PROCESS FOR PREPARING (9e, 11z)-9,11-HEXADECADIENAL
First Claim
1. A process for preparing (9E,11Z)-9,11-hexadecadienal of the following formula (4):
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Abstract
An efficient process for preparing (9E,11Z)-9,11-hexadecadienal of formula (4)
is provided. The process includes at least steps of: conducting a nucleophilic substitution reaction between an (8E,10Z)-8,10-pentadecadienyl magnesium halide derived from an (8E,10Z)-1-halo-8,10-pentadecadiene of (1):
and an orthoformate ester (2)
to thereby prepare a (9E, 11Z)-1,1-dialkoxy-9, 11-hexadecadiene (3):
and hydrolyzing the (9E, 11Z)-1,1-dialkoxy-9,11-hexadecadiene (3) to obtain (9E, 11Z)-9,11-hexadecadienal (4).
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Citations
2 Claims
- 1. A process for preparing (9E,11Z)-9,11-hexadecadienal of the following formula (4):
Specification