Method and apparatus for automatically measuring distribution of reflectance of coals

• US 4,030,837 A
• Filed: 09/29/1975
• Issued: 06/21/1977
• Est. Priority Date: 09/29/1975
• Status: Expired due to Term

• Current Assignee: Nippon Steel Corporation
• Original Assignee: Nippon Steel Corporation
• Inventors: Sakurai, Yoshihisa, Motegi, Masayoshi, Sugai, Tetuya, Kojima, Kojiro
• Primary Examiner(s): Corbin, John K.
• Assistant Examiner(s): Rosenberger, R. A.
• Application Number:
  US05/617,490
• Time in Patent Office: 631 Days
• Field of Search: 356/30, 356/209, 356/210, 356/215, 250/571, 250/572
• US Class Current: 356/445
• CPC Class Codes: G01N 21/55 Specular reflectivity

Abstract

A method and apparatus for automatically measuring the distribution of reflectance of coals is given, which comprises the steps of vertically projecting light to samples of coals on a movable stage, allowing a photodetector to receive said light through a microscope as the stage moves, thereby measuring the reflectance of the samples at a great number of points to obtain the distribution of reflectance, and determining the property of the coals from this distribution of reflectance.

Claims

1. A method for measuring the reflectance of the coals which comprises providing a movable sample stage below a microscope, said stage moving stepwise by a predetermined distance at each predetermined time, placing a sample on said sample stage, projecting light onto said sample, conducting light reflected by said sample to a photodetector via said microscope for converting said reflected light to an electrical output, integrating said output, repeating the above measuring operation at each such movement of said stage so as to measure the reflectance at a large plurality of points, introducing into a calculation unit outputs accumulated in said integrating unit by the instruction of a control unit controlling the movement of said stage, said calculation unit and a record indication unit, said calculation unit conducting an operation for measuring the distribution of the reflectance, and displaying the results of such calculation unit operation so as to indicate the distribution of the reflectance.

2. A method according to claim 1 in which the reflectance of the sample to be measured is measured at 10,000 points or more with predetermined distance and the distribution of that reflectance is measured.

3. A method according to claim 1 for predicting the coking property of the coals by determining the distribution of the reflectance, which comprises measuring quantitatively the "reactives" and the "inerts" based on the respective reflectance characteristics and also determining the reflectance of the "reactives".

4. An apparatus adapted for use in automatically measuring the reflectance of coals which comprises a photodetector mounted to receive light from a microscope for converting the reflected light from a sample via said microscope to an electric output, a sample stage mounted below said microscope, means for moving said sample stage in longitudinal and lateral directions by predetermined distances, an integrating unit connected to said photodetector for integrating such electric outputs, a calculation unit connected to said integrating unit for determining reflectance distribution, a controlling unit for controlling the operations of said sample stage, of said integrating unit and of said calculation unit, and a recording indication unit for recording the distribution of the reflectance.

5. An apparatus according to claim 4 in which such moving means move said sample stage stepwise laterally and longitudinally for a predetermined distance in the range of 10 and 100 μ

m and stops such movement completely for a measuring time in the range of 5 to 50 ms.

6. A method for measuring the reflectance of the coals which comprises providing a movable sample stage below a microscope, said stage moving stepwise by a predetermined distance at each predetermined time, placing a sample on said sample stage, projecting light onto said sample, conducting light reflected by said sample to a photodetector via said microscope for converting said reflected light to an electrical output, integrating said output, repeating the above measuring operation at each such movement of said stage so as to measure the reflectance at a large plurality of points, introducing into a calculation unit outputs accumulated in said integrating unit by the instruction of a control unit controlling the movement of said stage, said calculation unit and a record indication unit, said calculation unit conducting an operation for measuring the distribution of the reflectance, and displaying the result of such calculation unit operation so as to indicate the distribution of the reflectance, said predetermined distance in such stepwise movement of said stage being selected from first measures of about 100 μ

m and second measures of about 100 μ

m, said calculation unit operation involving only those integrated electrical outputs obtained in cases where the difference of the reflectance between adjacent points spaced by such 10 μ

m distance is not more than 0.025%, such reflectance distribution thereby being determined as that of "reactives".