Method and apparatus for inspecting liquids in transparent containers

• US 3,966,332 A
• Filed: 09/12/1974
• Issued: 06/29/1976
• Est. Priority Date: 09/12/1974
• Status: Expired due to Term

• Current Assignee: Schering Corporation (Merck & Co., Inc.)
• Original Assignee: Schering Corporation (Merck & Co., Inc.)
• Inventors: Knapp, Julius Z., Zeiss, John C.
• Primary Examiner(s): McGraw, Vincent P.
• Application Number:
  US05/505,431
• Time in Patent Office: 656 Days
• Field of Search: 356/196, 356/197, 356/198, 356/239, 356/240, 250/227, 250/222 PC, 250/223 B, 209/111.7
• US Class Current: 356/427
• CPC Class Codes: G01N 2033/0081 containers; packages; bottles
• CPC Class Codes: G01N 21/9009 Non-optical constructional details affecting optical inspection, e.g. cleaning mechanisms for optical parts, vibration reduction
• CPC Class Codes: G01N 21/9027 in containers after filling

Abstract

A method and apparatus for automatically inspecting liquid filled containers for particulate contaminants in relative size. The method comprising the steps of illuminating the liquid with a constant intensity light source, dissecting the image of the entire illuminated liquid volume, including the meniscus, with fiber optic bundles and monitoring the fiber optic bundles with an array of constant sensitivity photo sensors. Each photo sensor continually translates the illumination value of an assigned and separate cross sectional unit area of the vial image into a voltage signal and monitors each signal for a signal change indicative of particulate movement. The interfering output signal due to the meniscus decay is corrected, and the accept/reject decision is based upon a composite signal representative of all the differentiated signals received from the array of photo sensors.

Claims

1. A method for inspecting a liquid-filled transparent container, that may have a multiplicity of specular reflections on or in itself, to detect foreign particles in the liquid, said method comprising the steps of:

a. placing the article at an inspection station,

b. rotating said liquid about an axis while holding said container stationary,

c. illuminating said article,

d. dissecting the article image into a plurality of columns which extend from the bottom of the container through the top of the liquid meniscus,

e. monitoring each of said columns with separate sensing means for changes in illumination,

f. electronically translating said changes in illumination into voltage signals,

g. forming a composite signal of said voltage signals,

h. comparing said composite signal to a standard reference signal and based thereon accepting or rejecting said article for particulate contamination;

whereby the image of particulate matter which moves past a column with a saturated sensing means will be detected as it passes through a column with an unsaturated sensing means.

2. A method as in claim 1 wherein said step of dissecting said article image is accomplished by means of a plurality of fiber optic bundles.

3. A method as in claim 2 wherein said step of monitoring each of said columns is accomplished by monitoring the change in illumination of each of said fiber optic bundles by means of a constant sensitivity photo sensor.

4. A method as in claim 1 wherein said columns are spaced from one another and parallel to said axis of rotation.

5. A method as in claim 1 wherein each of said columns is further dissected into a plurality of unit areas wherein the sub-meniscus volume of the liquid is monitored by the unit areas at one end of said columns and the meniscus volume image is monitored by the remainder of said unit areas.

6. A system for inspecting a liquid filled container for particulate contamination comprising:

a. a source of radiation directed at said liquid filled container,

b. means to rotate said liquid about an axis while said container is held stationary at an inspection station,

c. means to dissect the article image into a plurality of columns which extend from the bottom of the container through the top of the liquid meniscus,

d. sensing means to separately monitor each of said columns to detect changes in illumination,

e. means to translate said changes in illumination into voltage signals,

f. means to form a composite signal of all of said voltage signals.

g. means to accept or reject said liquid filled container based upon a comparison of said composite signal to a standard reference signal.

7. A system as in claim 6 wherein said dissection means dissects the image of said container into a plurality of columns spaced from one another and aligned parallel to said axis

8. A system as in claim 6 wherein said monitoring means is a constant sensitivity photo sensor means.

9. A system as in claim 8 further comprising a means to differentiate the voltage signals from said photo sensor means so that only signal changes will be transmitted therefrom.

10. A system as in claim 6 wherein said source of radiation is a light source of constant intensity.

11. A system as in claim 6 wherein said dissection means is a fiber optic bundle means and said monitoring means is a constant sensitivity photo sensor.

12. A system as in claim 11 wherein said source of radiation comprises a light means for directing at least two light beams at said liquid filled container along light paths angularly disposed to the fiber optic bundle viewing axis passing through said container so that said light paths intersect in said container and illuminate substantially all of said liquid and form an angular shadow zone at said fiber optic bundle.

31. A method as in claim 11 wherein said article is rotated below the speed that will cause cavitation and bubbling of the liquid.

13. A method for inspecting the meniscus of a rotating liquid in a transparent stationary container for particulate contamination comprising the steps of:

a. illuminating said meniscus,

b. monitoring said meniscus at two portions in which the voltage signals generated by the meniscus decay would be substantially similar for changes in illumination due to moving particulate matter and meniscus decay,

c. electronically translating each of said changes in illumination into a voltage signal,

d. substantially eliminating the voltage signals due to the meniscus decay by electronically subtracting the voltage signals originating in each of said two portions,

e. forming a composite signal of all of said moving particulate matter voltage signals,

f. comparing said composite signal to a standard reference signal and based thereon accepting or rejecting said liquid filled container for particulate contamination.

14. A method for inspecting a liquid filled transparent container for foreign particles in the liquid, said method comprising the steps of:

a. placing the article at an inspection station,

b. rotating said liquid about an axis below the speed that will cause cavitation and bubbling of the liquid while holding said container stationary,

c. illuminating said article,

d. dissecting said rotating liquid volume into a meniscus volume image and a sub-meniscus volume image,

e. monitoring said sub-meniscus volume image for changes in illumination which are indicative of moving particulate matter,

f. monitoring said meniscus volume image at two portions, in which the voltage signals generated by the meniscus decay would be substantially similar, for changes in illumination which are indicative of moving particulate matter and the meniscus decay of the rotating liquid,

g. electronically translating each of said changes in illumination into voltage signals,

h. substantially eliminating the voltage signals due to the meniscus decay by electronically subtracting the voltage signals originating in each of said two portions,

i. forming a composite signal of all of the moving particulate matter signals from said sub-meniscus volume and said meniscus volume,

j. comparing said composite signal to a standard reference signal and based thereon accepting or rejecting said liquid filled container for particulate contamination.

15. A method as in claim 14 wherein said sub-meniscus volume image is monitored from a first time immediately after the rotation of said container is stopped, and said meniscus volume image is monitored from a second time subsequent to said first time.

16. A method as in claim 14 wherein said two meniscus image portions are the two meniscus image edge portions and said meniscus image is further separately monitored at a center portion located between said two edge portions.

17. A method as in claim 16 wherein said sub-meniscus volume image is monitored from a first time immediately after the rotation of said container is stopped, said meniscus center portion image is monitored from a second time subsequent to said first time and said meniscus edge portion images are monitored from a third time subsequent to said second time.

18. A method as in claim 14 wherein said rotating liquid volume image is dissected into a plurality of columns each of which extend from the bottom of the rotating liquid image through the meniscus image of the rotating liquid, each of said columns being further dissected into a plurality of unit areas, wherein said sub-meniscus volume image is monitored by the unit areas at one end of said columns and the meniscus volume image is monitored by the remainder of said unit areas.

19. A method as in claim 18 wherein said unit areas are rectangular.

20. A method as in claim 18 wherein said meniscus volume image and said sub-meniscus volume image monitoring means comprises a plurality of fiber optic bundles, each of which are operatively connected to one of said unit areas.

21. A method as in claim 20 wherein said meniscus volume image and said sub-meniscus volume image monitoring means further comprises a plurality of constant sensitivity photo sensors, each of which are operatively connected to one of said fiber optic bundles.

22. A method as in claim 14 wherein said composite signal comprises a composite of the magnitude of all of said moving particulate matter voltage signals.

23. A method as in claim 14 wherein said composite signal comprises the integral of all of said moving particulate matter voltage signals.

24. A method as in claim 14 wherein said composite signal comprises any moving particulate matter signal detected over a certain predetermined value.

25. A system for inspecting a liquid filled container for particulate contamination comprising:

a. a source of radiation directed at said liquid filled container,

b. means to rotate said liquid about an axis while said container is held stationary at an inspection station,

c. means to dissect the image of said rotating liquid into a meniscus volume image and a sub-meniscus volume image,

d. means to monitor said sub-meniscus volume image for changes in illumination due to moving particulate matter,

e. means to monitor said meniscus volume image at two portions, in which the voltage signals generated by the meniscus decay would be substantially similar, for changes in illumination due to moving particulate matter and the meniscus decay of the rotating liquid,

f. means to electronically translate said changes in illumination into voltage signals,

g. means to substantially eliminate the voltage signals due to the meniscus decay by electronically subtracting the voltage signals originating in each of said two portions,

h. means to form a composite voltage signal of all of said moving particulate matter voltage signals,

i. means to compare said composite signal to a standard reference signal, and means to accept or reject said container based thereon.

26. A system as in claim 25 wherein said means for monitoring said meniscus and said sub-meniscus volume images comprise a plurality of constant sensitivity photo sensors.

27. A system as in claim 25 wherein a fiber optic bundle means is used as the means to dissect the image of the rotating liquid.

28. A system for inspecting in relative size particulate matter in a liquid comprising:

a. a light source,

b. means to maintain said light source at a constant intensity,

c. means to rotate said liquid about an axis while said container is held stationary at an inspection station,

d. sensing means to monitor only changes in the illumination value of selected portions of said liquid filled container and to translate said changes in illumination into voltage signals,

e. means to form a composite signal of all of said voltage signals,

f. means to accept or reject said liquid filled container based upon a comparison of said composite signal to a standard reference signal,

whereby the intensity of the illumination value reflected by particles of constant reflectivity are always proportionate to the cross sectional area of the particles viewed.

29. A system as in claim 28 wherein said light source is a lamp and said means of part b comprises:

a means for sensing the illumination intensity of said lamp, and a servo amplifier means to control the current to said lamp based on a comparison of said sensed intensity to a stored criterion.

30. A method for inspecting illuminated articles wherein each of said articles comprise a liquid-filled transparent container, that may have a multiplicity of specular reflections on or in itself, which liquid is to be inspected for the presence of foreign particles, said method comprising the steps of:

a. placing the article at an inspection station having associated article illuminating means,

b. rotating said article about an axis to cause any of said foreign particles to rotate in planes substantially parallel to said axis of rotation,

c. while the illuminated liquid and any particles therein continue to swirl, dissecting the article image into a plurality of columns each of which intersect all of said planes at more than one point,

d. continuously monitoring with separate sensing means each of said columns to detect changes in illumination,

e. electronically translating said changes in illumination into voltage signals,

f. forming a composite signal of said voltage signals,

g. comparing said composite signal to a standard reference signal and based thereon accepting or rejecting said article for particulate contamination;

whereby the image of particulate matter which moves past a column with a saturated sensing means will be detected as it passes through a column with an unsaturated sensing means.

32. A method as in claim 30 wherein said columns are spaced from one another and parallel to said axis of rotation.

33. A method as in claim 30 wherein said columns extend from the bottom of the container through the top of the liquid meniscus.

34. A method for inspecting a sub-meniscus volume of a rotating liquid within a stationary transparent container to detect particulate contamination, said method comprising the steps of:

a. placing the article at an inspection station,

b. rotating said liquid about an axis while holding said container stationary,

c. illuminating said article,

d. dissecting said sub-meniscus volume image into a plurality of columns each of which extend from the bottom of the container through the top of said sub-meniscus volume,

e. continuously monitoring with separate sensing means each of said columns to detect changes in illumination,

f. electronically translating said changes in illumination into voltage signals,

g. forming a composite signal of said voltage signals,

h. comparing said composite signal to a standard reference signal and based thereon accepting or rejecting said article for particulate contamination;

whereby the image of particulate matter which moves past a column with a saturated sensing means will be detected as it passes through a column with an unsaturated sensing means.

35. A method as in claim 34 wherein said columns are spaced from one another and parallel to said axis of rotation.

36. A method as in claim 34 wherein said columns extend from the bottom of the container to a point just below the maximum meniscus displacement.

37. A method as in claim 34 wherein each of said columns is further dissected into a plurality of unit areas.