Process for impregnating wood

• US 3,967,011 A
• Filed: 06/25/1973
• Issued: 06/29/1976
• Est. Priority Date: 05/13/1968
• Status: Expired due to Term

• Current Assignee: The Dow Chemical Company (Dow, Inc.)
• Original Assignee: The Dow Chemical Company (Dow, Inc.)
• Inventors: Dunn, James L. Jr., Liddell, Harold G.
• Primary Examiner(s): Pianalto, Bernard D.
• Application Number:
  US05/372,875
• Time in Patent Office: 1,100 Days
• Field of Search: 117/147, 117/116, 117/57, 117/59, 117/149, 21/66, 21/7, 107/102 R, 107/102 A, 427/377, 427/397, 427/440, 427/345
• US Class Current: 427/345
• CPC Class Codes: B27K 3/0278 involving an additional treatment during or after impregnation
• CPC Class Codes: B27K 3/08 Impregnating by pressure , e.g. vacuum impregnation
• CPC Class Codes: B27K 3/34 Organic impregnating agents polymers B27K3/15
• CPC Class Codes: B27K 5/001 Heating

Abstract

An improved method of impregnating wood with a preservative is achieved by using halogenated solvents as carriers for the preservative or other wood treating chemicals and removing the carrier from the treated wood by treatment with steam. Benefits derived from this process include fewer steps, substantially complete removal of solvent, and the production of a natural appearing wood product having a surface suitable for painting.

Claims

1. A substantially non-polluting wood treating process for the impregnation of wood with preservatives to obtain substantially uncolored, natural appearing wood which consists ofcontacting, in a pressure vessel, wood with a solution of a wood preservative dissolved or suspended in a liquid halogenated hydrocarbon solvent at a pressure of from atmospheric pressure up to about 150 psig for a period of time sufficient to incorporate an amount of preservative into the wood and penetrate preservative to a depth into the wood to provide the desired protection, said solvent being non-flammable by Tag Closed Cup;

having a specific gravity greater than 1.1, a heat of vaporization less than 150 BTU/No. (78.6 cal/gm) and immiscible with water;

2. removing excess solution from contact with the impregnated wood and

3. heating the wood under ambient pressure by contacting said wood with a flow of steam for a time sufficient to substantially remove the chlorinated hydrocarbon solvent therefrom, said steam being at from its atmospheric boiling point to its boiling point at about 30 psig;

withdrawing the vapors from the pressure vessel and

4. condensing the vapors;

3. A process according to claim 1 wherein the wood preservative solution additionally contains up to about 5 weight percent of a polyether as an antiblooming agent.

5. The process of claim 1 wherein the preservative concentration in the solvent is from about 4.5 to about 5.5 weight percent and the solvent is methylene chloride.

6. The process of claim 1 wherein the preservative is pentachlorophenol.

7. The process of claim 1 wherein the pressure is from about 40 to about 150 psig.

2. separating the solvent from the water condensate;

6. recycling the condensate water to the steam treatment for generation of steam, recycling the solvent for reuse in preparing the solution of wood preservative for the impregnation step.

4. The process of claim 2 wherein the polyether is a polypropylene glycol having an average molecular weight of between about 400 and 4000.