High sensitivity absorptiometer

• US 4,094,609 A
• Filed: 02/11/1977
• Issued: 06/13/1978
• Est. Priority Date: 02/19/1976
• Status: Expired due to Term

• Current Assignee: Hitachi, Ltd.
• Original Assignee: Hitachi, Ltd.
• Inventors: Fujii, Yoshio, Ohnuma, Sadabumi, Shimada, Mitsuo
• Primary Examiner(s): Corbin, John K.
• Assistant Examiner(s): Rosenberger, R. A.
• Application Number:
  US05/767,888
• Time in Patent Office: 487 Days
• Field of Search: 356/201, 356/204, 356/205, 356/206, 356/208, 353/52
• US Class Current: 356/435
• CPC Class Codes: G01J 3/02 Details
• CPC Class Codes: G01J 3/0286 Constructional arrangements for compensating for fluctuations caused by temperature, humidity or pressure, or using cooling or temperature stabilization of parts of the device; Controlling the atmosphere inside a spectrometer, e.g. vacuum
• CPC Class Codes: G01J 3/10 Arrangements of light sources specially adapted for spectrometry or colorimetry
• CPC Class Codes: G01N 21/255 Details, e.g. use of specially adapted sources, lighting or optical systems

Abstract

A high sensitivity absorptiometer comprises a light source lamp accompanied inevitably with heat generation, a sample container through which the light from the light source is transmitted and a detector device for detecting the light which has transmitted through the sample container. The light emitted from the light source lamp and directed to the sample container is adapted to pass through a chamber which is formed fluid-tight on a surface portion of the light source lamp or through a solid state optical conductor such as optical fiber having a light inlet end face closely fitted to the surface portion of the lamp, thereby to suppress movement and turbulence of air as caused by heat generated by the light source lamp with a view to excluding noise and drift ascribable to the air movement or turbulence phenomenon from the signal obtained from the detector device.

Claims

1. A high sensitivity absorptiometer comprising a light source lamp with an inevitable heat generation, sample containing means through which light from said light source lamp transmits, detecting means for detecting the light transmitted through said sample accommodating means, and a chamber formed by at least a surface portion of said light source lamp and an enclosing wall member fitted tightly to said surface so that said chamber is inhibited from fluid communication with the exterior, wherein said light emitted from said light source lamp and directed to said sample containing means is caused to pass through said chamber.

2. An absorptiometer as set forth in claim 1, wherein said chamber is formed by a surface portion of said light source lamp, an enclosing wall member tightly fitted to said surface and a light collecting lens mounted fluid-tight onto said enclosing wall member.

3. An absorptiometer as set forth in claim 1, wherein said chamber is formed by a surface portion of said light source lamp, an enclosing wall member closely fitted to said surface portion, and a light transmissive heat-shield member mounted fluid-tightly on said enclosing wall member.

4. An absorptiometer is set forth in claim 1, wherein said enclosing wall member is made of a material having a high thermal conductivity.

5. An absorptiometer as set forth in claim 1, wherein a plurality of chambers are provided between said light source lamp and said sample containing means, each of said chambers being enclosed by said enclosing wall member and partitioned from one another by light transmissive members so that said chambers are inhibited from fluid communication with ambient exterior, and wherein said light emitted by said light source lamp is guided to said sample containing means through said partitioned individual chambers.

6. An absorptiometer as set forth in claim 5, wherein at least one of said light tansmissive members is composed of a heat shielding element.

7. An absorptiometer as set forth in claim 5, wherein a space between said sample containing means and said detecting means is defined by a chamber closed fluid-tight from the ambient exterior.

8. An absorptiometer as set forth in claim 1, wherein said chamber is accommodated within a fluid-tight closed chamber.

9. An absorptiometer as set forth in claim 1, wherein said chamber and said sample containing means are housed within a fluid-tight closed chamber.

10. An absorptiometer as set forth in claim 1, wherein said chamber is housed within a first fluid-tight chamber and said sample containing means is housed within a second fluid-tight chamber.

11. An absorptiometer as set forth in claim 7, wherein all of said chambers are housed within at least one fluid-tight chamber.

12. An absorptiometer as set forth in claim 1, wherein said chamber is maintained at a lower pressure than the atmospheric pressure.

13. An absorptiometer as set forth in claim 1, including means for maintaining said chamber at a constant temperature.

14. An absorptiometer as set forth in claim 1, wherein said sample containing means is composed of a flow cell.

15. An absorptiometer as set forth in claim 1, wherein a pipe through which a liquid to be detected passes is thermally conductively contacted to a member which is thermally conductively coupled to said sample containing means.

16. An absorptiometer as set forth in claim 14, wherein said absorptiometer is used as a detector for a liquid chromatography.

17. A high sensitivity absorptiometer comprising a light source lamp with an inevitable heat generation, sample containing means through which light from said light source lamp is caused to pass, an optical fiber having a light input end face positioned in contact with a surface portion of said light source lamp and serving to guide the light from said light source lamp to said sample containing means, and detecting means for detecting light transmitted through said sample containing means.

18. A high sensitivity absorptiometer comprising a light source lamp with an inevitable heat generation, sample containing means through which light emitted from said light source lamp is caused to pass, detecting means for detecting light transmitted through said sample containing means, an optical fiber for guiding the light from said light source lamp to said sample containing means, and a fluid-tight chamber formed by at least a surface portion of said light source lamp, an enclosing wall member closely fitted to said surface portion and a light input end face of said optical fiber.