Metering system

• US 3,987,808 A
• Filed: 01/07/1975
• Issued: 10/26/1976
• Est. Priority Date: 01/11/1974
• Status: Expired due to Term

• Current Assignee: Sandoz Inc. (Novartis Ag)
• Original Assignee: Sandoz Inc. (Novartis Ag)
• Inventors: Hasler, Rolf, Walliser, Roland, Carbonell, Jose
• Primary Examiner(s): Nilson, Robert G.
• Application Number:
  US05/539,228
• Time in Patent Office: 658 Days
• Field of Search: 222/52, 222/129, 137/3, 137/4, 137/5, 137/6, 137/7, 137/88, 137/91, 137/92, 137/93, 137/624.11
• US Class Current: 137/3
• CPC Class Codes: B01F 35/82 by adding a material to be mixed to a mixture in response to a detected feature, e.g. density, radioactivity, consumed power or colour
• CPC Class Codes: B01J 4/02 for feeding measured , i.e. prescribed quantities of reagents
• CPC Class Codes: G05D 21/02 characterised by the use of electric means
• CPC Class Codes: Y10T 137/0329 Mixing of plural fluids of diverse characteristics or conditions
• CPC Class Codes: Y10T 137/2509 By optical or chemical property

Abstract

The invention concerns a novel automatic metering system for producing a liquor containing a predetermined concentration of at least one component thereof, which comprises a mixing tank in which the liquor components are mixed, a metering device adapted to meter out at least one of the components into the mixing tank, an analyzer adapted to measure the concentration of the component(s) required at a predetermined concentration and a data processing unit, with an input from the analyzer and an output to the metering device, being programmed to effect an operational cycle which comprises computing the deviation of the measured concentration from the predetermined concentration of the component(s), correlating the deviation with the amount of at least one of the components necessary to be metered out, substantially to reduce said deviation by a reduction factor of less than 100 percent, and automatically operating the metering device to meter out the correlated amount, and to repeat said operational cycle until the predetermined concentration has been substantially reached, and a method of operating the system.

Claims

1. An automatic metering system for producing a liquid at least one component of which is present at a predetermined concentration which comprises a mixing tank in which the liquor components are mixed, a metering device adapted to meter out varying amounts of at least one of the components into the mixing tank, an analyser adapted to measure the concentration in the mixed liquor components of a component which is to be ultimately present at a predetermined concentration and a data processing unit with an imput from the analyser and an output to the metering device, being programmed to effect an operational cycle which comprises computing the deviation of the measured concentration from the predetermined concentration, correlating the deviation with the amount of at least one of the components necessary to be metered out substantially to reduce said deviation by a reduction factor of less than 100 percent and automatically operating the metering device to meter out the correlated amount, and to repeat said operational cycle until the predetermined concentration has been substantially reached.

2. An automatic metering system according to claim 1, wherein the data processing unit is programmed to operate the metering device before commencing the operational cycle to meter out into the mixing chamber a proportion of the amount of the liquor component which is to be present at a predetermined concentration.

3. An automatic metering system according to claim 2, wherein said proportion corresponds to the reduction factor applied in the operational cycle.

4. An automatic metering system according to claim 1, wherein said reduction factor is from 40 to 95 percent.

5. An automatic metering system according to claim 4, wherein said reduction factor is from 80 to 90 percent.

6. An automatic metering system according to claim 1, wherein the data processing unit is programmed to repeat the operational cycle thereof from 1 to 10 times.

7. An automatic metering system according to claim 6, wherein the data processing unit is programmed to repeat the operational cycle 2 or 3 times.

8. An automatic metering system according to claim 1, wherein the analyser comprises a spectrophotometer.

9. An automatic metering system according to claim 8, wherein the spectrophotometer incorporates a device enabling the spectrophotometer to operate over the optimum absorption range.

10. An automatic metering system according to claim 9, wherein said device comprises a liquor dilution device.

11. An automatic metering system according to claim 1, wherein the metering device comprises from 2 to 5 metering heads, each adapted to handle a separate liquor component.

12. An automatic metering system according to claim 11, wherein the metering device comprises 3 metering heads, each adapted to handle a separate liquor component.

13. An automatic metering system according to claim 11 wherein the analyser is adapted to measure the concentrations of a plurality of components which are to be present at predetermined concentrations, and the data processing unit is programmed to compute the deviation of the measured concentrations from the respective predetermined concentrations, correlate the deviations with the amounts of the respective components to be metered out to reduce said deviations by a reduction factor of less than 100% and automatically operate the metering devices to meter out the correlated amounts.

14. An automatic metering system according to claim 13 wherein the analyser is a spectrophotometer having a diluting device for diluting the samples of liquor to be analysed and adapted to measure the extinction coefficient of each measured component at its respective absorption maximum and the data processing unit is additionally programmed to correct the extinction coefficient data at the absorption maximum of a particular component for the absorption due to other components in the liquor at the absorption maximum of the particular component under observation and convert the corrected extinction coefficient data into data compatible with the predetermined concentration data.

17. A method according to claim 6, wherein the said proportion corresponds to the reduction factor applied in the operational cycle.

15. A method of automatically producing a liquor containing a predetermined concentration of at least one component thereof which comprises effecting the operational cycle of measuring the concentration in a premixed liquor of a component which is to be ultimately present at a predetermined concentration, automatically determining the deviation of the measured concentration from the predetermined concentration, correlating the deviation with the amount of at least one of the components to be added to the liquor substantially to reduce said deviation by a reduction factor of less than 100 percent and automatically metering out the correlated amount into the premixed liquor, and repeating said operational cycle until the predetermined concentration has been substantially reached.

16. A method according to claim 15, wherein the premixed liquor is prepared before effecting the operational cycle, the component which is to be ultimately present at the predetermined concentration being automatically metered out in an amount corresponding to a proportion of the amount necessary to give said predetermined concentration.

18. A method according to claim 15, wherein said reduction factor is from 40 to 95 percent.

19. A method according to claim 18, wherein said reduction factor is from 80 to 90 percent.

20. A method according to claim 15, wherein the operational cycle is repeated from 1 to 10 times.

21. A method according to claim 20, wherein the operational cycle is repeated 2 or 3 times.

22. A method according to claim 15, when applied to the production of a liquor having a predetermined concentration of 2 to 5 separate liquor components.

23. A method according to claim 22, when applied to the production of a liquor having a predetermined concentration of 3 separate liquor components.

24. A method according to claim 15, when applied to the production of a dye liquor.

25. A method according to claim 15 which comprises measuring, by means of a spectrophotometer, the extinction coefficients at their respective absorption maxima of each of a plurality of dyes in a dye liquor, correcting the extinction coefficient data for each dye at its absorption maximum for the absorption due to the other dyes in the liquor, converting the corrected extinction coefficients into corresponding concentration measurements for each dye, computing the deviation between the measured concentration and the predetermined concentration for each dye, correlating each deviation with the amount of each dye to be added to the liquor to reduce each deviation by a factor of 50 to 95 percent, metering out the correlated amount of each dye into the liquor and repeating the foregoing until the predetermined concentration of each dye has been substantially reached.