Liquid dropping device

• US 4,042,153 A
• Filed: 11/17/1975
• Issued: 08/16/1977
• Est. Priority Date: 03/14/1973
• Status: Expired due to Term

• Current Assignee: Standard Oil Company (BP PLC)
• Original Assignee: Standard Oil Company (BP PLC)
• Inventors: Shaw, Wilfrid G., Miller, Arthur F., Callahan, James L.
• Primary Examiner(s): Tollberg, Stanley H.
• Assistant Examiner(s): Lane, Hadd
• Application Number:
  US05/632,536
• Time in Patent Office: 638 Days
• Field of Search: 222/207, 222/420-422, 417/478, 417/472, 417/473
• US Class Current: 222/207
• CPC Class Codes: B01J 2/02 by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops

Abstract

Distinct droplets of a slurry are dispersed by a dropping device consisting of a resilient tube connected to a liquid reservoir so that the liquid flows through the tube, and two valves and a plunger which work in a six-movement cycle on the outer surface of the resilient tube to discharge uniform droplets of liquid at equal drop intervals.

Claims

1. A dropping device for forming uniform droplets of a liquid comprising:

a liquid reservoir;

a resilient tube having a substantially circular cross-section in respose and one end connected to said liquid reservoir in such manner that liquid from the liquid reservoir can flow through the resilient tube and out of a second end, said second end being in a vertical position and being capable of retaining liquid within said tube, and producing a uniform and distinct drop when force is asserted on the outer surface of said resilient tube;

a first valve which is located toward the second end of said resilient tube and being capable of restricting the flow of liquid through the resilient tube by action on the outer surface of said resilient tube in a closed position and allowing flow of liquid through the resilient tube in an open position;

a second valve located along the resilient tube between said first valve and said liquid reservoir and being capable of restricting the flow of liquid through the resilient tube by action on the outer surface of said resilient tube in a closed position and allowing flow of liquid through said resilient tube in an open position; and

a plunger located between said first valve and said second valve, said plunger being capable of applying force on the outer surface of the resilient tube when said second valve is in the closed position and said first valve is in the open position, whereby a uniform and distinct drop is produced from said second end of the resilient tube.

2. The process of forming droplets from a slurry consisting of a suspending liquid and small particles suspended in the liquid comprising:

using as the dropping device the device of claim 1.

3. The process of claim 2 wherein the slurry consists of an aqueous mixture of metal oxides or metal oxide precursors.