Device for taking samples of molten metals flowing in pipes

• US 3,968,695 A
• Filed: 08/28/1975
• Issued: 07/13/1976
• Est. Priority Date: 09/11/1974
• Status: Expired due to Term

• Current Assignee: Interatom Internationale Atomreaktorbau GmbH
• Original Assignee: Interatom Internationale Atomreaktorbau GmbH
• Inventors: Cremer, Dieter, Weiss, Hansjakob, Kranz, Eginhard
• Primary Examiner(s): Swisher, S. Clement
• Application Number:
  US05/608,702
• Time in Patent Office: 320 Days
• Field of Search: 73/422 R, 73/DIG. 9
• US Class Current: 73/863.11
• CPC Class Codes: G01N 1/10 in the liquid or fluent state burettes, pipettes B01L3/02; sampling of ground water E02D1/06; metering by volume of fluids or fluent solid material G01F11/00, G01F13/00
• CPC Class Codes: G01N 1/18 with provision for splitting samples into portions G01N1/12, G01N1/14 take precedence; fraction-collection apparatus for chromatography B01D15/08
• CPC Class Codes: G01N 2001/1037 from an enclosure (hazardous waste, radioactive)
• CPC Class Codes: G01N 2001/2064 using a by-pass loop
• CPC Class Codes: G01N 2033/0093 radioactive materials
• CPC Class Codes: G01N 33/2025 Gaseous constituents
• CPC Class Codes: G01N 33/205 in liquid state, e.g. molten metals
• CPC Class Codes: G21C 17/025 for monitoring liquid metal coolants molten metal sampling in general G01N1/125
• CPC Class Codes: Y02E 30/30 Nuclear fission reactors

Abstract

A device is described for taking samples from a liquid-metal-carrying pipe loop, in which the flowing liquid metal is a hot molten metal and may also be radioactive, e.g., metal in a main coolant loop of a sodium-cooled nuclear reactor. The device is suited for in-line as well as out-line operation and uses the conventional crucibles. The crucibles are arranged in a vertical housing in a circle around a vertical feed line for the liquid metal and extending upwardly into the housing. The liquid metal flowing into the device from the feed line'"'"'s upper end, is deflected downwardly into the crucibles by a downwardly facing concave baffle surface which is concentric with the feed line. The crucibles can be taken out of the device, hanging on an insert forming a closure for the housing'"'"'s top and that can be unscrewed and lifted, to obtain the crucibles. Improved arrangements of the thermocouples used for measuring the temperature of the liquid metal, and of the electric system required for heat the device are disclosed.

Claims

1. A device for obtaining samples of liquid metal and comprising a housing having an inlet and an outlet for the liquid metal, and containing crucibles having open tops and which can be filled while in the housing with the liquid metal and subsequently removed from the housing;

wherein the improvement comprises positioning means in said housing for positioning said crucibles so they form a horizontal ring of crucibles, said inlet comprising a vertical feed pipe extending upwardly in said housing within said ring of crucibles and having an open top for the upward ejection of the liquid metal at a level above the open tops of the ring of crucibles, and baffle means for forming a baffle surface spaced above the feed pipe'"'"'s open top and the open tops of said ring of crucibles, said baffle surface being contoured to deflect liquid metal ejected upwardly from the feed pipe'"'"'s open top, downwardly into the open tops of said ring of crucibles.

2. The device of claim 1 in which said housing has an open top and an upwardly removable insert normally closing the housing'"'"'s open top, and means for connecting said baffle and said positioning means to said insert so that upward removal of the insert lifts said ring of crucibles from said housing.

3. The device of claim 1 in which said baffle surface is in the form of a downwardly facing annular concave surface having a periphery forming an annular run-off edge for liquid metal deflected downwardly into the open tops of said ring of crucibles.

4. The device of claim 3 in which the open tops of said ring of crucibles form an annular zone having radially inner and outer limits and said run-off edge extends over one of said limits.

5. The device of claim 1 in which said housing has a bottom up through which said feed pipe extends and in which said outlet is formed around said feed pipe, said housing having inside surfaces extending from said run-off edge to said outlet and all of said inside surfaces smoothly declining to avoid entrapment of the liquid metal on said inside surfaces.

6. The device of claim 3 in which said baffle surface has a central depending conical part with an apex positioned in the open top of said feed pipe to form therewith an annular liquid metal ejection opening leading to said annular concave surface.

7. The device of claim 2 in which said insert has an exposed top surface and includes radiation shielding material interposed between said baffle means and the insert'"'"'s exposed top surface.

8. The device of claim 1 in which an electric heating coil having a non-uniform pitch encircles said housing in an area at least encompassing said positioning means for said ring of crucibles inside of the housing.

9. The device of claim 8 in which said coil extends above and below said area and said pitch is larger at said area and smaller above and below said area.

10. The device of claim 9 in which said pitch is larger above said area than it is below said area.

11. The device of claim 2 in which said insert and housing have Stellite clad inter-sealing surfaces.

12. The device of claim 11 in which at least one of said inter-sealing surfaces is crowned in shape.

13. The device of claim 1 having thermocouples soldered to said mounting means.

14. The device of claim 6 having a thermocouple positioned in said apex and signal wires extending from the thermocouple upwardly through said conical part.