THERMAL TREATMENT OF PANE ELEMENTS FOR VACUUM INSULATING GLASS UNITS

• US 20190062195A1
• Filed: 02/16/2018
• Published: 02/28/2019
• Est. Priority Date: 02/17/2017
• Status: Active Grant

• Current Assignee: VKR Holding A/S (Villum Fonden)
• Original Assignee: VKR Holding A/S (Villum Fonden)
• Inventors: Sonderkaer, Peter
• Granted Patent: US 10,640,412 B2
• Time in Patent Office: Days
• CPC Class Codes: C03B 2225/00 Transporting hot glass sheets during their manufacture
• CPC Class Codes: C03B 23/245 Hollow glass sheets
• CPC Class Codes: E06B 3/6612 Evacuated glazing units
• CPC Class Codes: E06B 3/66357 Soldered connections or the like
• CPC Class Codes: E06B 3/6733 by applying, e.g. extruding, a ribbon of hardenable material on or between the panes
• CPC Class Codes: E06B 3/67334 by soldering; Preparing the panes therefor
• CPC Class Codes: E06B 3/67365 Transporting or handling panes, spacer frames or units during assembly E06B3/67304 - E06B3/67339 take precedence
• CPC Class Codes: Y02A 30/249 Glazing, e.g. vacuum glazing
• CPC Class Codes: Y02B 80/22 Glazing, e.g. vaccum glazing

Abstract

A method for manufacturing a plurality of vacuum insulating glass (VIG) units, wherein the method comprises providing a plurality of first glass panes, applying a soldering material arranged for subsequent connection with a second glass pane to provide a seal between an outside of the VIG unit and an inside void of the VIG unit, moving the first glass panes comprising the soldering material into a treatment compartment, wherein the treatment compartment is pre-heated, drying the soldering material in a heating step by evaporating solvent, wherein the heating is forced convection heating, moving the first glass panes to a cooling compartment, cooling first glass panes and the soldering material thereon in a cooling step, wherein the cooling is by forced convection cooling, moving the first glass panes from the cooling compartment, and subsequently connecting the first glass panes to second glass panes using the dried soldering material.

Claims

1. A method for manufacturing a plurality of vacuum insulating glass (VIG) units,

wherein the method comprises the steps of:

providing a plurality of first glass panes,

applying a soldering material in paste form to a first surface along side edges of the first glass panes, wherein the soldering material is arranged for subsequent connection with a second glass pane to provide a seal between an outside of the VIG unit and an inside void of the VIG unit,

moving the first glass panes comprising the soldering material into a first thermal treatment compartment of a furnace arrangement, wherein the first thermal treatment compartment is pre-heated,

drying the soldering material on the first glass panes in a heating step by evaporating solvent from the soldering material in the first thermal treatment compartment, wherein the heating is forced convection heating,

moving the first glass panes from the first thermal treatment compartment to a cooling compartment of the furnace arrangement,

cooling first glass panes and the soldering material thereon in a cooling step in the cooling compartment, wherein the cooling is by forced convection cooling,

moving the first glass panes from the cooling compartment, and

subsequently connecting the first glass panes to second glass panes using the dried soldering material.

2. The method according to claim 1, wherein the forced convection heating and/or the forced convection cooling is provided to a second surface opposite to the first surface of each of the first glass panes using a plurality of nozzles in the first thermal treatment compartment and/or the cooling compartment directed towards the second surfaces.

3. The method according to claim 1, wherein the forced convection heating is at a temperature between 140°

C. and 240°

C.

4. The method according to claim 1, wherein a total treatment time for the heating step and the cooling step is between 4 and 15 minutes.

5. The method according to claim 1, wherein the heating step is provided in the first thermal treatment compartment, and wherein the cooling step is provided in the cooling compartment that is arranged after the first thermal treatment compartment.

6. The method according to claim 5, wherein the first thermal treatment compartment and the cooling compartment are separated by a heat insulating arrangement.

7. The method according to claim 1, wherein the soldering material and/or the first glass pane has a temperature of between 40°

C. and 100°

C. after cooling in the cooling step.

8. The method according to claim 1, wherein the heating step and/or cooling step is provided by a plurality of first nozzles directed towards a second surface opposite to the first surface of each of the first glass panes, and one or more second nozzles directed towards the first surfaces comprising the soldering material.

9. The method according to claim 1, wherein the heating step and/or the cooling step is provided by forced convection of a temperature controlled gas, by supplying a larger gas flow at a second surface opposite to the first surface of each of the first glass panes compared to a second gas flow provided simultaneously to the first surface of the first glass panes in the first thermal treatment compartment.

10. The method according to claim 1, further comprising conveying the first glass panes through the first thermal treatment compartment and the cooling compartment using a conveyer system,

wherein the first glass panes are transported through an inlet opening of the furnace arrangement to an outlet opening of the furnace arrangement.

11. The method according to claim 10, wherein a second surface of each of the first glass panes is supported on one or more conveyer elements of the conveyer system, and

wherein the heating step and/or the cooling step is provided by forced convection of a temperature controlled gas supplied to the second surface of each of the first glass panes between or through the one or more conveyer elements.

12. The method according to claim 1, further comprising supplying a gas during the heating step and/or the cooling step, wherein the gas is filtered air.

13. The method according to claim 1, wherein the first and second glass panes are tempered glass.

14. The method according to claim 1, wherein the method is provided in a substantially continuous manufacturing process comprising

a first manufacturing line for preparing the first glass panes, and

a second manufacturing line for preparing the second glass panes,

wherein the first manufacturing line provides the forced convection heating and cooling,

wherein the second manufacturing line is configured to prepare the second glass panes for connecting to the first glass panes after the heating step and the cooling step, and

wherein the first and second manufacturing lines are substantially parallel processes.

15. The method according to claim 14, wherein the second manufacturing line comprises a pillar placing process where a pillar placement arrangement system distributes and places a plurality of pillars on an upper surface of the second glass panes.

16. The method according to claim 1, wherein the soldering material on the first glass panes comprises

at least 50% by weight of glass frit, based on the total weight of the soldering material;

a binder material; and

a solvent,

wherein the soldering material is a paste.

17. The method according to claim 1, wherein said moving of the first glass panes from the first thermal treatment compartment to a cooling compartment of the furnace arrangement is provided by a conveyer system.

18. A method for manufacturing a plurality of vacuum insulating glass (VIG) units, wherein the method comprises the steps of:

providing a plurality of first glass panes;

applying a soldering material in paste form on a first surface of each first glass pane along side edges, wherein the soldering material is configured for subsequent connection with a second glass pane to provide a seal between the outside of the VIG unit and an inside void of the VIG unit where vacuum is to be provided,

moving the first glass panes comprising the soldering material into a thermal treatment compartment;

providing a thermal treatment to the soldering material to evaporate a solvent from the soldering material;

moving the first glass panes from the thermal treatment compartment; and

subsequently connecting the first glass panes to the second glass panes using the dried soldering material,

wherein a gas convection treatment process is provided during the thermal treatment step, wherein the gas convection treatment process comprises heat exchange between the first glass panes and the thermal treatment compartment by forced convection of a temperature controlled gas that is supplied to the first surface and/or a second surface of the first glass panes opposite to the first surface using a plurality of nozzles in the thermal treatment compartment directed towards the first and/or the second surfaces, and

wherein the temperature controlled gas supplied during the gas convection treatment process is purified air.

19. The method according to claim 18, further comprising filtering the temperature controlled gas with a filtering unit before it is directed to the first glass panes.

20. The method according to claim 18, wherein the forced convection of the temperature controlled gas by the plurality of nozzles is provided at an angle between 3°

and 80°

to the first and/or second pane surface(s).

21. The method according to claim 18, wherein the gas convection treatment process comprises a first thermal treatment step and a second thermal treatment step,

wherein the first thermal treatment step comprises a heating step where the soldering material at the first surface is dried by evaporating the solvent from the soldering material by forced convection heating using a convection heating system,

wherein the second thermal treatment step comprises a cooling step where forced convection cooling is provided by a convection cooling system to cool the soldering material and the first glass panes subsequent to the heating step.

22. The method according to claim 18, wherein the method is provided in a substantially continuous manufacturing process comprising

a first manufacturing line for preparing the first glass panes, and

a second manufacturing line for preparing the second glass panes,

wherein the first manufacturing line provides the gas convection treatment process,

wherein the second manufacturing line provides a pillar placing process where a pillar placement arrangement system distributes and places a plurality of pillars on an upper surface of the second glass panes, and

wherein the first and second manufacturing lines are substantially parallel processes.