GRAIN BOUNDARY ENGINEERING FOR ADDITIVE MANUFACTURING

• US 20180085830A1
• Filed: 09/28/2016
• Published: 03/29/2018
• Est. Priority Date: 09/28/2016
• Status: Active Grant

• Current Assignee: General Electric Company
• Original Assignee: General Electric Company
• Inventors: Lou, Xiaoyuan, Dolley, Evan Jarrett, Morra, Martin Matthew
• Granted Patent: US 10,639,719 B2
• Time in Patent Office: Days
• CPC Class Codes: B22F 10/28 Powder bed fusion, e.g. selective laser melting [SLM] or electron beam melting [EBM]
• CPC Class Codes: B22F 10/32 of the atmosphere, e.g. composition or pressure in a building chamber
• CPC Class Codes: B22F 10/36 of energy beam parameters
• CPC Class Codes: B22F 10/366 Scanning parameters, e.g. hatch distance or scanning strategy
• CPC Class Codes: B22F 2003/248 Thermal after-treatment
• CPC Class Codes: B22F 2998/10 Processes characterised by the sequence of their steps
• CPC Class Codes: B22F 3/24 After-treatment of workpieces or articles B22F3/1146 takes precedence
• CPC Class Codes: B33Y 10/00 Processes of additive manufacturing
• CPC Class Codes: B33Y 80/00 Products made by additive manufacturing
• CPC Class Codes: C21D 1/34 Methods of heating C21D1/06 takes precedence
• CPC Class Codes: C21D 2201/05 Grain orientation
• CPC Class Codes: Y02P 10/25 Process efficiency

Abstract

In one embodiment, a method of manufacturing a metal part using a laser or electron beam during a powder bed additive manufacturing process includes melting each of a number of layers of metal powder of the metal part with an effective amount of energy using the laser or electron beam to form the metal part such that at least one or more portions of the metal part have a critical amount of residual strain. The method also includes performing a heat treatment on the metal part that transforms the residual strain into substantially distributed coincidence site lattice (CSL) grain boundaries, low angle grain boundaries, or both in the metal part.

Claims

1. A metal part, comprising:

a material, wherein at least a portion of the material is formed by melting metal powder with a laser or electron beam during a powder bed additive manufacturing process, wherein the portion receives an effective amount of energy from the laser or electron beam during the powder bed additive manufacturing process to introduce an amount of residual strain, and wherein the portion is configured to substantially release the residual strain and transform into a grain boundary engineered material having substantially distributed coincidence site lattice (CSL) grain boundaries, low angle grain boundaries, or both upon heat treatment.

2. The metal part of claim 1, wherein the heat treatment comprises a time parameter and a temperature parameter that are based on at least the substantial amount of residual strain present in the material.

3. The metal part of claim 1, wherein the CSL grain boundaries comprise less than Σ

29 grain boundaries and the low angle grain boundaries comprise Σ

3 grain boundaries.

4. The metal part of claim 1, wherein the amount of residual strain comprises a residual strain of between approximately 5% and approximately 15%.

5. The metal part of claim 1, wherein the CSL grain boundaries and the low angle grain boundaries exhibit improved stress corrosion cracking resistance, hold time fatigue, or both.

6. The metal part of claim 1, wherein the effective amount of energy is provided by the laser by using at least a laser scan speed of between approximately 0.1 and approximately 5 meters per second, a laser output energy between 100 watts to 800 watts, or both.

7. The metal part of claim 1, wherein the effective amount of energy is provided by the laser or electron beam by controlling a scan speed of the laser or electron beam, an energy output of the laser or electron beam, a hatching space, a thickness of a deposited layer of metal powder, or some combination thereof.

8. The metal part of claim 7, wherein the scan speed of the laser is between 0.1 meters per second and 5 meters per second, the laser energy output is between 100 watts and 800 watts, the hatching space is between 30 micrometers and 500 micrometers, and the layer thickness is between 10 micrometers and 100 micrometers.

9. The metal part of claim 1, wherein at least another portion of the material comprises equiaxed grain boundaries.

10. The metal part of claim 1, wherein the metal part has a complex three-dimensional (3-D) geometry.

11. The metal part of claim 1, wherein the metal part comprises a crack growth rate in the range of 1×

10<sup>−

9</sup> millimeters per second to 1×

10<sup>−

7</sup> millimeters per second in oxygenated high temperature water.

12. A method of manufacturing a metal part using a laser or electron beam powder bed additive manufacturing process, comprising:

melting each of a plurality of layers of metal powder of the metal part with an effective amount of energy using a laser or electron beam to form the metal part such that at least one or more portions of the metal part have a critical amount of residual strain; and

performing a heat treatment on the metal part that transforms the residual strain into substantially distributed coincidence site lattice (CSL) grain boundaries, low angle grain boundaries, or both in the metal part.

13. The method of claim 12, wherein the heat treatment comprises a time parameter and a temperature parameter that are based on the amount of residual strain present in the metal part, a type of the metal powder, particle size of the metal powder, or some combination thereof

14. The method of claim 12, wherein the metal part comprises mix-mode cracking comprising intergranular cracking and transgranular cracking that results in a crack growth rate in the range of 1×

10<sup>−

9</sup> millimeters per second to 1×

10<sup>−

7</sup> millimeters per second in oxygenated high temperature water.

15. The method of claim 12, wherein the effective amount of energy is provided by the laser using parameters comprising a scan speed between 0.1 meters per second and 5 meters per second, an output energy between 100 watts and 800 watts, or some combination thereof.

16. The method of claim 12, wherein the parameters further comprise using a hatching space between 30 micrometers to 500 micrometers, using a layer thickness between 10 micrometers and 100 micrometers, or some combination thereof

17. A metal part, comprising:

a metal microstructure, wherein at least a portion of the metal microstructure comprises substantially distributed coincidence site lattice (CSL) grain boundaries, low angle grain boundaries, or both that improve hold time fatigue and resistance to stress corrosion cracking, wherein the metal microstructure is formed using a laser or electron beam powder bed additive manufacturing process that delivers an effective amount of energy to introduce an amount of residual strain, and wherein the metal part subsequently undergoes a heat treatment that converts the residual strain into the substantially distributed CSL grain boundaries, low angle grain boundaries, or both in the portion.

18. The metal part of claim 17, wherein the metal microstructure enables a crack growth rate in the range of 1×

10<sup>−

9</sup> millimeters per second to 1×

10<sup>−

7</sup> millimeters per second in oxygenated high temperature water.

19. The metal part of claim 17, wherein the metal part comprises a complex three-dimensional (3-D) geometry.

20. The metal part of claim 17, wherein parameters of the laser powder bed additive manufacturing process include a laser scan speed between 0.1 meters per second and 5 meters per second, a laser energy output between 100 watts and 800 watts, a hatching space between 30 micrometers and 500 micrometers, a layer thickness between 10 micrometers and 100 micrometers, or some combination thereof