Apparatus and method for detecting explosives

• US 3,997,787 A
• Filed: 04/25/1975
• Issued: 12/14/1976
• Est. Priority Date: 04/25/1975
• Status: Expired due to Term

• Current Assignee: Bain Griffith
• Original Assignee: Bain Griffith
• Inventors: Fearon, Robert E., Scherbatskoy, Serge A.
• Primary Examiner(s): Dixon, Harold A.
• Application Number:
  US05/571,702
• Time in Patent Office: 599 Days
• Field of Search: 250/303, 250/312, 250/358, 250/359, 250/363, 250/367, 250/499, 250/500, 250/492 R, 250/494
• US Class Current: 250/359.1
• CPC Class Codes: G01N 2223/071 combination of measurements, at least 1 secondary emission
• CPC Class Codes: G01N 2223/074 activation analysis
• CPC Class Codes: G01N 23/09 the radiation being neutrons
• CPC Class Codes: G01N 23/10 the material being confined in a container, e.g. in a luggage X-ray scanners
• CPC Class Codes: G01N 23/222 using neutron activation analysis [NAA]
• CPC Class Codes: G01N 33/22 Fuels, explosives liquid hydrocarbons G01N33/28
• CPC Class Codes: G01V 5/224 Multiple energy techniques using one type of radiation, e.g. X-rays of different energies
• CPC Class Codes: G01V 5/234 Measuring induced radiation, e.g. thermal neutron activation analysis

Abstract

Apparatus and method for detecting the presence of nitrogen and oxygen-containing explosives within a container by irradiating the container with thermal and high energy neutrons, and then measuring the quantity of thermal energy neutrons passing through the container and the quantity of radioactive nitrogen 16 generated within the container. The measurements of neutron absorption and nitrogen 16 are correlated to provide an output signal indicative of whether the material within the container is an explosive.

Claims

1. A method of detecting the presence of a substance within a container, which substance contains at least first and second component materials in amounts exceeding predetermined amounts, comprising the steps of:

a. irradiating said container with energy of a first kind,

b. measuring the quantity of said first kind of energy passing through said container to obtain an indication corresponding to the amount of said first component material within said container,

c. storing said indication,

d. irradiating said container with energy of a second kind for transferring said second component material to a radioactive material,

e. removing said container from the source of said second kind of energy,

f. measuring the quantity of radioactive material within said container to obtain an indication corresponding to the amount of said second component material within said container, and

g. correlating said indications of the amounts of said first and second component materials to provide an output signal.

2. The method defined by claim 1 wherein said first kind of energy comprises thermal energy neutrons and said second kind of energy comprises neutrons having energies in excess of 10.6 ×

10⁶ electron volts per neutron.

3. A method of detecting the presence of a substance located within a container, which substance includes oxygen and nitrogen in amounts exceeding predetermined amounts comprising:

a. irradiating said container with thermal energy neutrons,

b. measuring the quantity of said thermal energy neutrons passing through said container to obtain an indication corresponding to the amount of neutron absorbing material including nitrogen within said container,

c. storing said indication,

d. irradiating said container with higher energy neutrons having energies in excess of 10.6 ×

10⁶ electron volts per neutron to transform the oxygen within said container to radioactive nitrogen of atomic weight 16,

e. removing said container from the source of higher energy neutrons,

f. measuring the quantity of said radioactive nitrogen 16 within said containers to obtain an indication corresponding to the amount of oxygen within said container, and

g. correlating said indications of nitrogen and oxygen to provide an output signal.

4. The method defined by claim 3 wherein the step of measuring the quantity of thermal energy neutrons passing through the container comprises placing a film adjacent said container while said container is being irradiated by said thermal energy neutrons, said container being located between the source of said neutrons and said film;

and placing said film adjacent a first array of Geiger counters to obtain an output corresponding to the beta ray emission from said film.

5. The method defined by claim 3 wherein the step of measuring the quantity of radioactive nitrogen 16 within said container comprises placing said container adjacent a second array of Geiger counters, said second array of counters including a plurality of sets of counters, each of said sets comprising at least two axially spaced counters;

and eliminating from the outputs of each set of counters all signals produced by high energy neutrons not intercepted by all of the axially spaced counters in said set of counters.

6. The method defined by claim 3 wherein the step of measuring the quantity of thermal energy neutrons passing through the container comprises placing a film adjacent said container while said container is being irradiated by said thermal energy neutrons, said container being located between the source of said neutrons and said film;

and placing said film adjacent a first array of Geiger counters to obtain an output corresponding to the beta ray emission from said film, and wherein the steps of measuring the quantity of radioactive nitrogen 16 within said container comprises placing said container adjacent a second array of Geiger counters, said second array of counters including a plurality of sets of counters, each of said sets comprising at least two axially spaced counters; and

eliminating from the outputs of each set of counters all signals produced by high energy neutrons not intercepted by all of the axially spaced counters in said set of counters.

7. The method defined by claim 3 wherein said thermal energy neutrons have energies in the range 0.01 to 0.10 electron volt per neutron.

8. Apparatus for detecting the presence of a substance within a container, which substance contains oxygen and nitrogen in amounts exceeding predetermined amounts comprising:

a. a thermal energy neutron source for irradiating said container with thermal energy neutrons,

b. a high energy neutron source for transforming oxygen within said container to radioactive nitrogen of atomic weight 16,

c. means for positioning said container in the path of energy emitted by said thermal and high energy neutron sources respectively,

d. first measuring means for measuring the quantity of thermal energy neutrons passing through said container,

e. second measuring means for measuring the quantity of radioactive nitrogen 16 within said container, and

f. means coupled to said first and second measuring means for correlating the outputs of said means for measuring the quantity of thermal energy neutrons passing through said container and said means for measuring the quantity of radioactive nitrogen 16 within said enclosure to obtain indications of the amount of neutron absorbing material including nitrogen within the container and the amount of oxygen with said container.

9. The apparatus defined by claim 8 wherein said means for measuring the quantity of thermal energy neutrons passing through said container comprises a film positioned adjacent said container, said container being located between said thermal energy neutron source and said film;

and a first Geiger counter array for obtaining an output corresponding to the beta ray emission from said film.

10. The apparatus defined by claim 9 wherein said film is made of indium.

11. The apparatus defined by claim 8 wherein said means for measuring the quantity of radioactive nitrogen 16 within said container comprises a second Geiger counter array, said second Geiger counter array comprising at least two coplanar groups of counters positioned in registration to form a plurality of sets of counters spaced along axes perpendicular to the planes of said groups of counters, the output of the counters in each set being connected to a common output terminal.

12. The apparatus defined by claim 11 wherein said Geiger counter array comprises three coplanar groups of counters.

13. The apparatus defined by claim 8 wherein said correlating means comprises:

a. first and second threshold means coupled to said first and second measuring means respectively, said first and second threshold means producing output signals only when said first and second measuring means have outputs exceeding predetermined magnitudes,

b. first and second storage means coupled to the outputs of said first and second threshold means respectively for storing said threshold output signals, and

c. display means coupled to the output of said first and second storage means respectively for displaying the amounts of nitrogen and oxygen in the substance located within said container.

14. The apparatus defined by claim 13 wherein said display means comprises a cathode ray tube having its first and second deflection plates coupled to the outputs of said first and second storage means respectively, the position of the electron beams of said cathode ray tube providing an indication corresponding to the relative amounts of nitrogen and oxygen within said container.

15. The apparatus defined by claim 14 wherein said cathode ray tube is provided with a mask having an aperture therein for displaying only predetermined positions of said electron beam.

16. The apparatus defined by claim 13 wherein said display means comprises first and second light emitting diodes coupled to the outputs of said first and second storage means respectively, said first and second diodes emitting light when the outputs of said first and second measuring means exceed respectively said predetermined threshold magnitudes.

17. The apparatus defined by claim 13 wherein said display means comprises a cathode ray tube having its first and second deflection plates coupled to the outputs of said first and second storage means respectively, the position of the electron beams of said cathode ray tube providing an indication corresponding to the relative amounts of nitrogen and oxygen within said container, and first and second light emitting diodes coupled to the outputs of said first and second storage means respectively, said first and second diodes emitting light when the outputs of said first and second measuring means exceed respectively said predetermined threshold magnitudes.