Method of repairing leaky hollow fiber permeability separatory devices

• US 3,968,192 A
• Filed: 04/19/1974
• Issued: 07/06/1976
• Est. Priority Date: 04/19/1974
• Status: Expired due to Term

• Current Assignee: The Dow Chemical Company (Dow, Inc.)
• Original Assignee: The Dow Chemical Company (Dow, Inc.)
• Inventors: Hoffman, Sargent Glenn III, Mather, Frank Watkins III
• Primary Examiner(s): White, Robert F.
• Assistant Examiner(s): Pavelko, Thomas P.
• Application Number:
  US05/462,457
• Time in Patent Office: 809 Days
• Field of Search: 264/36, 264/267, 264/320, 264/322, 165/11, 165/78, 138/97, 138/98, 156/94
• US Class Current: 264/36.15
• CPC Class Codes: B01D 65/106 Repairing membrane apparatus or modules

Abstract

There is disclosed a method of repairing leaky permeability separatory devices, said devices comprising a membrane in the form of a multiplicity of hollow fibers having end portions potted in one or more resinous tubesheet bodies and terminating in an accessible surface of said tubesheet. According to the present invention, each surface opening communicating with a given leak in a tubesheet or fiber is selectively plugged by applying heat and pressure to the tubesheet and fiber material in the immediate vicinity of each such opening. The openings are first located by sealing the tubesheet/fiber assembly in an appropriately adapted jacket and applying pressure to a fluid in the portion of the jacket volume exterior to the fibers.

Claims

1. A process for remedying leaks in a tubesheet/hollow fiber assembly comprising a plurality of hollow fiber lengths having end portions potted in and extending through a solid body of fusible resin and opening upon an accessible surface of said body, said process comprisingdisposing said assembly within an opening in a casing, said casing being adapted for connection to a fluid pressure source, in such manner that the accessible tubesheet surface is exposed,effecting a seal between the periphery of said tubesheet and the portion of said casing adjacent said opening,

3. The process of claim 1 in which said rod means is a rigid, fine-pointed heat conductor and is employed to supply heat and pressure simultaneously to said assembly materials.

4. The process of claim 1 in which the location of a leak-connected opening is determined and then marked by insertion into the resin body of a readily removed, needle-like article.

5. The process of claim 3 in which the rod means is an electric soldering iron.

6. The process of claim 1 in which the potted fiber ends make an angle of 45°

or less with said accessible surface.

2. supplying a fluid under pressure to the volume within said casing exterior to said fiber lengths, thereby pressurizing said volume,locating an opening in said accessible surface from which egress of said fluid occurs,heating the assembly materials in the immediate vicinity of the opening in said accessible surface and applying pressure to the heated materials with rod means until said opening is sealed.