Conversion of cellulose and lignin organic waste material into a more digestible and manageable form

• US 4,082,859 A
• Filed: 07/01/1975
• Issued: 04/04/1978
• Est. Priority Date: 07/01/1975
• Status: Expired due to Term

• Current Assignee: Sol Katzen
• Original Assignee: Sol Katzen
• Inventors: Katzen, Sol
• Primary Examiner(s): Penland, R. B.
• Application Number:
  US05/592,227
• Time in Patent Office: 1,008 Days
• Field of Search: 127/36-38, 426/635, 426/636, 426/2, 426/69, 426/74, 426/807, 426/623, 426/626, 71/25, 210/45, 210/59
• US Class Current: 426/636
• CPC Class Codes: A23K 10/32 from hydrolysates of wood or straw
• CPC Class Codes: Y02P 60/87 Re-use of by-products of food processing for fodder production
• CPC Class Codes: Y10S 426/807 Poultry or ruminant feed

Abstract

A process for the conversion of cellulose and lignin organic waste materials into a more digestible and manageable form. The process includes reducing, if necessary, the cellulose or lignin organic waste material to a size to 2 inches or less. An acid selected from the group consisting of phosphoric acid, hydrochloric acid, sulfuric acid and mixtures thereof is admixed with about 40 to about 60 percent by weight of the organic waste material. Before, after or simultaneously with such admixing steps, a base selected from the group consisting of calcium hydroxide, sodium hydroxide, potassium hydroxide, ammonium hydroxide and mixtures thereof is admixed with the remainder of the organic waste material. The acidified waste material is mixed and reacted with the basified organic waste material, a more digestible form of said organic waste material resulting. About 80 to 120 parts by weight of the acidified organic waste material is used per 100 parts by weight of the basified organic waste material. Water is converted to steam by heat of such reaction provided the reaction mixture contains about 20 to 60 percent by weight, based on the total weight of the reaction mixture, of water. The reacted mixture is formed into pellets, cubes, blocks or other similar forms.

Claims

1. A process for the conversion of cellulose and lignin organic waste material into a more digestible and manageable form which consists of the steps:

(a) reducing said cellulose or lignin organic waste material to a size less than 2 inches to facilitate further handling, when said organic waste material has a size greater than 2 inches, said cellulose or lignin organic waste material being selected from the group consisting of straw, stover, wood shavings, bagesse, corn cobs, peanut hulls, peat, tobacco stems, cocoa shells, rice hulls and soybean hulls;

(b) admixing an acid selected from the group consisting of phosphoric acid, hydrochloric acid, sulfuric acid, and mixtures thereof with about 40 to 60 percent by weight of said organic waste material;

(c) admixing, before, after or simultaneously with step (b), a base selected from the group consisting of calcium hydroxide, sodium hydroxide, potassium hydroxide, ammonium hydroxide and mixtures thereof with the remainder of said organic waste material;

(d) mixing and reacting said acidified organic waste material with said basified organic waste material, a more digestible form of said organic waste material resulting, about 80 to 120 parts by weight of said acidified organic waste material being used per 100 parts by weight of said basified organic waste material, said reaction mixture contains about 20 to 60 percent by weight of water based on the total weight of said reaction mixture, said water level being achieved whenever said water level is not present by drying said starting cellulose or lignin organic waste material or adding water to said cellulose or lignin organic waste material or portion thereof used in step (b) or step (c), whereupon part of said water in said reaction mixture converted to steam by exothermic heat produced as said reaction progresses, and whereby said organic waste material is converted into a substantially dry, more digestible form; and

(e) forming the reacted mixture of the step (d) into pellets, cubes, blocks or other similar forms.

2. A process as claimed in claim 1 wherein said size reduction is achieved by chopping or grinding.

3. A process as claimed in claim 1 wherein each portion of the waste material resulting from step (a) is conveyed to the subsequent admixing site by means of a belt, screw or pneumatic conveyor.

4. A process as claimed in claim 1 wherein said admixing steps (b) and (c) are each achieved in a continuous mixer.

5. A process as claimed in claim 4 wherein step (b) is achieved in a first continuous mixer and step (c) is achieved in a second continuous mixer.

6. A process as claimed in claim 4 where steps (b) and (c) are achieved sequentially in a single continuous mixer.

7. A process as claimed in claim 1 wherein said admixing steps (b) and (c) are achieved at a temperature between about 20°

and about 150°

F.

8. A process as claimed in claim 1 wherein all of said acids are used in step (b) and all of said bases are used in step (c).

9. A process as claimed in claim 1 wherein said acidified organic waste material of step (b) and said basified organic waste material of step (c) are immediately mixed together in step (d).

10. A process as claimed in claim 1 wherein said mixing step (d) is achieved in a continuous mixer.

11. A process as claimed in claim 1 wherein step (d) is achieved at a temperature between 20°

and 150°

F.

12. A process as claimed in claim 1 wherein step (e) involves pelletizing.