at the tensioning lever.

28. The rotary evaporator in accordance with claim 27,

wherein the first end of the control arm is pivotably supported at a tensioning element that is inserted into a correspondingly configured mount of the connector section that prevents a rotation of the tensioning element relative to the connector section.

29. The rotary evaporator in accordance with claim 28,

wherein the tensioning element inserted between two radially outwardly projecting engagement elements of the connector section.

30. The rotary evaporator in accordance with claim 27,

wherein the control cam has a first section and a second section adjoining it at an angle at a kink point, with the second section having an end point.

31. The rotary evaporator in accordance with claim 30,

wherein, in the closed position of the tensioning lever, the first section extends tangentially and/or, in the open position, extends radially to the retainer element;

and/or wherein the second section is angled away from the retainer element with respect to the first section in the closed position of the tensioning lever.

32. The rotary evaporator in accordance with claim 30,

wherein the guide element is at a starting point in the first section in the starting position of the retainer element and is traveled by a first part distance toward the end point on the rotation of the retainer element relative to the connector section;

and/or wherein the guide element remains at the end point on a rotation of the retainer element by a second part distance relative to the connector section.

33. The rotary evaporator in accordance with claim 30,

wherein the guide element is traveled by the second part distance to the kink point on a rotating back of the retainer element relative to the connector section;

and/or wherein the guide element is traveled by the first part distance to the starting point on a rotating back of the retainer element relative to the connector section.

34. The rotary evaporator in accordance with claim 27,

wherein the control arm is longitudinally adjustable.

35. The rotary evaporator in accordance with claim 34,

wherein a starting point of the guide element in the first section of the control cam is adjustable via the length of the control arm.

36. The rotary evaporator in accordance with claim 20,

wherein a latching device is provided to latch the tensioning lever to the retainer element in the closed position.

37. The rotary evaporator in accordance with claim 1,

wherein the radially inner edge of the retainer element remote from the connector section is provided with an outer edge protective ring and/or the radial inner edge of the connector section facing the retainer element is provided with an inner edge protective ring.

38. The rotary evaporator in accordance with claim 37,

wherein the radially inner edge of the outer edge protective ring remote from the connector section is chamfered;

and/or the radially inner edge of the inner edge protective ring facing the retainer element is chamfered.

39. The rotary evaporator in accordance with claim 37,

wherein the largest inner diameter of the chamfer of the inner edge protective ring is not smaller than the smallest inner diameter of the chamfer of the outer edge protective ring.

40. A fastening device comprising a receiving space for receiving a laboratory container, wherein the fastening device comprises a connector section and a retainer element that is coupled to the connector section and that is rotatable between a starting position and an end position relative to the connector section,

wherein the fastening device comprises at least one clamping element that is moved, on the rotation of the retainer element relative to the connector section from the starting position into the end position, from a release position radially inwardly into a holding position in which the respective clamping element projects into the receiving space to hold a flange-shaped connection region of a piece of laboratory equipment received in the receiving space of the fastening device in a form-fitting and/or force-fitting manner and to secure it against a removal from the receiving space.