Slab gel dryer and method

• US 4,020,563 A
• Filed: 04/21/1975
• Issued: 05/03/1977
• Est. Priority Date: 04/21/1975
• Status: Expired due to Term

• Current Assignee: Hoefer Scientific Instruments (Danaher Corporation)
• Original Assignee: Hoefer Scientific Instruments (Danaher Corporation)
• Inventors: Hoefer, Stanton A.
• Primary Examiner(s): Camby, John J.
• Assistant Examiner(s): Schwartz, Larry I.
• Application Number:
  US05/569,838
• Time in Patent Office: 743 Days
• Field of Search: 34/16, 34/48, 34/92, 34/15, 219/243, 219/385, 219/460, 264/101, 264/102, 264/349
• US Class Current: 34/552
• CPC Class Codes: F26B 25/22 Controlling the drying process in dependence on liquid content of solid materials or objects
• CPC Class Codes: F26B 5/045 for drying thin, flat articles in a batch operation, e.g. leather, rugs, gels
• CPC Class Codes: F26B 9/003 Small self-contained devices, e.g. portable

Abstract

An apparatus for drying slab gels having a metal platen with electrical strip heaters mounted on one side thereof and a depression formed in the other side which serves as a drying chamber. The slab gel is laid on a sheet of porous filter paper over which is laid a sheet of non-porous material having non-adhesive qualities relative to the slab gel. The mounted and covered slab gel is placed in the depression and a compliant cover sheet is placed over the top of the depression overlapping the platen around the periphery of the depression. An open passage is formed through one edge of the platen in communication with the depression therein. The strip heaters are connected to an electrical power source and the open passage is connected to a vacuum source. The pressure in the depression is reduced relative to ambient pressure causing the compliant cover to be forced against the platen around the periphery of the depression for sealing the drying chamber. Moisture vaporized from the slab gel is removed through the open passage. A thermostat may be used to control the temperature of the platen and a timer may be used to provide for a predetermined period of heating and evacuation of the drying chamber. A temperature sensor may be placed in intimate contact with the slab gel for producing a signal to a relay for interrupting heater power when slab gel temperature rises through a predetermined temperature after substantially all of the moisture content has been vaporized from the slab gel.

Claims

1. An apparatus for dehydrating slab gels comprising a porous filter sheet for contacting the slab gel on one side thereof, an overlay sheet for contacting the slab gel on the other side thereof, said overlay sheet having a smooth non-porous surface thereby being nonadherent to the slab gel, a platen, said platen having a depression formed on one side having boundaries including a bottom with a predetermined area for receiving said overlay and porous filter sheets, a compliant cover overlaying said depression and having a size greater than said predetermined area, said depression having an opening through one boundary thereof, means for communicating a vacuum source with said opening for producing low pressure in said depression, means for uniformly supporting and for providing substantially uniform dispersal of said low pressure over the side of said porous filter sheet facing said bottom boundary, and a heater disposed on the other side of said platen, so that when the slab gel is placed between said overlay and porous filter sheets and disposed in said depression and low pressure is induced therein, ambient pressure forces said compliant cover against the periphery of said depression thereby providing a seal therebetween and said overlay sheet holds the slab gel firmly against said porous filter sheet, whereby moisture in the slab gel is vaporized by said heater and removed from said depression through said opening and the slab gel is fixed onto said porous filter sheet in a dehydrated condition.

2. An apparatus as in claim 1 wherein said means for uniformly supporting comprises a screen having a plurality of holes therethrough for passing the vaporized moisture, said screen being disposed between said porous filter sheet and said bottom boundary of said depression, whereby the slab gel is supported during dehydration without fracturing or distorting the slab gel.

3. An apparatus as in claim 1 together with means for electrically actuating said heater, a thermostat, said thermostat being in electrical contact with said means for actuating and in thermal contact with said platen and having a preset control temperature, whereby said platen temperature is controlled at substantially said control temperature.

4. An apparatus as in claim 1 together with means for timing a period for energizing said heater, said means for timing being adjustable over a predetermined time range, whereby the slab gel may be dehydrated for said period within said predetermined time range.

5. An apparatus as in claim 4 wherein the vacuum source is electrically actuated, together with an electrical connection between said means for timing and the vacuum source, whereby vaporized moisture is removed from said depression for said period.

6. An apparatus as in claim 1 together with means for electrically actuating said heater, a temperature sensor mounted adjacent to the slab gel, said temperature sensor providing a first signal level indicative of the wet temperature of the slab gel and a second signal level indicative of the dry temperature of the slab gel, and means for disconnecting said means for electrically actuating from said heater, said means for disconnecting being responsive to said second level.

7. An apparatus for drying slab gels comprising a support frame, a platen supported on said support frame and having a drying chamber formed on one side thereof, means for supporting a slab gel formed for positioning in said drying chamber, said means for supporting contacting one side of the slab gel, whereby the other side is an exposed side, a cover for contacting said platen around the periphery of said drying chamber, means for heating said drying chamber, means for overlying the exposed side of the slab gel and in contact therewith, said means for overlying having a smooth nonporous surface thereby being nonadherent to the slab gel, and vacuum means in communication with said drying chamber for reducing the pressure therein relative to ambient pressure, whereby ambient pressure forces said cover against said platen thereby providing a peripheral seal for said drying chamber, so that when a wet slab gel is placed on said means for supporting, moisture vapor is removed therefrom and from said drying chamber by said vacuum means and the slab gel is fixed on the means for supporting.

8. An apparatus as in claim 7 together with means for timing a predetermined period, and producing a timer output at the end thereof, a thermostat adjacent to said means for heating for controlling the temperature in said drying chamber during said predetermined period, said timer output being connected to interrupt said means for heating at the end of said predetermined period, thereby producing a preset drying time at a controlled temperature.

9. An apparatus as in claim 7 wherein said means for heating is electrically energized, together with a temperature sensor adjacent to the slab gel producing an output signal indicative of a dry slab gel circuit means having closed and open circuit conditions connected between said means for heating and an electrical source, so that when the moisture in the slab gel is substantially all removed said output signal opens said circuit means and disconnects said means for heating from the electrical source.

10. An apparatus as in claim 7 wherein said means for supporting a slab gel comprises porous filter member for mounting the slab gel on said one side, and a screen underlying said porous filter member in contact therewith, said porous filter member operating to adhere to the dried slab gel and said screen supplying support to reduce fracture and distortion in the slab gel during drying.

11. An apparatus as in claim 7 together with means for exposing one side of said means for supporting t0 substantially uniform pressure thereacross, whereby slab gels are protected from fracture or distortion during drying.