Low carbohydrate oilseed lipid-protein comestible

• US 4,088,795 A
• Filed: 11/19/1976
• Issued: 05/09/1978
• Est. Priority Date: 11/19/1976
• Status: Expired due to Term

• Current Assignee: Mead Johnson & Company (Reckitt Benckiser Group PLC)
• Original Assignee: Mead Johnson & Company (Reckitt Benckiser Group PLC)
• Inventors: Hartman, Grant H. Jr., Goodnight, Kenneth C. Jr.
• Primary Examiner(s): Jones, Raymond N.
• Assistant Examiner(s): Yoncoskie, R. A.
• Application Number:
  US05/743,246
• Time in Patent Office: 536 Days
• Field of Search: 426/615, 426/629, 426/634, 426/656, 426/489, 426/271, 426/598, 426/632, 210/23 H, 210/23 F, 260/123.5
• US Class Current: 426/598
• CPC Class Codes: A23C 11/103 containing only proteins from pulses, oilseeds or nuts, e.g. nut milk
• CPC Class Codes: A23J 1/14 from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds
• CPC Class Codes: A23L 11/65 Soy drinks

Abstract

An oilseed lipid-protein product adapted for food use is prepared by aqueous extraction of fat containing oilseed materials including the ground raw oilseed or full-fat oilseed flour or flake at a pH in excess of the isoelectric range of the protein for the purpose of solubilizing the protein. Insoluble material is removed by centrifugation or filtration, and soluble carbohydrate is removed from the resulting lipid-protein emulsion by membrane filtration.

Claims

1. The process for preparing an oilseed lipid-protein comestible which comprises:

(a) forming an aqueous suspension of edible oilseed containing suspended oilseed lipid, dissolved oilseed protein, and dissolved oilseed carbohydrate at a pH in excess of the isoelectric range of said protein, said suspension being obtained by aqueous extraction of particulate oilseed material containing lipid, protein, and carbohydrate at a pH in excess of the isoelectric range of said protein;

(b) separating particulate material from said suspension to yield an emulsion containing suspended lipid, dissolved protein, and dissolved carbohydrate; and

(c) separating carbohydrate from said emulsion by filtration employing a semi-permeable membrane which has the capability to retain suspended lipid and dissolved protein as retentate, and to pass dissolved carbohydrate as permeate.

2. The process of claim 1 wherein said oilseed is selected from the group consisting of chickpea, rapeseed, coconut, cottonseed, peanut, safflower seed, sesame seed, soybean, and sunflower seed.

3. The process of claim 1 wherein said oilseed is soybean.

4. The process of claim 3 wherein said particulate oilseed material in step (a) comprises ground soybean.

5. The process of claim 3 wherein said particulate oilseed material in step (a) comprises fat-containing soybean flour.

6. The process of claim 1 wherein said filtration employing a semi-permeable membrane in step (c) includes diafiltration.

7. The process of claim 6 wherein diafiltration is continued until said retentate has a protein coefficient of at least about 0.8.

8. The process of claim 6 wherein said diafiltration is continued until said retentate has a protein coefficient of at least about 0.9.

9. The process of claim 1 wherein said emulsion and said retentate in step (c) are maintained at a temperature within the range of about 45°

C. to 75°

C. during membrane filtration.

10. The process of claim 3 wherein said forming an aqueous suspension in step (a) and said separating particulate material in step (b) are conducted at a pH in excess of pH 10.1.

11. The process of claim 10 wherein steps (a) and (b) are carried out at a temperature in excess of about 10°

C.

12. The process of claim 10 wherein steps (a) and (b) are carried out at a temperature in the range of about 15°

C. to about 30°

C.

13. The process of claim 10 wherein said pH is within the range of pH 11 to pH 12.

14. The process of claim 3 wherein said forming an aqueous suspension in step (a) and said separating particulate material in step (b) is conducted at pH 10 or less.

15. The process of claim 14 wherein said pH is within the range of pH 7-9.

16. The process of claim 3 wherein said filtration employing a semi-permeable membrane in step (c) is conducted within the range of pH 6.5 to pH 7.5.

17. The process of claim 3 wherein step (b) includes heating said emulsion at a temperature of from 60°

C. to 150°

C. for a period sufficient to;

(i) improve the protein efficiency ratio of said lipid-protein comestible,

(ii) improve the functionality of said lipid-protein comestible as measured by sedimentation index, nitrogen solubility index, or emulsion stability index,

(iii) increase the ultrafiltration flux rate in step (c), or

(iv) reduce the microbial population of said emulsion produced in step (b) sufficiently to substantially eliminate spoilage thereof during filtration employing a semi-permeable membrane in step (c) said emulsion having a pH in excess of the isoelectric value of said protein but less than pH 10 during said heating.

18. The process of claim 17 wherein said period is from 1 sec. to 30 min.

19. The process of claim 17 wherein said heating is at a temperature in the range of from 60°

C. to 130°

C. for a period of from 45 sec. to 30 min.

20. The process of claim 3 wherein said retentate produced in step (c) is heated at a temperature in the range of from 60°

C. to 150°

C. for a period sufficient to

(i) improve the protein efficiency ratio of said retentate, or

(ii) improve the functionality of said retentate as measured by sedimentation index, nitrogen solubility index, or emulsion stability index.

21. The process of claim 20 wherein said retentate is combined with additional nutritional ingredients before heating.

22. The process of claim 20 wherein said period is from 1 sec. to 30 min.

23. The process of claim 20 wherein said temperature is in the range of from 60°

C. to 130°

C. and said period is from 45 sec. to 30 min.

24. The process for preparing a liquid food product containing oilseed protein and oilseed fat wherein said oilseed protein constitutes the principle protein ingredient of said product which comprises combining said retentate produced by the process of claim 1 with other nutritional ingredients.

25. The process of claim 1 wherein said retentate produced in step (c) is dried.

26. The product produced by the process of claim 1.

27. The product produced by the process of claim 3.

28. The product produced by the process of claim 10.

29. The product produced by the process of claim 14.

30. The product produced by the process of claim 17.

31. The product produced by the process of claim 20.

32. The product produced by the process of claim 24.

33. The product produced by the process of claim 25.