Optical analyzer for agricultural products

• US 4,037,970 A
• Filed: 01/30/1976
• Issued: 07/26/1977
• Est. Priority Date: 08/24/1972
• Status: Expired due to Term

• Current Assignee: NIR Instruments Company
• Original Assignee: Neotec, Inc.
• Inventors: Webster, Donald R., Ganssle, Eugene R.
• Primary Examiner(s): Evans, F. L.
• Application Number:
  US05/653,848
• Time in Patent Office: 543 Days
• Field of Search: 356/36, 356/39, 356/51, 356/83, 356/84, 356/96, 356/97, 356/99, 356/100, 356/179, 356/180-186, 356/188, 356/189, 356/195, 356/201, 356/204-206, 356/209-212 , 356/243-246, 350/166, 350/266, 350/275, 350/311, 350/315, 350/318, 235/151.35, 250/226, 250/233
• US Class Current: 356/418
• CPC Class Codes: B07C 2501/009 Sorting of fruit
• CPC Class Codes: G01J 2001/182 with SH sample and hold circuits
• CPC Class Codes: G01J 2003/1243 Pivoting IF or other position variation
• CPC Class Codes: G01J 2003/2866 Markers; Calibrating of scan
• CPC Class Codes: G01N 2021/3129 Determining multicomponents by multiwavelength light
• CPC Class Codes: G01N 2021/3159 Special features of multiplexing circuits
• CPC Class Codes: G01N 2021/4769 Fluid samples, e.g. slurries, granulates; Compressible powdery of fibrous samples
• CPC Class Codes: G01N 21/314 with comparison of measurements at specific and non-specific wavelengths dual wavelength spectrometry G01J3/427
• CPC Class Codes: G01N 21/35 using infrared light G01N21/39 takes precedence
• CPC Class Codes: G01N 21/3563 for analysing solids; Preparation of samples therefor
• CPC Class Codes: G01N 21/4738 Diffuse reflection precedence is given to G01N21/55 - G01N21/57 if specular component is taken into consideration, e.g. also for testing fluids, fibrous materials
• CPC Class Codes: G01N 2201/1283 Opaque part
• CPC Class Codes: G01N 33/10 Starch-containing substances, e.g. dough

Abstract

An automatic test instrument for gaging the percentage of various constituents in organic substances by comparing the reflective optical density of the subject at various wavelengths. Narrow band optical filters are connected together in the form of a rotatable paddle wheel positioned so that the filters can be individually swept through the incident light path between the specimen and wideband light source. As the filter wheel turns, the band of light passed by each filter is progressively shifted with the changing angle of the filter relative to the light path. The filter wheel configuration includes opaque vanes extending from the ends of the filters to periodically interrupt the passage of light to the specimen. Photocells are positioned to sense the level of light reflected from the specimen. The output of the photocells is sampled at predetermined times relative to the rotation of the filter wheel to yield values indicative of reflected intensity at certain wavelengths. Using these values, an electronic circuit in one embodiment calculates three optical density difference values corresponding to moisture, protein and oil content of the specimen. The difference values are automatically inserted in three linear equations which are solved to obtain readings representing the true percentages of oil, water and protein contained in the specimen. Each time a new specimen is loaded for testing, the instrument is automatically calibrated against a standard sample, preferably Teflon (Trademark). The output of the photocells is amplified in a special circuit which subtracts the level of dark period current from the output when the photocells are illuminated.

Claims

1. Optical apparatus, comprising a source of wide band light for illuminating an object, a multiple filter assembly having a rotatable axle and a plurality of narrow bandwidth optical interference filters fixed to said axle and radiating therefrom at the same axial location in respective planes forming therewith a paddlewheel configuration, said filter assembly being positioned relative to the light path defined between said light source and the object such that said filters are swept through said light path individually during rotation of said axle, said wide band light impinging on each successive one of said filters as the orientation thereof relative to said light path is changing, whereby light passing through each one of said filters is restricted to continuously shifting bandwidths as a function of the instantaneous angle between said light path and a given filter during rotation, photosensitive means positioned to receive light from said source of light after passing through one of said filters and coming into optical contact with said object and to produce a signal representative of the level of light received, and means responsive to said signal to provide an indication of a characteristic of said object.

2. The apparatus of claim 1, wherein said filters are equally spaced angularly about said axle, and the planes of said filters interesect approximately in a line coincident with the axis of rotation of said filter assembly.

3. The apparatus of claim 2, wherein the axis of rotation of said filter assembly is approximately perpendicular to and spaced laterally from said light path.

4. The apparatus of claim 3, wherein said filters are three in number.

5. The apparatus of claim 1, wherein the optical characteristics of said filters are predetermined such that the respective ranges of wavelengths passed by said filters during rotation are approximately contiguous, whereby a composite range of wavelengths is spanned during each complete revolution of said filter assembly.

6. The apparatus of claim 1, further comprising drive means operatively connected to said axle for imparting continuous rotation thereto, the position of said axle along the axis of rotation being fixed.

7. The apparatus of claim 1, further comprising means fixed to and extending from the outer end of at least one of said filters for at least partially interrupting the passage of light from said light source to the object.

8. The apparatus of claim 7, wherein said interrupting means includes a vane extending perpendicularly to the plane of the filter.

9. The apparatus of claim 1, further comprising a substantially opaque vane fixed to the outer end of each of said filter and extending perpendicularly to the plane of said filter a predetermined distance such that the passage of light from said source to the object is interrupted for a period of time between sweeps of adjacent filters through said light path.

10. The apparatus of claim 1, further comprising transducer means responsive to the rotation of said axle for providing a fixed number of pulses per axle revolution, counter means connected to receive the output of said transducer means for registering the number of pulses produced thereby per revolution, and logic means operatively connected to said counter means for providing a plurality of output signals at times corresponding approximately to predetermined discrete orientations of each said filter in said light path.

11. Optical apparatus, comprising a source of wide band light for illuminating an object, a multiple filter assembly having a rotatable axle and a plurality of narrow band width optical filters fixed to said axle and radiating therefrom at the same axial location in respective planes forming therewith a paddlewheel configuration, said filter assembly being positioned relative to the light path defined between said light source and the object such that said filters are swept through said light path individually during rotation of said axle such that light passing through each one of said filters is restricted to continuously shifting band widths corresponding to the instantaneous angle between said light path and a given filter during rotation, said filter assembly further including substantially opaque vanes each fixed to the outer end of a respective one of said filters and extending perpendicularly to the plane of said filter a predetermined distance such that the passage of light from said source to the object is interrupted for a period of time between sweeps of adjacent filters through said light path, at least one photosensitive means positioned to receive light from said source after passing through one of said filters and coming to optical contact with the object for producing an electrical output indicative of the level of received light, and analyzer means connected to receive the output of said light sensitive means for producing an electrical output indicative of the difference between the output of said light sensitive means when the object is illuminated via said filter assembly and when the object is in relative darkness due to interruption of the passage of light by one of said vanes.

12. Optical measuring apparatus comprising a source of wide band light for illuminating an object, a multiple filter assembly having a rotatable axle and a plurality of optical filters fixed to said axle forming therewith a paddlewheel configuration, said assembly being positioned relative to the light path defined between said light source and the object such that the filters are swept through said light path individually during rotation of said axle, light sensitive means operatively positioned to produce an output indicative of the level of light received from said source after passing through one of said filters and coming into optical contact with said object, logic means responsive to the rotation of said axle for producing a plurality of outputs indicative of illumination of said object by certain wavelengths of light, logarithmic amplifier means operatively receiving the output of said light sensitive means, a pair of sample and hold circuits operatively connected to receive the output of said logarithmic amplifier means and connected respectively for selective control by said logic means, differential amplifier means operatively connected to receive the outputs of said pair of sample and hold circuits to produce an output indicative of Δ

OD, wherein Δ

OD represents the difference in optical density at a pair of different wavelengths, a plurality of additional sample and hold circuits operatively connected to receive the output of said differential amplifier and respectively connected for selective control by said logic means to store separate outputs indicative of Δ

OD at different pairs of wavelengths, and computer means operatively receiving the outputs of said additional sample and hold circuits for computing the value of a mathematical function of the outputs of said additional sample and hold circuits.

13. The apparatus of claim 12, further comprising transducer means operatively connected to said axle for providing an output to said logic means indicative of the instantaneous angular position of said filter assembly during rotation.

14. The apparatus of claim 13, further comprising sensor amplifier means connected between said light sensitive means and said logarithmic amplifier means, said filter assembly including means for regularly interrupting the passage of light from said light source to the object to produce dark periods, said logic means producing an output to said sensor amplifier means indicative of said dark periods, said sensor amplifier unit having means responsive to the output of said logic means indicative of said dark periods for producing an output proportional to the difference between the outputs of said light sensitive means when said object is illuminated and when said object is in relative darkness.

15. Optical apparatus, comprising a source of wide band light for illuminating an object, a light path being defined between said source and said object, a plurality of narrow band optical interference filters, mounting means for successively moving individual ones of said filters through said light path to intercept and filter said wide band light and for continuously reorienting each said filter through a range of angles of incidence of said light path relative to said filter as said filter moves through said light path, light passing through each one of said filters being restricted to continuously shifting bandwidths as a function of the instantaneous size of said angle of incidence for a given filter, at least one photosensitive means positioned to receive light from said source after passing through one of said filters and coming into optical contact with said object and to produce a signal representing the amplitude of said reflected light, and means responsive to said signal to provide an indication of the characteristic of said object.

16. The apparatus of claim 15, further comprising indicator means interconnected with said mounting means for providing output signals corresponding respectively to a plurality of predetermined discrete orientations of each said filter in said light path in order to identify the bandwidth of light being passed to the object at any given time.