METHOD AND APPARATUS FOR IMPREGNATING THE SURFACE REGION OF AN ARTICLE

• US 20190329287A1
• Filed: 04/15/2019
• Published: 10/31/2019
• Est. Priority Date: 04/30/2018
• Status: Abandoned Application

• Current Assignee: Rolls-Royce PLC (Rolls-Royce Holdings Plc)
• Original Assignee: Rolls-Royce PLC (Rolls-Royce Holdings Plc)
• Inventors: CENDROWICZ, Aleksander M., WILSON, Paul J., BHATT, Akshay, RAJIV, Athira, NOHLERT, Per, BELL, David A.
• Application Number:
  US16/383,734
• Publication Number:
  US 20190329287A1
• Time in Patent Office: Days
• CPC Class Codes: B05D 1/18 performed by dipping
• CPC Class Codes: B05D 3/007 After-treatment
• CPC Class Codes: B22C 9/10 Cores; Manufacture or installation of cores breaker cores B22C9/084
• CPC Class Codes: B22C 9/12 Treating moulds or cores, e.g. drying, hardening
• CPC Class Codes: C04B 35/00 Shaped ceramic products characterised by their composition porous ceramic products C04B38/00; ceramic articles characterised by particular shape, see the relevant classes, e.g. linings for casting ladles, tundishes, cups or the like B22D41/02; ceramic substrates for microelectronic semi-conductors H01L23/15; Ceramics compositions containing free metal bonded to carbides, diamond, oxides, borides, nitrides, silicides, e.g. cermets, or other metal compounds, e.g. oxynitrides or sulfides other than as macroscopic reinforcing agents C22C; shaping of ceramics B28B; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products chemical preparation of powders of inorganic compounds C01; infiltration of sintered ceramic preforms with molten metal C04B41/51
• CPC Class Codes: C04B 38/00 Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof treating slag with gases or gas generating material C04B5/06 ; expanded graphite C04B35/536
• CPC Class Codes: C04B 41/009 characterised by the material treated
• CPC Class Codes: C04B 41/4523 applied from the molten state vitreous materials C04B41/5022; Thermal spraying, e.g. plasma spraying
• CPC Class Codes: C04B 41/46 with organic materials
• CPC Class Codes: C04B 41/82 with organic materials

Abstract

An article 6 made from a porous material, such as a ceramic material, is dipped into a liquid impregnating material 12, such as molten urea in a bath 14. After withdrawal from the bath 14, excess impregnating material 12 is removed from the article 6 by means of an air knife 22. The air knife 22 is directed obliquely into an enclosure 18, which is maintained at a temperature above the melting point of urea. The article is passed into the enclosure 18 through the flow from a further air knife 20 which creates a separation airflow separating the interior of the enclosure 18 from the ambient surroundings. The article is carried by a fixture 6 to be conveyed along the processing line on a conveyor 2.

Claims

1. A method of impregnating a surface region of an article made from a porous material, the method comprising the steps of:

i) immersing the article in a liquid impregnating material;

ii) withdrawing the article from the liquid impregnating material into a transfer region;

iii) transferring the article from the transfer region into a removal region separated from the transfer region by a separation gas flow; and

iv) displacing excess impregnating material (12) from the surface of the article by exposing the article to the separation flow and a flow of gas in the removal region,

wherein the separation gas flow is directed generally horizontally across an opening of the removal region; and

,

the flow of gas to remove excess impregnating material is directed obliquely with respect the separation gas flow.

2. The method as claimed in claim 1, wherein the liquid impregnating material is in a solid-state at ambient temperature.

3. The method as claimed in claim 1, wherein the gas in the separation flow and the flow of gas are discharged at a temperature higher than the melting point of the impregnating material.

4. The method as claimed in claim 1, wherein the impregnating material has a melting point that is higher than 130°

C.

5. The method as claimed in claim 1, wherein the gas in the separation flow and the flow of gas are discharged at a temperature higher than 150°

C.

6. The method as claimed in claim 1, in which the impregnating material is urea.

7. The method as claimed in claim 2, in which, between withdrawal of the article from the liquid impregnating material and exposure of the article to the separation gas flow and the flow of gas, at least some of the impregnated material solidifies, the temperature of the gas in the gas flow being sufficient to return the solidified impregnated material to the liquid state.

8. The method as claimed in claim 1, in which, in exposing the article to the separation gas flow and the flow of gas, the article is displaced across the separation gas flow and the flow of gas.

9. The method as claimed in claim 1, in which the article is conveyed from the transfer region to the removal region.

10. The method as claimed in claim 1, in which the removal region is a higher temperature, in use, than the transfer region.

11. The method as claimed in claim 1, in which the separation gas flow and the flow of gas are provided by an air knife.

12. The method as claimed in claim 1, in which the article is a ceramic article.

13. The method as claimed in claim 12, in which the article is a ceramic core for use in an investment casting process.

15. An apparatus for carrying out the method as claimed in claim 1, the apparatus comprising:

i) a bath of liquid impregnating material;

ii) an excess impregnating material removal station provided with a first blower generating the separation gas flow and a second blower generating the flow of gas;

iii) a conveyor for conveying the article from the bath of liquid impregnating material to the excess impregnating material removal station and into the path of the separation gas flow and the flow of gas respectively.

16. The apparatus as claimed in claim 15, wherein the excess impregnating material removal station comprises an enclosure comprising an opening permitting passage of the article between the transfer region and the removal region.

17. The apparatus as claimed in claim 16, wherein the first blower is positioned at the opening to discharge the separation gas flow generally horizontally across the opening to separate the transfer region from the removal region.

18. The apparatus as claimed in claim 17, wherein the second blower is positioned within the enclosure to discharge the flow of gas obliquely with respect the separation gas flow.

19. The apparatus as claimed in claim 16, wherein a partition extends across the opening to separate the transfer region from the removal region.

20. The apparatus as claimed in claim 19, wherein the partition is provided with an aperture permitting passage of the article between the transfer region and the removal region.

14. A method of impregnating a surface region of an article made from a porous ceramic material with urea, the method comprising the steps of:

i) immersing the article in molten urea;

ii) withdrawing the article from the molten urea; and

iii) displacing excess urea from the surface of the article by exposing the article to a separation gas flow and a flow of gas within a removal region, at a temperature higher than the melting point of urea,

wherein the separation gas flow is directed generally horizontally across an opening of a removal region; and

,

the flow of gas to remove excess urea is directed obliquely with respect the separation gas flow.