Method of reconstituting mica

• US 3,966,862 A
• Filed: 09/27/1974
• Issued: 06/29/1976
• Est. Priority Date: 09/27/1974
• Status: Expired due to Term

• Current Assignee: Franklin C. Farnam
• Original Assignee: Franklin C. Farnam
• Inventors: Farnam, Franklin C.
• Primary Examiner(s): Silbaugh, Jan H.
• Assistant Examiner(s): Parrish, John
• Application Number:
  US05/509,910
• Time in Patent Office: 641 Days
• Field of Search: 264/110, 264/332, 264/63, 264/125, 241/4
• US Class Current: 264/110
• CPC Class Codes: B29B 17/0026 by agglomeration or compacting
• CPC Class Codes: C04B 14/20 Mica; Vermiculite mechanical splitting B28D
• CPC Class Codes: C04B 18/04 Waste materials; Refuse
• CPC Class Codes: C04B 26/18 Polyesters; Polycarbonates
• CPC Class Codes: C04B 40/00 Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability active ingredients C04B22/00 - C04B24/00; hardening of a well-defined composition C04B26/00 - C04B28/00; making porous, cellular or lightening C04B38/00; mechanical aspects B28, e.g. conditioning the materials prior to shaping B28B17/02
• CPC Class Codes: C08J 11/06 without chemical reactions
• CPC Class Codes: C08J 2367/02 Polyesters derived from dicarboxylic acids and dihydroxy compounds; C08J2367/06 takes precedence
• CPC Class Codes: Y02W 30/62 Plastics recycling; Rubber recycling
• CPC Class Codes: Y02W 30/91 Use of waste materials as fillers for mortars or concrete

Abstract

A method of making reconstituted mica sheet in which dry ground mica is blended together with dry ground thermoplastic polyester to produce a dry powder mixture having no more than about 90% mica by weight of mixture, the dry powder mixture is formed into a layer, and the layer of dry powder is subjected to heat and pressure for softening the polyester and bonding the mica into sheet form. The mica used preferably is scrap mica and the polyester used preferably is scrap polyethylene terephthlate, ground to have particle size distributions as set forth in detail hereinafter.

Claims

1. In a method of making reconstituted mica sheet including the steps of blending mica and polyester, forming the mixture into a layer, and subjecting the layer to heat and pressure for bonding the layer into sheet form, the improvement comprising providing dry ground mica having a particle size in the range of from about 200 mesh to about 14 mesh;

providing ground thermoplastic polyester having a particle size of less than about 60 mesh;

proportioning the mixture to have from about 90 to about 50% mica by weight of the mixture;

forming the layer to have a thickness in the range of from about 1/8 inch to about 3/4 inch;

bonding the layer into a sheet having a thickness in the range of from about 1/64 inch to about 3/34 inch; and

maintaining the ground mica and ground polyester free from water during the steps of blending while producing the mixture, forming the layer and subjecting the layer to heat and pressure.

2. A method according to claim 1 comprising sifting the mixture onto a substrate and temporarily supporting the layer on the substrate during softening of the polyester and bonding of the mica into sheet form.

3. A method according to claim 1 wherein the step of providing ground polyester further comprises grinding scrap polyethylene terephthlate.

4. A method according to claim 1 wherein the subjecting of the layer to heat and pressure comprises heating the layer to a temperature in the range of from about 400°

to about 500°

F. and pressing the layer with a force in the range of from about 300 psi to about 1,000 psi.

5. A method according to claim 1 wherein the subjecting of the layer to heat and pressure further comprises simultaneously heating and compressing the layer.

6. A method according to claim 1 wherein the proportioning of the mixture comprises producing a mixture having about 75% mica by weight of mixture and about 25% polyethylene terephthlate by weight of mixture.

7. In a method of making reconstituted mica sheet including the steps of blending mica and polyester together while producing a mixture of mica and polyester, forming the mixture into a layer, and subjecting the layer to heat and pressure for bonding the layer into sheet form, the improvement comprising providing dry ground mica having a particle size in the range of from about 200 mesh to about 14 mesh;

providing ground polymerized polyethylene terephthlate having a particle size of less than about 60 mesh;

proportioning the mixture to consist of about 75% mica and about 25% polyethylene terephthlate by weight of mixture;

forming the layer to have a thickness in the range of from about 1/8 inch to about 3/4 inch;

bonding the layer into a sheet having a thickness in the range of from about 1/64 inch to about 3/34 inch; and

maintaining the mica and polyethylene terephthlate free from water during the steps of blending while producing the mixture, forming the layer and subjecting the layer to heat and pressure.